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(08-23-96) Hazardous Waste Combustors; Revised Standards; Proposed Rule: Federal Register: EPA

 [Federal Register: August 23, 1996 (Volume 61, Number 165)]
[Proposed Rules]               
[Page 43501-43515]
>From the Federal Register Online via GPO Access [wais.access.gpo.gov]

ENVIRONMENTAL PROTECTION AGENCY
40 CFR Parts 60, 63, 260, 261, 264, 265, 266, 270 and 271

[FRL-5558-5]
RIN 2050-AF01

Hazardous Waste Combustors; Revised Standards; Proposed Rule-- Notice of Data Availability and Request for Comments

AGENCY: Environmental Protection Agency (EPA).

ACTION: Notice of data availability and request for comments.


SUMMARY: This document is a notice of availability and invitation for comment on the following information pertaining to the proposed revised standards for hazardous waste combustors (61 FR 17358 (April 19, 1996)): Reports from an independent peer review of technical aspects of the rule; additional analyses of various fuel oils to be used to establish a specification to exclude comparable fuels; and information on a synthesis gas process and product gas specifications that was inadvertently not included in the docket. Readers should note that only comments about new information discussed in this document will be considered during the comment period. Issues related to the April 19, 1996 proposed rule that are not directly affected by the documents or data referenced in this Notice of Data Availability are not open for further comment.

DATES: Written comments on the peer review reports, the new comparable fuels analyses, and the synthesis gas process and product information must be submitted by September 23, 1996.

ADDRESSES: Commenters must send an original and two copies of their comments referencing Docket Number F-96-RCSP-FFFFF to: RCRA Docket Information Center, Office of Solid Waste (5305G), U.S. Environmental Protection Agency Headquarters (EPA, HQ), 401 M Street, S.W., Washington, D.C. 20460. Comments may also be submitted electronically through the Internet to: rcra-docket@epamail.epa.gov. Comments in electronic format should also be identified by the docket number F-96- RCSP-FFFFF. All electronic comments must be submitted as an ASCII file avoiding the use of special characters and any form of encryption. Commenters should not submit electronically any confidential business information (CBI). An original and two copies of the CBI must be submitted under separate cover to: RCRA CBI Document Control Officer, OSW (5305W), 401 M Street, SW, Washington D.C. 20460. For other information regarding submitting comments electronically, viewing the comments received, and supporting information, please refer to the proposed rule (61 FR 17358 (April 19, 1996)). The RCRA Information Center is located at Crystal Gateway One, 1235 Jefferson Davis Highway, First Floor, Arlington, Virginia and is open for public inspection and copying of supporting information for RCRA rules from 9:00

[[Page 43502]]

am to 4:00 pm Monday through Friday, except for Federal holidays. The public must make an appointment to view docket materials by calling (703) 603-9230. The public may copy a maximum of 100 pages from any regulatory document at no cost. Additional copies cost $0.15 per page.

FOR FURTHER INFORMATION CONTACT: For general information, call the RCRA Hotline at 1-800-424-9346 or TDD 1-800-553-7672 (hearing impaired) including directions on how to access electronically some of the documents and data referred to in this notice via EPA's Cleanup Information Bulletin Board System (CLU-IN). The CLU-IN modem access phone number is 301-589-8366 or Telnet to clu-in.epa.gov for Internet access. Callers within the Washington Metropolitan Area must dial 703- 412-9810 or TDD 703-412-3323 (hearing impaired). The RCRA Hotline is open Monday-Friday, 9:00 a.m. to 6:00 p.m., Eastern Standard Time. For other information on this notice, contact Shiva Garg (5302W), Office of Solid Waste, 401 M Street, S.W., Washington, DC 20460, phone (703) 308- 8459, e-mail: garg.shiva@epamail.epa.gov.

SUPPLEMENTARY INFORMATION: On April 19, 1996, EPA proposed revised standards for hazardous waste combustors (i.e., incinerators and cement and lightweight aggregate kilns that burn hazardous waste). See 61 FR 17358. The Agency originally established a 60-day comment period, but later extended it to 120 days (61 FR 27038 (May 30, 1996)). The last date for receipt of comments on the Federal Register notice of April 19, 1996 continues to remain August 19, 1996. The Agency is today providing notice and opportunity to comment on the following additional information pertaining to the proposed rule: (1) Reports from an independent peer review of technical aspects of the rule; (2) additional analyses of various fuel oils to be used to establish a specification to exclude comparable fuels; and (3) information on a synthesis gas process and product gas specifications that was inadvertently not included in the docket.

