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Analytical Chemistry Division Publications in 2009

The following papers were published in 2009. If your institution subscribes to the journal named, clicking on an individual reference will direct you to the journal's website, where you can access the publication. If NIST has the right to post a reprint, clicking on the link will provide you with a pdf copy of the paper. [Note: Linking to these pages is currently in progress.]

Addona, T., Abbatiello, S. E., Schilling, B., Skates, S. J., Mani, D. R., Bunk, D. M., Spiegelman, C. H., Zimmerman, L. J., Ham, A. L., Keshishian, H., Hall, S. C., Allen, S., Blackman, R. K., Borchers, C. H., Buck, C., Cardasis, H. L., Cusack, M. P., Dodder, N. G., Gibson, B. W., Held, J. M., Hiltke, T., Jackson, A., Johansen, E. B., Kinsinger, C. R., Li, J., Mesri, M., Neubert, T. A., Niles, R. K., Pulsipher, T. C., Rodriguez, H., Rudnick, P. A., Smith, D., Tabb, D. L., Tegeler, T. J., Variyath, A. M., Vega-Montoto, L., Wahlander, A., Waldemarson, S., Wang, M., Whiteaker, J. R., Zhao, L., Anderson, N. L., Fisher, S. J., Liebler, D. C., Paulovich, A. G., Regnier, F. E., Tempst, P., Carr, S. A., and CPTAC Network, "Multi-site Assessment of the Precision and Reproducibility of Multiple Reaction Monitoring-based Measurements of Proteins in Plasma," Nat. Biotechnol., 27(7):633-U85 (2009)

Baer, I., de la Calle, B., Sander, L. C., Verbist, I., Vendelbo, D., Emteborg, H., and Taylor, P., "IMEP-28: Total Arsenic, Cadmium, Lead and Mercury in Food Supplements," JRC Scientific and Technical Reports, JRC 55721:1-44 (2009)

Bode, P., Greenberg, R. R., and De Nadai Fernandes, E. A., "Neutron Activation Analysis: A Primary (Ratio) Method of Measurement to Determine SI-Traceable Values of Element Content in Complex Samples," Chimia, 63(12):678-680 (2009)

Boroujerdi, A. F. B., Vizcaino, M. I., Meyers, A., Pollock, E. C., Huynh, S. L., Schock, T. B., Morris, P. J., and Bearden, D. W., "NMR-Based Microbial Metabolomics and the Temperature-Dependent Coral Pathogen Vibrio coralliilyticus," Environ. Sci. Technol., 43(20):7658-7664 (2009)

Brennan, R., Rabb, S., Holden, M., Winchester, M. R., and Montaser, A., "Potential Primary Measurement Tool for the Quantification of DNA," Anal. Chem., 81(9):3414-3420 (2009)

Brennan, R. G., Rabb, S. A., Jorabchi, K., Rutkowski, W. F., Montaser, A., and Turk, G. C., "Heat-Assisted Argon Electrospray Interface for Low-Flow Rate Liquid Sample Introduction in Plasma Spectrometry," Anal. Chem., 81(19):8126-8133 (2009)

Decker, J. E., Hight Walker, A. R., Bosnick, K., Clifford, C. A., Dai, L., Fagan, J., Hooker, S., Jakubek, Z.J., Kingston, C., Makar, J., Mansfield, E., Postek, M. T., Simard, B., Sturgeon, R., Wise, S., Vladar, A. E., Yang, L., and Zeisler, R., "Sample Preparation Protocols for Realization of Reproducible Characterization of Single-Walled Carbon Nanotubes,"  Metrologia, 46(6):682-692 (2009)

De la Calle Guntinas, M. B., Sander, L. C., Long, S. E., Christopher, S. J., Day, R. D., Murphy, K. E., Cordeiro Raposo, F., Linsinger, T., Emteborg, H., Verbist, I., and Vendelbo, D., "Report of the Sixth Interlaboratory Comparison Organised by the Community Reference Laboratory for Heavy Metals in Feed and Food – Total Cd, Pb, As and Hg in Food Supplements," JRC Scientific and Technical Reports, JRC54402:1-42 (2009)

