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Dimensional Metrology with Small Angle X-ray Scattering
  Sidewall Angle Metrology
  Dimensional Changes during Fabrication
Characterization of Porous Low-k Dielectric Thin Films
 
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Dimensional Metrology with Small Angle X-ray Scattering

 

Introduction

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Dimensional Metrology with Small Angle X-ray Scattering
  • Sidewall angle is one of five major inspection metrology challenges in the “International Technology Roadmap for Semiconductors” (ITRS).
  • Need for fast, nondestructive measurement method.
  • Cross-sectional SEM and AFM cannot meet projected need.
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    Experimental Approach

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    Dimensional Metrology with Small Angle X-ray Scattering: Experimental Approach
  • Measurement of a test sample at multiple angles of incidence
    Construct Fourier space map of the pattern cross section.
  • Left: Theoretical result of this protocol for a model trapezoid The intensity streaks provide the sidewall angle.
  • The intensity map also provides a check for a particular model cross-sectional profile; a limitation in current metrologies such as light scatterometry.
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    Results

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    Results
  • Left: The intensity of one Bragg diffraction peak recorded as a function of sample rotation angle. This data is compared with the theoretical model.
  • The distance between the maxima determines the average sidewall angle of the features.
  • For a trapezoidal cross section, the sidewall angle precision is approximately +/- 0.2 degrees.
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    Additional Benefits

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  • Method applicable to dense, high aspect ratio patterns, even sub-10 nm.
  • Methodology applicable to arbitrary cross section, requiring only the solution of a new model for analysis.
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    Publication

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    “Sidewall and Pattern Cross Section Metrology using Small Angle X-ray Scattering”
    Journal of Applied Physics to appear in 2004.
     

    NIST Contributors

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    Wen-li Wu*
    Ronald L. Jones*
    Tengjiao Hu
    Christopher Soles
    Bryan Vogt
    Eric Lin
     

    Collaborators:

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    Diego Casa (Argonne)
    Qinghuang Lin (IBM)
     
     
     
     
     
     
     
     
     
     
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    Electronics Materials Group
    Polymers Division
    Materials Science and Engineering Laboratory

     
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