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Analytical Chemistry Division Publications in 2008

The following papers were published in 2008. If your institution subscribes to the journal named, clicking on an individual reference will direct you to the journal's website, where you can access the publication. If NIST has the right to post a reprint, clicking on the link will provide you with a pdf copy of the paper. [Note: Linking to these pages is currently in progress.]

Arsene, C. G., Ohlendorf, R., Burkitt, W., Pritchard, C., Henrion, A., O’Connor, G., Bunk, D. M., and Guttler, B., “Protein Quantification by Isotope Dilution Mass Spectrometry of Proteolytic Fragments: Cleavage Rate and Accuracy” Anal. Chem., 80(11):4154-4160 (2008)

Bedner, M., Schantz, M. M., Sander, L. C., and Sharpless, K. E., “Development of Liquid Chromatographic Methods for the Determination of Phytosterols in Standard Reference Materials Containing Saw Palmetto,” J. Chromatogr. A., 1192 (1):74-80 (2008)

Burkitt, W., Pritchard, C., Arsene, C., Henrion, A., Bunk, D. M., and O’Connor, G., “Toward Système International d’Unité-Traceable Protein Quantification: From Amino Acids to Proteins,” Anal. Bioanal. Chem., 376(2):242–251 (2008)

Cetiner, S. M., Unlu, K., and Downing, R.G., “Development and Applications of Time-of-Flight Neutron Depth Profiling (TOF-NDP),” J. Radioanal. Nucl. Chem., 276(3):623-630 (2008)

Christopher, S., Pugh, R. S., Moors, A. J., Ellisor, M. B., Mackey, E., Spatz, R. O., Porter, B. J., Bealer, K., Kucklick, J., Becker, P. R., and Rowles, T. K., “National Marine Analytical Quality Assurance Program: Results and Description of the NIST/NOAA 2007 Interlaboratory Comparison Exercise for Trace Elements in Marine Mammals,” NISTIR 7528, National Institute of Standards and Technology, Gaithersburg, MD (2008)

DeLorenzo, M. E., Keller, J. M., Arthur, C. D., Finnegan, M. C., Harper, H. E., Winder, V. L., and Zdankiewicz, D. L., “Toxicity of the Antimicrobial Compound Triclosan and Formation of the Metabolite Methyl-Triclosan in Estuarine Systems,” Environ. Toxicol., 23(2):224-232 (2008)

Downing, R. G., “High Resolution Position Sensitive Neutron Detector (HRPSND),” Neutron Radiography, 8:616-621 (2008)

Duewer, D. L., Schantz, M. M., Parris, R. M., and Ulberth, F., “Evaluation of Performance Characteristics of Multi-step Analytical Methods from Collaborative Study of Linked Samples,” Anal. Chem., 80(19):7327-7335 (2008)

Duewer, D. L., “The Distribution of Interlaboratory Comparison Data: Response to the Contribution by K. Heydorn,” Accredit. Qual. Assur., 13(12):725-726 (2008)

Duewer, D. L., “A Comparison of Location Estimators for Interlaboratory Data Contaminated with Value and Uncertainty Outliers,” Accred. Qual. Assur., 13(4-5):193-216 (2008)

Dwyer, J. T., Picciano, M. F., Betz, J. M., Fisher, K. D., Saldanha, L. G., Yetley, E.A., Coates, P.M., Milner, J. A., Whitted, J., Burt, V., Radimer, K., Wilger, J., Sharpless, K. E., Holden, J. M., Andrews, K., Roseland, J., Zhao, C., Schweitzer, A., Harnly, J., Wolf, W. R., and Perry, C. R., “Progress in Developing Analytical and Label-Based Dietary Supplement Databases at the NIH Office of Dietary Supplements,” J. Food Compos. Anal., 21:S83-S93, Suppl. S. (2008)

Fletcher, R. A., Brazin, J. A., Staymates, M. E., Benner, B. A., and Gillen, J. G.,“Fabrication of Polymer Microsphere Particle Standards Containing Trace Explosives Using an Oil/Water Emulsion Solvent Extraction Piezoelectric Printing Process,” Talanta, 76(4):949-955 (2008)

