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Extrusion Visualization Facility

 
An instrumented slit die located at the exit of a twin screw extruder allows in-situ optical measurements of blend morphology and critical processing parameters. The combination of in-line optical microscopy and light scattering probes a size range from 0.1 microns to 100 microns. The facility has been used for the study of polymer blends, reactive blends, in-situ fiber formation and slippage.
 
Extrusion Visualization Facility graphic
 
The properties of a polymeric material can frequently be enhanced by blending it with a second immiscible polymer containing synergistic properties. An example is the blending of rubber into nylon, in which a significant increase in impact strength can be acheived. The final properties depend strongly on the morphology of the dispersed phase.
 
Extrusion Visualization Facility Graphic
 
The shear stress in the channel has a profound effect on the morphology as seen in these three light scattering (upper panel) / optical microscopy (panel) pairs. At low shear (left side) , the disperesed phases is shperical. At intermediate shear, long fibers of the dispersed phase form, parallel to the shear direction. At higher shear (right side), the fibers break up into ellipsoidal droplets.
 

Contact Information

 
Dr. Kalman Migler
Polymers Division
National Institute of Standards and Technology

Tel: 301 975 4876
Fax:301-975-4924
Email: Kalman.Migler@NIST.gov


 
NIST Materials Science & Engineering Laboratory - Polymers Division
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Research Facilities
   
bullet Small Angle X-ray Scattering
   
bullet X-Ray Reflectivity
   
bullet Neutron Reflectivity
   
bullet Small Angle Neutron Scattering
   
bullet Macromolecular Mass Spectrometry
   
bullet Fiber-Matrix Interface Strength
   
bullet Combinatorial Methods
   
bullet Optical Coherence Tomography
   
bullet Extrusion Visualization
   
bullet Mercury Dilatometer
   
 
 
 
 
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