Peer Review Reports

As part of the rule development process, the Agency initiated a peer review of the proposed rule, preamble and relevant supporting background documents in three subject areas of the rule: engineering, risk assessment and economic analysis. The review panel members were tasked with conducting a comprehensive and critical review of the proposed rule in their designated subject areas, addressing a set of questions pertaining to the technical basis of the approaches adopted by the Agency, and providing comments and/or recommendations where warranted. Each subject area panel prepared a summary report highlighting the key points of discussion, including the consensus reports or the dissenting opinions. Copies of the peer review panel report of each subject area and individual review comments of each panel member are available in the docket.

Comparable Fuel Specification

As part of the proposed comparable fuel specification, EPA used a benchmark approach to develop a series of technical specifications that would allow hazardous waste similar in composition to a commercially available fossil fuel to be excluded under RCRA when burned. One of these specifications included the Agency's proposal to limit the Appendix VIII, Part 261, constituents in comparable fuels 1 to those found in the benchmark fossil fuel. As discussed in the preamble of the proposal (61 FR 17461), EPA was unable to analyze for some compounds on the Appendix VIII list because either an analytical method was not available or could not be identified in time for initial analysis. Those compounds were not listed in the proposed specifications published on April 19, 1996.


\1\ The specification would also include two metals that are identified in Clean Air Act section 112(b) as hazardous air pollutants: cobalt and manganese. See 61 FR 17460.


EPA has subsequently been able to identify methods for analyzing some additional Appendix VIII compounds and is presenting a proposed specification level or detection limit for these compounds. These compounds are listed in today's notice and also can be found, along with the analytical methods, in the Draft Technical Support Document for HWC MACT Standards, Addendum to Volume VI: Development of Comparable Fuels Specifications, August 1996. EPA invites comment on today's new individual specifications, as well as the composite specifications, and the analytical methods used in EPA's new analysis. In addition, we want to clarify the rationale for proposing comparable fuel specification limits for total halogens and total nitrogen. Although neither total halogens nor total nitrogen are listed on Appendix VIII, Part 261 (or proposed for Appendix X), we believe that they should be limited to ensure that halogenated and nitrated products of incomplete combustion (PICs) from burning excluded waste would not be emitted at higher levels than from burning benchmark fossil fuel. Halogenated and nitrated organic compounds can pose a particular hazard to human health and the environment.

Synthesis Gas Comparable Fuel Exclusion

In discussing the exclusion of synthesis gas (syngas) fuel in the proposed rule, EPA referenced a Molten Metals Technology (MMT) letter that presented data on the MMT syngas process, including relevant specifications. See preamble discussion at 61 FR 17465. In placing the MMT information in the docket, an attachment to the letter containing the data was inadvertently not placed in the docket until late in the comment period. EPA has since received a request to extend the comment period pertaining only to the syngas exclusion to allow adequate time to review this attachment and provide comment on the syngas exclusion. In response to this request, EPA is granting 30 days from the publication date of this notice to comment on the proposed syngas fuel exclusion.

Appendix--Comparable Fuel Constituent and Physical Specifications

Note 1: All numbers in the tables of this appendix are expressed to two significant figures.

Table 1.--Detection and Detection Limit Values for a Possible Gasoline

                              Specification                             

                                                               Maximum  
                                      Concentration limit     detection 
Chemical name (mg/kg at 10,000 Btu/ limit (mg/
                                              lb)                kg)    

1,1,1-Trichloroethane.............. Non-detect........... 34

[[Page 43503]]