Goenaga-Infante, H., Sturgeon, R., Turner, J., Hearn, R., Sargent, M., Maxwell, P., Yang, L., Barzev, A., Pedrero, Z., Camara, C., Diaz Huerta, V., Fernandez Sanchez, M. L., Sanz-Medel, A., Emese, K., Fodor, P., Wolf, W., Goldschmidt, R., Vacchina, V., Szpunar, J., Valiente, L., Huertas, R., Labarraque, G., Davis, W. C., Zeisler, R. L., Turk, G. C., Rizzio, E., Mackay, L. G., Myors, R., Saxby, D., Askew, S., Chao, W., and Jun, W., “Total Selenium and Selenomethionine in Pharmaceutical Yeast Tablets; Assessment of the State-of-the-Art of Measurement Capabilities through International Intercomparison Study CCQM-P86,” Anal. Bioanal. Chem., 390(2):629-642 (2008)

Greenberg, R. R., “Pushing the Limits of NAA: Accuracy, Uncertainty and Detection Limits,” J. Radioanal. Nucl. Chem., 278(2):231-240 (2008)

Greenberg, R. R., “Final Report on Key Comparison CCQM-K49: Essential and Toxic Elements in Bovine Liver,” Metrologia Tech. Suppl., 45, (2008)

Holbrook, R. D., Murphy, K. E., Morrow, J. B., and Cole, K. D., “Trophic Transfer of Nanoparticles in a Simplified Invertebrate Food Web,” Nat. Nanotechnol., 3(6):352-355 (2008)

Kamangar, F., Schantz, M. M., Abnet, C. C., Fagundes, R. B., and Dawsey, S. M., “High Levels of Carcinogenic Polycyclic Aromatic Hydrocarbons in Mate Drinks,” Cancer Epidemiol Biomarkers Prev, 17(5):1262-1268 (2008)

Kelly, W. R., MacDonald, B. S., and Guthrie, W. F., “Gravimetric Approach to the Standard Addition Method in Instrumental Analysis - 1,” Anal. Chem., 80(16):6154-6158 (2008)

Liao, W-L. and Turko, I. V., “Strategy Combining Separation of Isotope-Labeled Unfolded Proteins and Matrix-Assisted Laser Desorption/Ionization Mass Spectrometry Analysis Enables Quantification of a Wide Range of Serum Proteins,” Anal. Bioanal. Chem., 377(1):55-61 (2008)

Lindstrom, R. M., Zeisler, R., Mackey, E. A., Liposky, P. J., Popelka-Filcoff, R. S., and Williams, R. E., “Neutron Irradiation in Activation Analysis: A New Rabbit for the NBSR,” J. Radioanal. Nucl. Chem. 278:665-669 (2008)

Lippa, K., Sieber, J., and Duewer, D. L., “D. Brynn Hibbert: Quality Assurance for the Analytical Chemistry Laboratory,” Accred. Qual. Assur., 13(2):115-116 (2008)

Mackey, E. A., Cronise, M. P., Fales, C. N., Greenberg, R. R., Leigh, S. D., Long, S. E., Marlow, A. F., Murphy, K. E., Oflaz, R., Sieber, J. R., Rearick, M. S., Wood, L. J., Yu, L. L., Hall, W., and Kane, P., “Multi-Nutrient Fertilizer Standard Reference Material for Trace Elements,” Am. Lab. News Edition, 40(17):20-21 (2008)

Mann, J. L., Shuman, C.A., Kelly, W.R., and Kreutz, K.J., “Seasonal 34S Variations in Two High Elevation Snow Pits Measured by 33S-36S Double Spike Thermal Ionization Mass Spectrometry,” Geochim. Cosmochim. Acta, 72(15):3907-3927 (2008)

Molloy, J. L., and Sieber, J. R., “Classification of Micoheterogeneity in Solid Samples Using mu XRF,” Anal. Bioanal. Chem., 392(5):995-1001 (2008)

Molloy, J.L., and Sieber, J.R., “Microscale Heterogeneity,” Anal. Bioanal. Chem., 392(5):1618-2642 (2008)

Mountain, R. D., and Lippa, K. A., “Solvation of Perfluorooctane and Octane in Water, Methanol, Acetonitrile, and Aqueous Mixtures of Methanol and Acetonitrile,” J. Phys. Chem. B, 112(26):7785-7793 (2008)

Nagourney, S. J., Wilson, S. A., Buckley, B., Kingston, H. M. S., Yang, S. Y., and Long, S. E., “Development of A Standard Reference Material for Cr(VI) in Contaminated Soil,” J. Anal. At. Spectrom., 23(11): 1550-1554 (2008)

Nelson, B. C., Pfeiffer, C., Zhang, M., Duewer, D. L., Sharpless, K. E., and Lippa, K. A., “Commutability of NIST SRM 1955 Homocysteine and Folate in Frozen Human Serum with Selected Total Homocysteine Immunoassays and Enzymatic Assays,” Clin. Chim. Acta, 395(1-2):99-105 (2008)

