Polymer division banner Polymer division home page Research areas link Research projects link Research facilities link Staff contact link Search link NIST link Polymer division home page Materials Science and Engineering Laboratory  
  `

Research Facilities

The Polymers Division has several state of the art laboratories and facilities which are available for your research needs. Detailed information about each facility describing its capabilities, typical applications, and availability is provided in the links below. Please also note the NIST disclaimer.
 
 

Small Angle X-ray Scattering (SAXS) Facility

SAXS is a powerful non-destructive technique to probe the structure of materials over length scales of (1 to 100) nm. The SAXS facility in the Division is unique with several configurations available through two target sources, a Bonse-Hart camera, and a pinhole geometry.
bullet More information on Small Angle X-Ray Scattering Facility
 
 

X-Ray Reflectivity Facility

X-ray reflectivity is a non-destructive technique for characterizing surfaces of solids and liquids in terms of their roughness and electron density depth profile. A depth up to micrometers can be resolved with a resolution less than one nanometer. This capability makes it an ideal tool for characterizing thin films.
bullet More information on X-Ray Reflectivity Facility
 
 

Neutron Reflectivity Facility

The polymers division at NIST utilizes neutron reflection (NR) for probing a wide range of surface and interfacial problems in polymer science.
bullet More information on Neutron Reflectivity Facility
 
 

Small Angle Neutron Scattering Facility

The US's leading neutron scattering facility is maintained by the NIST Center for Neutron Research. Neutron scattering is used to probe molecular and microstructural features of polymers and other materials. Within the Facility there is an 8 m beam line that is particularly useful for studies of polymers.
bullet More information on Small Angle Neutron Scattering Facility
 
 

Macromolecular Mass Spectrometry

The Mass Spectrometry Facility is used in the measurement of molecular mass and molecular mass distribution of synthetic polymers, as well as in studies of the molecular architecture of prepolymers and copolymers.
MALDI Mass Spectrometer
bullet More information on Mass Spectrometery Facility
 
 

Fiber-Matrix Interface Strength Facility

NIST has three machines used to measure and assess the interfacial shear properties between fibers and polymeric matrices. The first is an automated single fiber fragmentation testing (SFFT) machine. The second is a manual sfft machine. The third is a microdrop shear apparatus.

Fiber-Matrix Interface Strength Facility

bullet More information on Fiber-Matrix Interface Strength Facility
 
 

Combinatorial Methods

Novel combinatorial methods for polymer "library" design and characterization have been developed in the Polymers Division. These include gradient flow coating with elevated temperature control, automated interferometric mapping of film thickness and refractive index, composition gradient library preparation, UV and wet etch for gradient surface hydrophobicity modification of inorganic and polymer surfaces, infrared spectroscopic composition mapping, temperature gradient processing stage, automated optical reflection and transmission microscopy with polarization and process control programming, automated multi-solvent contact angle instrument, high throughput opto-adhesion methodology, and state of the art on-line data analysis tools for image and pattern processing.
bullet More information on Combinatorial methods
 
 

Optical Coherence Tomography Facility

Optical coherence tomography (OCT) is a powerful tool for non-destructive, bulk volumetric imaging of synthetic materials. With this technique, information about features with a size of 10 mm and above is obtained. A requirement for this type of tomography is that the material be transparent to near infrared light, making many polymer systems excellent candidates.

bullet More information on Optical Coherence Tomography Facility
 
 

Extrusion Visualization Facility

An instrumented slit die located at the exit of a twin screw extruder allows in-situ optical measurements of blend morphology and critical processing parameters. The combination of in-line optical microscopy and light scattering probes a size range from 0.1 microns to 100 microns. The facility has been used for the study of polymer blends, reactive blends, in-situ fiber formation and slippage.
Extrusion Visualization Facility
bullet More information on Extrusion Visualization Facility
 
 

Mercury Dilatometer Facility

The Mercury Dilatometer Facility is used for the kinetic measurement of volumetric changes in polymers. It is ideal for dynamically determining the rate and time dependence of shrinkage or expansion in polymetric materials subjected to chemical or photo polymerization.

 

Mercury Dilatometer Facility
bullet More information on Mercury Dilatometer Facility
 
 
 
NIST Materials Science & Engineering Laboratory - Polymers Division
  line
 
 
Research Facilities
   
bullet Small Angle X-ray Scattering
   
bullet X-Ray Reflectivity
   
bullet Neutron Reflectivity
   
bullet Small Angle Neutron Scattering
   
bullet Macromolecular Mass Spectrometry
   
bullet Fiber-Matrix Interface Strength
   
bullet Combinatorial Methods
   
bullet Optical Coherence Tomography
   
bullet Extrusion Visualization
   
bullet Mercury Dilatometer
   
 
 
 
 
line