                                                                        
1,1,2-Trichloro-1,2,2- Non-detect........... 30
 trifluoroethane.                                                       
1,1-Dichloro-1-propene............. Non-detect........... 30 1,1-Dichloroethane................. Non-detect........... 34 1,2,3,4,6,7,8-Heptachlorodibenzo-p- Non-detect........... 8.8
 dioxin.                                                                
1,2,3,4,6,7,8-Heptachlorodibenzo-p- Non-detect........... 8.8
 furan.                                                                 
1,2,3,4-Tetrachlorobenzene......... Non-detect........... 14 1,2,3,5-Tetrachlorobenzene......... Non-detect........... 14 1,2,3,6,7,8-Hexachlorodibenzo-p- Non-detect........... 8.8
 dioxin.                                                                
1,2,3,6,7,8-Hexachlorodibenzo-p- Non-detect........... 8.8
 furan.                                                                 
1,2,3,7,8-Pentachlorodibenzo-p- Non-detect........... 8.8
 dioxin.                                                                
1,2,3,7,8-Pentachlorodibenzo-p- Non-detect........... 8.8
 furan.                                                                 
1,2,3-Trichlorobenzene............. Non-detect........... 14 1,2-Dichloroethane................. Non-detect........... 34 1,2-Dichloropropane................ Non-detect........... 34 1,3-Dichloro-2-propanol............ Non-detect........... 30 1,3-Dichloropropane................ Non-detect........... 30 1,3-Propane sultone................ Non-detect........... 14 1-Chloronaphthalene................ Non-detect........... 14 2,2-Dichloropropane................ Non-detect........... 30 2,3,4,5-Tetrachlorophenol.......... Non-detect........... 14 2,3,4-Trichlorophenol.............. Non-detect........... 14 2,3,5-Trichlorophenol.............. Non-detect........... 14 2,3,6-Trichlorophenol.............. Non-detect........... 14 2,3,7,8-Tetrachlorodibenzo-p-dioxin Non-detect........... 3.5 2,3,7,8-Tetrachlorodibenzo-p-furan. Non-detect........... 3.5 2,3-Dichloro-1-propene............. Non-detect........... 30 2,3-Dichlorophenol................. Non-detect........... 14 2,4-D.............................. Non-detect........... 7.0 2,5-Dichlorophenol................. Non-detect........... 14 2-Fluoroacetamide.................. Non-detect........... 14 2-Methylnaphthalene................ 1200................. ............ 2-Nitropropane..................... Non-detect........... 30 3,3'-Dimethoxybenzidine............ Non-detect........... 14 3,4-Dichlorophenol................. Non-detect........... 14 3,5-Dichlorophenol................. Non-detect........... 14 3-/4-Chlorophenol.................. Non-detect........... 14 3-Nitroaniline..................... Non-detect........... 670 4,4'-methylene-bis(2-chloroaniline) Non-detect........... 14 4-Aminopyrridine................... Non-detect........... 14 4-Chlorophenyl phenyl ether........ Non-detect........... 670 6-Propyl-2-thiouracil.............. Non-detect........... 14 Acenaphthene....................... Non-detect........... 670 Acetone cyanohydrin................ Non-detect........... 14 Allyl alcohol...................... Non-detect........... 30 Ammonium vanadate.................. Non-detect........... 32 Anthracene......................... Non-detect........... 670 Arochlor-1016...................... Non-detect........... 1.4 Arochlor-1221...................... Non-detect........... 1.4 Arochlor-1232...................... Non-detect........... 1.4 Arochlor-1242...................... Non-detect........... 1.4 Arochlor-1248...................... Non-detect........... 1.4 Arochlor-1254...................... Non-detect........... 1.4 Arochlor-1260...................... Non-detect........... 1.4 Arsenic acid....................... Non-detect........... 0.27 Arsenic pentoxide.................. Non-detect........... 0.22 Arsenic trioxide................... Non-detect........... 0.19 Barium Cyanide..................... Non-detect........... 3.7 Benzal chloride.................... Non-detect........... 14 Benzenethiol....................... Non-detect........... 30 Benzyl chloride.................... Non-detect........... 14 Bis(2-chloroethoxy)methane......... Non-detect........... 670 Bis(2-chloroethyl)ether............ Non-detect........... 670 Bis(2-ethylhexyl)phthalate......... Non-detect........... 670 Bromide............................ Non-detect........... 5.0 Bromodichloromethane............... Non-detect........... 34 Calcium Cyanide.................... Non-detect........... 1.8 Calcium chromate................... Non-detect........... 4.2 Chlordane.......................... Non-detect........... 14 Chloride........................... 6.2.................. ............

[[Page 43504]]