Oatis, J. E., Brunsfeld, P., Rushing, J. W., Moeller, P. D., Bearden, D., Gallien, T. N., and Cooper, G. W., “Isolation, Purification, and Full NMR Assignments of Cyclopamine from Veratrum californicum,” Chem. Cent. J, 2:12 (2008)

Paul, R. L. and Cao, R., “Characterization of Materials for a Hydrogen-Based Economy by Cold Neutron Prompt Gamma-Ray Activation Analysis,” Mater. Res. Soc. Symp. Proc., 1098E (2008)

Paul, R. L., Lindstrom, R. M., Brocker, C., and Mackey, E. A., “Design of A New Instrument for Cold Neutron Prompt Gamma-Ray Activation Analysis at NIST,” J. Radioanal. Nucl. Chem., 278(3):697-701 (2008)

Paul, R. L., “Determination of Sulfur in Steels by Radiochemical Neutron Activation Analysis with Liquid Scintillation Counting,” J. Radioanal. Nucl. Chem., 276(1): 243-249 (2008).

Peck, A. M., Pugh, R. S., Moors, A., Ellisor, M. B., Porter, B. J., Becker, P. R., and Kucklick, J. R., “Hexabromocyclododecane in White-Sided Dolphins: Temporal Trend and Stereoisomer Distribution in Tissues,” Environ. Sci. Technol., 42(7):2650-2655 (2008)

Peden-Adams, M. M., Keller, J. M., EuDaly, J. G., Berger, J., Gilkeson, G. S., and Keil, D. E., “Suppression of Humoral Immunity in Mice Following Exposure to Perfluorooctane Sulfonate (PFOS),” Toxicol. Sci., 104(1):144-154 (2008)

Phinney, K. W., “Development of a Standard Reference Material for Vitamin D in Serum,” Am. J. Clin. Nutr. 88(2):511S-512S, Suppl. S (2008)

Pikuleva, I., Mast, N., Liao, W. L., and Turko, I., “Studies of Membrane Topology of Mitochondrial Cholesterol Hydroxylases CYPs 27A1 and 11A1,” Lipids, 43(12):1127-1132 (2008)

Point, D., Ignacio Carcia Alonso, J., Davis, W. C., Christopher, S. J., Guichard, A., Donard, O. F. X., Becker, P. R., Turk, G. C., and Wise, S. A., “Consideration and Influence of Complexed Forms of Mercury Species on the Reactivity Patterns Determined by Speciated Isotope Dilution Model Approaches: A Case for Natural Biological Reference Materials,” J. Anal. At. Spec., 23(3):385-396 (2008)

Point, D., Day, R. D., Sonke, J. E., Vander Pol, S. S., Roseneau, D. G., Donard, O. F. X., Simac, K., Moors, A. J., Pugh, R. S., and Becker, P. R., “Mercury Isotopes Fractionation in the Alaskan Marine Environment along an Arctic/Subarctic Transect,” Geochim. Cosmochim. Acta., 72(12):A755-A755, Suppl. 1. (2008)

Pugh, R. S., Becker, P. R., Porter, B. J., Ellisor, M. B., Moors, A. J., and Wise, S. A., “Design and Applications of the National Institute of Standards and Technology's (NIST’s) Environmental Specimen Banking Programs,” Cell. Preserv. Technol., 6(1):59-72 (2008)

Rabb, S. A., Winchester, M. R., and Yu, L. L., “Accurate Determinations of Ge Atom Fractions in SiGe Semiconductor Chips Using High Performance ICP-OES,” J. Anal. At. Spectrom., 23(4):550-554 (2008)

Rabb, S. A., and Olesik, J. W., “Assessment of High Precision, High Accuracy Inductively Coupled Plasma-Optical Emission Spectroscopy to Obtain Concentration Uncertainties Less Than 0.2% with Variable Matrix Concentrations,” Spectrochim. Acta Part B At. Spectrosc., 63(2):244-256 (2008)

Rhoderick, G. C., “NIST Gas Standards Containing Volatile Organic Compounds in Support of Ambient Air Pollution Measurements,” in: Air Pollution XVI, Brebbia, C.A. and Longhurst, J.W.S., (eds.), WIT Press, Southampton, UK, 357-367 (2008).