Duewer, D. L., Lippa, K. A., Long, S. E., Murphy, K. E., Sharpless, K. E., Sniegoski, L. T., and Welch, M. J., "Demonstrating the Comparability of Certified Reference Materials," Anal. Bioanal. Chem., 395(1):155-169 (2009)

Duewer, D. L., May, W. E., Parris, R. M., Schantz, M. M., Wise, S. A., Piechotta, C., Philipp, R., Win, T., Avila, M., Pérez Urquiza, M., Ulberth, F., Kim, B., Ishikawa, K., Chen, D., Krylov, A. I., Kustidov, Y. A., and Lopushanskaya, E. M., "Final Report on CCQM-K38: Determination of PAHs in Solution," Metrologia, 46(Tech Suppl 1A):08003 (2009)

Epstein, M., Miles, D., and Yu, L. L., "What Were They Drinking? A Critical Study of the Radium Ore Revigator," Appl. Spectrosc. , 63(12):1406-1409 (2009)

Fletcher, R. A., Mulholland, G. W., Winchester, M. R., King, R. L., and Klinedinst, D. B., "Calibration of a Condensation Particle Counter Using a NIST Traceable Method," Aerosol Sci. Technol., 43(5):425-441 (2009)

Gupta, S., Muralikiran, M., Farmer, J., Cao, L. R., and Downing, R. G., "The Effect of Boron Doping and Gamma Irradiation on the Structure and Properties of Microwave Chemical Vapor Deposited Boron-Doped Diamond Films," J. Mater. Res., 24(4):1498-1512 (2009)

Holden, M. J., Haynes, R. J., Rabb, S. A., Blasic, J., Satija, N., and Yang, K., "Factors Affecting Quantification of Total DNA by UV Spectroscopy and PicoGreen Fluorescence,"  J. Agric. Food. Chem., 57(16):7221-7226 (2009)

Holmes, G., Park, E. S., Guttman, C., Flynn, K., Sieber, J. R., Watson, S., and Rice, K., "A Coherent Approach for Interrogating Polybenzoxazole Fibers for Residual Phosphoric Acid," NISTIR 7573, National Institute of Standards and Technology, Gaithersburg, MD (2009)

Keller, J. M., Swarthout, R. R., Carlson, B. K. R., Yordy, J., Guichard, A., Schantz, M. M., and Kucklick, J. R., "Comparison of Five Extraction Methods for Measuring PCBs, PBDEs, Organochlorine Pesticides, and Lipid Content in Serum," Anal. Bioanal. Chem., 93(2):747-760 (2009)

Kilpatrick, E. L. and Bunk, D. M., "Reference Measurement Procedure Development for C-Reactive Protein in Human Serum," Anal. Chem., 81(20):8610-8616 (2009)

Kipphardt, H., Matschat, R., Vogl, J., Gusarova, T., Czerwensky, M., Heinrich, H-J., Hioki, A., Konopelko, L. A., Methven, B., Miura, T., Petersen, O., Riebe, G., Sturgeon, R., Turk, G. C., and Yu, L. L., "Purity Determination as Needed for the Realisation of Primary Standards for Elemental Determination:  Status of International Comparability," Accredit. Qual. Assur., 15(1):29-37 (2009)

Kline, M. C., Duewer, D. L., Travis, J. C., Smith M.V., Redman, J. W., Vallone, P. M., Decker, A. E., and Butler, J. M., "Production and Certification of NIST Standard Reference Material 2372 Human DNA Quantitation Standard," Anal. Bioanal. Chem., 394:(4)1183-1192 (2009)

