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Onsite Research
Process Development

The goal of Process Development research at NETL is to generate information to help improve processes used in the production of materials that are being developed to improve efficiency and performance of power plant operation. Some of this research is helping to prove the feasibility of new fabrication processes used, for example, to produce economical, high-performance solid oxide fuel cells. In addition, process development research has a goal to protect the environment by developing effective, reliable, and affordable technologies for capturing and ameliorating the waste streams of fossil energy power production. By developing innovations that will form the basis of future power generation, process development is advancing the efficiency of the Nation's energy systems by evaluating and improving processes in existing power systems.

Process Development research specializes in the development of processes to:

  • efficiently produce prototype parts, castings, and/or plate or sheet from ferrous, non-ferrous, and refractory alloys;
  • formulate and develop alloys for use in high temperature applications;
  • recover or recycle valuable materials from wastes;
  • improve material production by melting or smelting;
  • develop processes for efficient carbon management including the sequester of greenhouse gas emissions;
  • improve efficiencies of high temperature melting or smelting systems; and
  • improve power plant efficiency, and reduce power plant emissions.

NETL understands and respects the need for confidentiality and the value of intellectual property that is developed in the conduct of all research conducted with industrial partnerships such as these. NETL partnership agreements are designed to protect company-specific proprietary information and intellectual property developed during a cooperative research agreement. NETL continues to develop new partnerships to collaborate with industry, for example, to s upport the development of new combustion technologies by providing solutions to the complex interactions of high temperature combustion and energy processes with the materials and metals that will be employed in these service environments .

The Liquid Metal Processing (LMP) Laboratory provides capabilities to melt, alloy, cast, forge, roll, and heat treat materials from a few grams up to 100s of kilograms. In addition, the division has a complete feed preparation facility capable of crushing, grinding, sizing, mixing, and agglomerating feed in batches from a few kg up to 1,000s of kg. For melting and smelting experimentation, the PDD has a state-of-the-art facility that allows for laboratory-scale (a few kg) up to pilot-scale (500 to 1,000 kg per hour of product) experimental trials that can be designed to last from a few seconds to more than 100 hours of continuous operation. With the excellent support that includes a state-of-the-art analytical laboratory , an outstanding mechanical testing facility, a world class metallography laboratory, a unique corrosion testing facility , and an experienced wear testing group, all products can be given a complete characterization with respect to chemical and phase composition, physical and mechanical properties, and wear and corrosion resistance.

Cooperative efforts with other industrial, academic, and governmental partners over the last 15 years have produced new processes and materials for use in many applications. Some examples include:
Alloy development:
1989-2004: Developed a new, lower-cost titanium alloys for use in non-aerospace applications to include military armor applications.
1992-2004: Developed a new, high density alloy for use in ballistic applications.
2000-2004: Developed a new precious metal/stainless steel alloy for medical devices.
2003-2004: Developed a new alloy for use in reciprocating saw blades.
2005-ongoing: Developed new alloys for use in high temperature applications such as solid oxide fuel cell components.
2005-ongoing: Developed a new, rare earth, surface treatment that improves the high- temperature corrosion resistance of alloys.
   
Casting:
1989-1996: Adapting the lost foam process for use in precision casting of steel armor for the Department of Defense.
1996-1998: Developed a process to centrifugally cast hardfaced aluminum camshafts and other rotating parts.
1994-2002: Developed a method to continuously cast titanium using induction furnace-based technology.
1998-2004: Developed a process to produce extremely thin wall steel castings for use in the transportation industry.
   
Cupola furnace technology:
1993-2003: Developed cupola furnace-based processes to model basic cupola practices; recover iron and zinc from steel making wastes; and recover metal values from high lime content steel making wastes.
   
Electric furnace technology:
1990-1993: Consulting role with the Defense Technology Security Agency to prevent the spread of nuclear technology.
1991-2004: The development of electric arc furnace-based processes to recover metal values from ores and steel making wastes; recover precious metals from converter wastes; and cast magnetite and nickel ferrites.
2005-ongoing: NETL Liquid Metals Processing Laboratory. Beginning in 2005, in conjunction with Sandia National Laboratory, a facility capable of melting and casting specialty metals with capacities from grams to over 500 Kg was established. Over the next 3 years, this facility will transfer, set up, and utilize larger scale melting equipment formerly sited at Sandia that will complement the existing smaller scale (grams to 50 Kg) equipment presently in use at the site. Upon completion, this unique facility will be used to study every aspect of electric furnace melting of specialty alloys and will be capable of producing large-scale prototype alloys and castings.
   
Environmental technology:
1989-1992: Developed a process to vitrify and detoxify municipal incinerator residues.
1992-1994: Developed a process to vitrify mixed wastes (hazardous and radioactive) that consolidated the material into a more disposable form.
1994-1996: Developed a process to turned liquid, radioactive tank wastes into a borosilicate glass suitable for long term storage.
1995-1997: Developed a process to vitrify naval shipyard residues, concentrating the hazardous elements into 6 pct of the original material with the balance landfillable.
1999-2004: Developed a method and accurate economic analysis of the process for long-term storage of atmospheric carbon dioxide as a mineral carbonate.
2004-ongoing: Developed a process for integrated pollutant removal from fossil fuel-fired power plants which, in conjunction with an oxy-fuel burner system, collects all of the pollutants into a CO 2 -rich stream that is 0.03 pct of the original volume for a conventional power plant.
2005-ongoing: Developed a process to seal CO 2 reservoirs to prevent leakage.
   
Fossil-Fuel Fired Melting Technology:
1999-2004: Developed processes to reduce cracking of large aluminum ingots and the production of dross during melting operation.
1999-2005: Developed processes for improving the efficiency in secondary melting of aluminum in fossil-fuel fired aluminum melters.
   
Power Plant Technology:
1994-2006: Worked with the USAID and the Indonesian Director General for Electricity and Energy Development to institute root-cause analysis for the identification of power generation problems, introduce fuel testing and treatment method and draft new energy policy, rules, and regulations;
2003-ongoing: In co-operation with the Iraq Coalition Provisional Authority (CPA) Electricity Office and the Iraqi Ministries of Electricity and Oil, developed methods to utilize alternate fuels for increased electric power generation and advised the CPA and Iraqi Ministries on ways to expedite the restoration of the Iraqi power grid.
   
Examples of our governmental, academic, and industrial partners in the past 15 years include:
  • AJT Enterprises, Inc.
  • Ames Laboratory
  • ALLVAC
  • Army Research Laboratory
  • Arizona State University
  • Boston Scientific
  • Coalition Provisional Authority Corus Staal
  • General Motors Corporation
  • Defense Technology Security Agency
  • Department of State Dow Chemical Corporation
  • Dow Corning Corporation
  • U. S. DOE, Office of Energy Efficiency and subsidiaries
  • Enercon, Inc.
  • Engelhard Corporation
  • Environ Metal, Inc.
  • Hedman Resources, Ltd.
  • Idaho National Environmental and Engineering Laboratory
  • International Titanium Powder, LLC
  • InterVentional Technologies, Inc.
  • Iraqi Reconstruction Management Organization
  • Jupiter Oxygen Corporation
  • Jim Ogilvy, father of modern military titanium applications
  • Los Alamos National Laboratory
  • Oxide Recovery Limited
  • PEL Technologies
  • RMI , Inc.
  • ScandUS
  • Secat, Inc. Specialty Metals Processing Consortium
  • TIMET, Inc.
  • United States Army Tank and Automotive Command
  • United States Army Materials Command
  • University of Idaho
  • University of Kentucky
  • University of Tennessee
  • Westinghouse Hanford Corporation