Rhoderick, G. C., “Differences between Propane in Nitrogen Versus Air Matrix Analyzed Using Gas Chromatography with Flame-Ionization Detection,” J. Chromatogr A, 1187(1-2):226-231 (2008)

Rimmer, C. A., Lippa, K., and Sander, L. C., “Shape Selectivity in Reversed-Phase Liquid Chromatography,” LC GC, 26(10):984-998 (2008)

Rimmer, C. A., Sander, L. C., Sharpless, K. E., and Wise, S.A., “Analytical Challenges in the Certification of Botanical Dietary Supplement Standard Reference Materials,” Planta Med., 74(3):S22 (2008)

Roseland, J. M., Holden, J. M., Andrews, K. W., Zhao, C., Schweitzer, A., Harnly, J., Wolf, W. R., Perry, C. R., Dwyer, J. T., Picciano, M. F., Betz, J. M., Saldanha, L. G., Yetley, E. A., Fisher, K. D., and Sharpless, K. E., “Dietary Supplement Ingredient Database (DSID): Preliminary USDA Studies on the Composition of Adult Multivitamin/Mineral Supplements,” J. Food Comp. Anal., 21:S69-S77, Suppl. S. (2008)

Sander, L. C., Putzbach, K., Nelson, B. C., Rimmer, C. A., Bedner, M., Brown Thomas, J., Porter, B. J., Wood, L. J., Schantz, M. M., Sharpless, K. E., Wise, S. A., Yen, J. H., Siitonen, P. H., NguyenPho, A., Roman, M. C., and Betz, J. M., “Certification of Standard Reference Materials Containing Bitter Orange,” Anal. Bioanal. Chem., 391(6):2023-2034 (2008)

Santana, J., Sharpless, K. E., and Nelson, B. C., “Determination of Para-Synephrine and Meta-Synephrine Positional Isomers in Bitter Orange-Containing Dietary Supplements by LC/UV and LC/MS/MS,” Food Chem., 109(3): 675-682 (2008)

Satterfield, M. B., Lippa, K., Lu, Z. Q., and Salit, M. L., “Microarray Scanner Performance over a Five-Week Period as Measured with Cy5 and Cy3 Serial Dilution Slides,” J. Res. Natl. Inst. Stand. Technol., 113(3):157-174 (2008)

Saupe, S. G., and Sharpless, K. E., “Solution to ‘Doctrine of Signatures’ Challenge,” Anal. Bioanal. Chem., 390(1): 79-83 (2008)

Schantz, M. M., Parris, R. M., and Wise, S. A., “NIST Intercomparison Exercise Program for Organic Contaminants in the Marine Environment: Description and Results of 2007 Organic Intercomparison Exercises,” NISTIR 7501, National Institute of Standards and Technology, Gaithersburg, MD (2008).

Schantz, M. M., Bedner, M., Murphy, K. E., Porter, B. J., Putzbach, K., Rimmer, C. A., Sander, L. C., Sharpless, K. E., Thomas, J. B., Wise, S. A., Wood, L. J., Yen, J. H., Yarita, T., NguyenPho, A., Sorenson, W. R., and Betz, J. M., “Development of Saw Palmetto (Serenoa repens) Fruit and Extract Standard Reference Materials,” Anal. Bioanal. Chem., 392(3):427-438 (2008)

Sharpless, K. E. and Duewer, D. L., “Certified and Ready,” World of Food Ingredients, June Issue:38-40 (2008).

Sharpless, K. E. and Duewer, D. L., “Standard Reference Materials for Analysis of Dietary Supplements,” J. AOAC Int., 91(6):1298-1302 (2008)

Stapleton, H. M. and Dodder, N. G., “Photodegradation of Decabromodiphenyl Ether in House Dust by Natural Sunlight,” Environ. Tox. Chem., 27(2):306-312 (2008)

Stefaniak, A. B., Turk, G. C., Dickerson, R. M., and Hoover, M. D., “Size-Selective Poorly Soluble Particulate Reference Materials for Evaluation of Quantitative Analytical Methods,” Anal. Bioanal. Chem., 391(6): 2071-2077 (2008)

Swarthout, R. F., Kucklick, J. R., and Davis, W. C., “The Determination of Polybrominated Diphenyl Ether Congeners by Gas Chromatography Inductively Coupled Plasma Mass Spectrometry,” J. Anal. At. Spectrom., 23(12):1575-1580 (2008)

Tewari, Y. B., Vanderah, D. H., Schantz, M. M., Goldberg, R. N., Rozzell, J. D., Liebman, J. F., Hui, R. W-M., and Parniani, A. R., “A Themodynamic Study of Ketoreductase-Catalyzed Reactions 5. Reduction of Substituted Ketones in n-Hexane,” J. Chem. Thermodynamics, 40(4):661-670 (2008)