Kucklick, J. R., Pugh, R. S., Becker, P. R., Guichard, A., Schantz, M. M., Wise, S. A., and Rowles, T. K., "Description and Results of the 2007 NIST/NOAA Interlaboratory Comparison Exercise Program for Organic Contaminants in Marine Mammal Tissues," NISTIR 7642, National Institute of Standards and Technology, Gaithersburg, MD (2009)

Kühnle, M., Friebolin, V., Albert, K., Rimmer, C. A., Lippa, K. A., and Sander, L. C., "Architecture and Dynamics of C18 Bonded Interphases with Small Molecule Spacers," Anal. Chem., 81(24):10136-10142 (2009)

Liao, W. L., Dodder, N. G., Mast, N., Pikuleva, I. A., and Turko, I. V., "Steroid and Protein Ligand Binding to Cytochrome P450 46A1 as Assessed by Hydrogen-Deuterium Exchange and Mass Spectrometry," Biochemistry, 48(19):4150-4158 (2009) Liao, W. L. and Turko, I. V., "Accumulation of Large Protein Fragments in Prematurely Senescent ARPE-19 Cells," Invest. Ophthalmol. Vis. Sci., 50(10):4992-4997 (2009)

Lindstrom, R. M., "Errors, PGAA, and Metrology," J. Radioanal. Nucl. Chem., 282(1):5-9 (2009)

Louchouarn, P., Kuo, L. J., Wade, T. L., and Schantz, M. M., "Determination of Levoglucosan and its Isomers in Size Fractions of Aerosol Standard Reference Materials," Atmos. Environ., 43(35):5630-5636 (2009)

MacCrehan, W. A., "A NIST Standard Reference Material (SRM) to Support the Detection of Trace Explosives," Anal. Chem., 81(17):7189-7196 (2009)

MacDonald, B. S., Molloy, J. L., Leigh, S. D., Kelly, W. R., and Rukhin, A. L., "A Statistic that Identifies Errant Standard Preparation and Instrument Nonlinearity Demonstrated with Mercury Standards Prepared by Blending NIST Fossil Fuel CRMs of Similar Matrices," Energy Fuels, 23:6048-6054 (2009)

Mackey, E. A. and Spatz, R. O., "Assessment of Stability of Trace Elements in Two Natural Matrix Environmental Standard Reference Materials: NIST-SRM 1547 Peach Leaves and NIST-SRM 1566a Oyster Tissue," J. Radioanal. Nucl. Chem., 281(1):91-96 (2009)  

Mann, J. L., Vocke, R. D., and Kelly, W. R., "Revised d 34S Reference Values for IAEA Sulfur Isotope Reference Materials S-2 and S-3," Rapid Commun. Mass Spectrom., 23:(8)1116-1124 (2009)

Mariassy, M., Pratt, K. W., and Spitzer, P., "Major Applications of Electrochemical Techniques at National Metrology Institutes," Metrologia, 46(3):199-213 (2009)

Mast, N., Liao, W. L., Pikuleva, I.A., and Turko, I.V., "Combined Use of Mass Spectrometry and Heterologous Expression for Identification of Membrane-Interacting Peptides in Cytochrome P450 46A1 and NADPH-Cytochrome P450 Oxidoreductase," Arch. Biochem. Biophys., 483(1):81-89 (2009)

Miller, W. G., Bruns, D. E., Hortin, G. L., Sandberg, S., Aakre, K. M., McQueen, M. J., Itoh, Y., Lieske, J. C., Seccombe, D. W., Jones, G., Bunk, D. M., Curhan, G. C., and Narva, A. S., "Current Issues in Measurement and Reporting of Urinary Albumin Excretion," Clin. Chem., 55:(1)24-38 (2009)

Moss, S., Keller, J.M., Richards, S., and Wilson, T.P., "Concentrations of Persistent Organic Pollutants in Plasma from Two Species of Turtle from the Tennessee River Gorge," Chemosphere, 76(2):194-204 (2009)

