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Chemistry Laboratory

Manager: Terry Arnold (terry.arnold@fhwa.dot.gov)

Overview
The purpose of the Chemistry Laboratory is to conduct fundamental studies of highway materials aimed at understanding failure mechanisms and superior performance, advancing state-of-the-art characterization tools, and testing and developing new materials.

The technology and data generated in these laboratories, as well as the expertise of the staff, are being used by State transportation agencies and industry to enhance the durability of highway materials and to reduce operating costs. Individual laboratories are discussed below.

The Chemistry Laboratory conducts the synthesis and characterization of highway materials using chemical methods. The laboratory is also capable of evaluating the susceptibility of materials to moisture damage and the beneficial and deleterious effects of deicing chemicals.

The Analytical/Spectroscopy Laboratory provides short-term analyses of materials via identification and semi-quantitative analysis of chemical functional groups, inorganic elemental analyses, separation and quantification, and thermal characterization.

The Chemistry-Analytical/ Spectroscopy Laboratory consists of equipment for characterizing coatings and paving materials, preparing modified asphalt binders, and researching damage induced by moisture and deicing chemicals. Included is thermal analysis (TA) equipment, Nicolet Infrared Spectrometers, a Waters High-Pressure Liquid Chromatograph, a Perkin Elmer Atomic Absorption Spectrometer, high- and low-shear Silverson blenders, and specialized equipment for evaluating moisture susceptibility of asphalt binders.

The Materials Characterization Laboratory enables researchers to see morphological differences, as well as identify mineralogical and chemical compositions of minerals, cementitious materials, metals, coatings, and other highway materials.

The Materials Characterization Laboratory contains equipment for imaging and analyzing (composition mapping) materials. This laboratory is equipped with an Amary 1810 Scanning Electron Microscope (SEM) fitted with an energy-dispersive x-ray spectrometer (EDS) and a Nicolet Optical Microscope.
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More Information.

Laboratory Procedure for the Determination of Lime in Hot Mix Asphalt

Test Method for Detecting the Presence of Phosphoric Acid in Asphalt

Related Research.
TFHRC Materials Technology Research

Pavements Research

Asphalt Pavement

TFHRC Structures Research

Recycled Materials

Publications.
Public Roads Magazine Articles

New Lime Test for Hot Mix Asphalt Unveiled
(March/April 2007)
by Terry S. Arnold, Jenny Rozario, and Jack Youtcheff
FHWA researchers have devised a test to measure lime in asphalt, promising greater pavement longevity and lower costs to all concerned.

A Revolution in Winter Maintenance
(Winter 1996)
by Brian Chollar
Where in the past, states focused their energies and resources on deicing wintry roads, new technologies stress preventive anti-icing measures.

New Technologies Improve Cost-Effectiveness of Calcium Magnesium Acetate (CMA)
(November/December 1999)
by W.C. Ormsby

 

 

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