Tomlin, B. E., Zeisler, R. L., and Lindstrom, R. M., “g-g Coincidence Spectrometer for INAA,” Nucl. Instrum. Methods Phys. Res., Sect. A, 589(2):243-249 (2008)

Turner, S., Sieber, J. R., Vetter, T. W., Zeisler, R., Marlow, A. F., Moreno-Ramirez, M. G., Davis, M. E., Kennedy, G. J., Borghard, W. G., Yang, S., Navrotsky, A., Toby, B. H., Kelly, J. F., Fletcher, R. A., Windsor, E. S., Verkouteren, J. R., and Leigh, S. D., “Characterization of Chemical Properties, Unit Cell Parameters and Particle Size Distribution of Three Zeolite Reference Materials: RM 8850-Zeolite Y, RM 8851-Zeolite A and RM 8852-Ammonium ZSM-5 Zeolite,” Microporous Mesoporous Mater., 107(3):252-267 (2008)

Vallone, P. M., Kline, M. C., Duewer, D. L., Decker, A. E., Redman, J. W., Travis, J. C., Smith M.V., and Butler, J. M., "Development and Usage of a NIST Standard Reference Materials for Real-Time PCR quantitation of Human DNA," Forensic Science International: Genetics Supplement Series, 1(1):80-82 (2008).

Viallon, J., Moussay, P., Wielgosz, R., Norris, J. and Guenther, F., “Final Report of the On-Going Key Comparison BIPM.QM-K1: Ozone at Ambient Level, Comparison with NIST, 2007,” Metrologia, 45 Tech. Suppl. 08008 (2008)

Wessel, R. M., van der Veen, A. M. H., Ziel, P.R., Steele, P., Langenfelds, R., van der Schoot, M., Smeulders, D., Besley, L., da Cunha, V. S., Zhou, Z., Qiao, H., Heine, H. J., Martin, B., Macé, T., Gupta, P. K., di Meane, E. A., Sega, M., Rolle, F., Maruyama, M., Kato, K., Matsumoto, N., Kim, J. S., Moon, D. M., Lee, J. B., Murillo, F. R., Nambo, C. R., Serrano Caballero, V.M., de Jesús Avila Salas, M., Pérez Castorene, A., Konopelko, L. A., Kustikov, Y. A., Kolobova, A. V., Pankratov, V. V., Efremova, O. V., Musil, S., Chromek, F., Valkova, M., Milton, M. J. T., Varga, G., Guenther, F., Miller, W. R., Botha, A., Tshilongo, J., Mokgoro, I. S., and Leshabane, N., “International Comparison CCQM-K52: Carbon Dioxide in Synthetic Air,” Metrologia, 45, Tech. Suppl., 08011 (2008)

Whitney, S. M., Downing, R. G., Biegalski, S., and O’Kelly, D. S., “Advancement of Light-Element Neutron Depth Profiling at the University of Texas,” J. Radioanal. Nucl. Chem., 276(1):257-261 (2008)

Wielgosz, R. I., Esler, M., Viallon, J., Moussay, P., Oh, S. H., Kim, B. M., Botha, A., Tshilongo, J., Mokgoro, I. S., Maruyama, M., Mace, T., Sutour, C., Stovcík, V., Valková, M., Musil, S., Pérez Castorena, A., Serrano Caballero, V., Rangel Murillo, F., Konopelko, L. A., Kustikov, Y. A., Pankratov, V.,V., Gromova, E. V., Thorn, W. J., Guenther, F. R., Smeulders, D., Baptista, G., Dias, F., Wessel, R. M., Nieuwenkamp, G., van der Veen, A. M. H., “Final Report on CCQM-P73: International Comparison of Nitrogen Monoxide in Nitrogen Gas Standards (30/70) µmol/mol,” Metrologia, 45, Tech. Suppl., 08002 (2008)

Zeisler, R., James, W. D., Mackey, E. A., Spatz, R. O., and Greenberg, R. R., “NAA Characterization of the New Bovine Liver SRM,” J. Radioanal. Nucl. Chem., 278(3)783-787 (2008)

Zhao, L., Robinson, L., Mackey, E. A., Paul, R. L., and Greenberg, R. R., “Determination of Carbon, Nitrogen, and Phosphorus in Cattail Using Thermal Neutron Prompt Gamma Activation Analysis,” J. Radioanal. Nucl. Chem., 277(1):275-280 (2008)