Murphy, K. E., Guthrie, W. F., Vetter, T. W., Turk, G. C., Palmer, C. D., Lewis, M. E., Geraghty, C. M., and Parsons, P. J., "Comparison of Clinical Methods with Isotope Dilution Inductively Coupled Plasma Mass Spectrometry for the New Standard Reference Material 955c Lead in Caprine Blood," J. Anal. At. Spectrom., 24(9):1170-1178 (2009)

Newman, J. D. S. and MacCrehan, W. A., "The Effect of Aniline Concentration in the Ligand Exchange Reaction with Citrate-Stabilized Gold Nanoparticles," Langmuir, 25(16):8993-8998 (2009)

Park, E. S., Sieber, J. R., Guttman, C., Rice, K., Flynn, K., Watson, S., and Holmes, G., "A Methodology for Detecting Residual Phosphoric Acid In Polybenzoxazole Fibers," Anal. Chem., 81(23):9607-9617 (2009)

Paul, R. L., Mackey, E. A., Zeisler, R., Spatz, R. O., and Tomlin, B. E., "Determination of Elements in SRM Soil 2709a by Neutron Activation Analysis," J. Radioanal. Nucl. Chem., 282(3):945-950 (2009)

Phelan, D., Millican, J. N., Thomas, E. L., Leao, J. B., Qiu, Y., and Paul, R. L., "Neutron Scattering Measurements of the Phonon Density of States of FeSe1-x Superconductors," Phys. Rev., B79:014519 (2009)

Pugh, R. S., Ellisor, M. B., Moors, A. J., Porter, B. J., Kucklick, J. R., Christopher, S. J., Davis, W. C., and Becker, P. R., "National Marine Mammal Tissue Bank 2007-2008,"  NISTIR 7675, National Institute of Standards and Technology, Gaithersburg, MD (2009)

Rhoderick, G. C., Thorn III, W. J., Miller, Jr. W. R., Guenther, F. R., Gore, E., and Fish, T., "Gas Standards Development in Support of NASA's Space Shuttle Monitoring Program," Anal. Chem., 81(10):3809-3815 (2009)

Rimmer, C. and Sander, L. C., "Shape Selectivity in Embedded Polar Group Stationary Phases for Liquid Chromatography," Anal. Bioanal. Chem., 394(1):285-291 (2009)

Samuels, M., Gulati, G., Shin, J. H., Opara, R., McSweeney, E., Sekedat, M., Long, S. E., Kelman, Z., and Jeruzalmi, D., "A Biochemically Active MCM-Like Helicase in Bacillus cereus," Nucleic Acids Res., 37(13):4441-4452 (2009)

Sander, L. C., Schantz, M. M., Sharpless, K. E., and Wise, S. A., "Standard Reference Materials to Support Measurement of Fatty Acids," Lipid Technology, 21(1):7-12 (2009)

Schantz, M. M., Christopher, S., Davis, W., Day, R., Keller, J., Kucklick, J., Long, S. E., Mackey, E., Point, D., Porter, B. J., Poster, D. L., Sharpless, K. E., Turk, G. C., and Wise, S. A., "Spotlighting NIST SRMs: Fish-Related Standard Reference Materials," Am. Lab., 41(2):50- (2009)

Shoenfelt, J., Mitkus, R. A., Zeisler, R., Spatz, R. O., Powell, J., Fenton, M. J., Squibb, K. A., and Medvedev, A. E., "Involvement of TLR2 and TLR4 in Inflammatory Immune Responses Induced by Fine and Coarse Ambient Air Particulate Matter," J. Leukocyte Biol., 86(2):303-312 (2009)

Sieber, J., "Portable X-ray Fluorescence Spectrometry Capabilities for In Situ Analysis," X-Ray Spectrom., 38(2):157 (2009)

Tomlin, B. E. and Zeisler, R., "Improvements in Determinations Using the Cu-64 Annihilation Gamma-Rays," Appl. Radiat. Isot., 67(12):2075-2078 (2009)

VanderPol, S. S., Becker, P. R., Chen, G. K., Ellisor, M. B., Moors, A. J., Pugh, R. S., Roseneau, D. G., and Simac, K. S., "Monitoring Organic Contaminants in Eggs of Glaucous and Glaucous-Winged Gulls (Larus hyperboreus and Larus glaucescens) from Alaska," Environ. Pollut., 157(3):755-762 (2009)

Vesper, H. W., Bhasin, S., Wang, C., Tai, S. S., Dodge, L. A., Singh, R. J., Nelson, J., Ohorodnik, S., Clarke, N. J., Salameh, W. A., Parker, Jr. C. R., Razdan, R., Monsell, E. A., and Myers, G. L., "Interlaboratory Comparison Study of Serum Total Testosterone [corrected] Measurements Performed by Mass Spectrometry Methods," Steroids, 74:(6)498-503 (2009)

Viant, M., Bearden, D., Bundy, J., Burton, I., Collette, T., Ekman, D., Karakach, T., Lin, C. Y., Rochfort, S., de Ropp, J., Teng, Q., Tjeerdema, R., Walter, J., and Wu, H., "International NMR-based Environmental Metabolomics Intercomparison Exercise," Environ. Sci. Technol., 43:(1)219-225 (2009)

Wang, L. L., Bunk, D. M., He, H. J., and Cole, K. D., "Removal of Inhibitory Effects in a Serum Cardiac Troponin I Immunoassay," Clin. Chem., 55(11):2055-2056 (2009)

Westwood, S., Josephs, R., Daireaux, A., Wielgosz, R., Davies, S., Kang, M., Ting, H., Phillip, R., Malz, F., Shimizu, Y., Frias, E., Pérez Urquiza, M., Apps, P., Fernandes-Whaley, M., De Vos, B., Wiangnon, K., Ruangrittinon, N., Wood, S., Duewer, D. L., Schantz, M. M., Bedner, M., Hancock, D., and Esker, J., "An International Comparison of Mass Fraction Purity Assignment of Theophylline: The Comité Consultatif pour la Quantité de Matière (CCQM) Pilot Study CCQM-P20.e(Theophylline)," Metrologia, 46:(Tech Suppl)08019- (2009)

Whitney, S. M., Biegalski, S. R. F., and Downing, R. G., "Benchmarking and Analysis of 6Li Neutron Depth Profiling of Lithium Ion Cell Electrodes," J. Radioanal. Nucl. Chem., 282(1):173-176 (2009)

Winchester, M. R., Turk, G. C., Butler, T. A., Oatts, T. J., Coleman, C., Nadratowski, D., Sud, R., Hoover, M. D., and Stefaniak, A. B., "Certification of Beryllium Mass Fraction in SRM 1877 Beryllium Oxide Powder Using High-Performance Inductively-Coupled Plasma Optical Emission Spectrometry with Exact Matching," Anal. Chem., 81:(6)2208-2217 (2009)

Zeisler, R., Tomlin, B. E., Murphy, K. E., and Kučera, J., "Neutron Activation Analysis with Pre- and Post- Irradiation Chemical Separation for the Value Assignments of Al, V, and Ni in the New Bovine Liver SRM 1577c," J. Radioanal. Nucl. Chem., 282(1):69-74 (2009)

Zeisler, R., Greenberg, R. R., Mackey, E. A., Murphy, K. E., Spatz, R. O., and Tomlin, B. E., "Challenges and Successes in the Use of Neutron Activation Analysis Procedures for Value Assignment of Animal Serum and Bovine Liver Standard Reference Materials," J. Radioanal. Nucl. Chem., 281 (1):11-15 (2009)  

Zeisler, R., Heller, Zeisler, S. F., Unlu, K., and Williamson, C., "Current Status, Trends, and Needs in Radiochemical Education: The US and Abroad," Am. Inst. Phys. Conf. Proc., 1164:3-8 (2009)