                                                                        
Chloroethane....................... Non-detect........... 34 Copper Cyanide..................... Non-detect........... 1.7 Cyanide............................ Non-detect........... 1.0 Cyanogen Bromide................... Non-detect........... 6.6 Cyanogen Chloride.................. Non-detect........... 100 Di-selenium-tetra-sulfide.......... Non-detect........... 830 Dibenzofuran....................... Non-detect........... 670 Dibromochloromethane............... Non-detect........... 34 Endosulfan I....................... Non-detect........... 1.4 Endosulfan II...................... Non-detect........... 1.4 Endothal........................... Non-detect........... 14 Endrin............................. Non-detect........... 1.4 Endrin aldehyde.................... Non-detect........... 1.4 Endrin ketone...................... Non-detect........... 1.4 Epichlorohydrin.................... Non-detect........... 30 Ethyl carbamate.................... Non-detect........... 14 Ethylene glycol monoethyl ether.... Non-detect........... 14 Ethylenethiourea (2- Non-detect........... 14
 Imidazolidinethione).                                                  
Fluoride........................... Non-detect........... 3.0 Heptachlor......................... Non-detect........... 1.4 Heptachlor epoxide................. Non-detect........... 2.8 Lead acetate....................... Non-detect........... 13 Lead phosphate..................... Non-detect........... 9.2 MNNG (N-Methyl-N-nitroso-N'- Non-detect........... 14
 nitroguanidine).                                                       
Methomyl........................... Non-detect........... 7.0 N-Nitrosodiphenylamine............. Non-detect........... 670 Nickel Cyanide..................... Non-detect........... 3.5 Nickel carbonyl.................... Non-detect........... 8.2 Nicotine........................... Non-detect........... 14 Octachlorodibenzodioxin............ Non-detect........... 18 Octachlorodibenzofuran............. Non-detect........... 18 Osmium tetraoxide.................. Non-detect........... 41 Phenanthrene....................... Non-detect........... 670 Phenylthiourea..................... Non-detect........... 7.0 Potassium Cyanide.................. Non-detect........... 2.5 Potassium Silver Cyanide........... Non-detect........... 2.9 Propargyl alcohol.................. Non-detect........... 30 Pyrene............................. Non-detect........... 670 Selenium dioxide................... Non-detect........... 0.20 Selenium sulfide................... Non-detect........... 0.31 Silver Cyanide..................... Non-detect........... 2.6 Silvex............................. Non-detect........... 7.0 Strychnine......................... Non-detect........... 14 Tetra-selenium-tetra-sulfide....... Non-detect........... 1600 Tetraethyl lead.................... Non-detect........... 11 Thallium acetate................... Non-detect........... 18 Thallium carbonate................. Non-detect........... 16 Thallium chloride.................. Non-detect........... 17 Thallium nitrate................... Non-detect........... 18 Thallium oxide..................... Non-detect........... 15 Thallium sulfate................... Non-detect........... 17 Thioacetamide...................... Non-detect........... 7.0 Thiofanox.......................... Non-detect........... 14 Thiourea........................... Non-detect........... 7.0 Toluene-2,4-diamine................ Non-detect........... 7.0 Toluene-2,6-diamine................ Non-detect........... 7.0 Vanadium pentoxide................. Non-detect........... 18 Zinc Cyanide....................... Non-detect........... 2.3 Zinc phosphide..................... Non-detect........... 0.37 alpha-BHC.......................... Non-detect........... 1.4 beta-BHC........................... Non-detect........... 1.4 delta-BHC.......................... Non-detect........... 1.4 gamma-BHC (Lindane)................ Non-detect........... 1.4 m-Dinitrobenzene................... Non-detect........... 670 p-Toluidine........................ Non-detect........... 14 trans-1,3-Dichloropropene.......... Non-detect........... 34

[[Page 43505]]

Table 2.--Detection and Detection Limit Values for a Possible Number 2

                         Fuel Oil Specification                         

                                                               Maximum  
                                      Concentration limit     detection 
Chemical name (mg/kg at 10,000 Btu/ limit (mg/
                                              lb)                kg)    

1,1,1-Trichloroethane.............. Non-detect........... 34 1,1,2-Trichloro-1,2,2- Non-detect........... 30
 trifluoroethane.                                                       
1,1-Dichloro-1-propene............. Non-detect........... 30 1,1-Dichloroethane................. Non-detect........... 34 1,2,3,4,6,7,8-Heptachlorodibenzo-p- Non-detect........... 75
 dioxin.                                                                
1,2,3,4,6,7,8-Heptachlorodibenzo-p- Non-detect........... 75
 furan.                                                                 
1,2,3,4-Tetrachlorobenzene......... Non-detect........... 100 1,2,3,5-Tetrachlorobenzene......... Non-detect........... 100 1,2,3,6,7,8-Hexachlorodibenzo-p- Non-detect........... 75
 dioxin.                                                                
1,2,3,6,7,8-Hexachlorodibenzo-p- Non-detect........... 75
 furan.                                                                 
1,2,3,7,8-Pentachlorodibenzo-p- Non-detect........... 75
 dioxin.                                                                
1,2,3,7,8-Pentachlorodibenzo-p- Non-detect........... 75
 furan.                                                                 
1,2,3-Trichlorobenzene............. Non-detect........... 100 1,2-Dichloroethane................. Non-detect........... 34 1,2-Dichloropropane................ Non-detect........... 34 1,3-Dichloro-2-propanol............ Non-detect........... 30 1,3-Dichloropropane................ Non-detect........... 30 1,3-Propane sultone................ Non-detect........... 100 1-Chloronaphthalene................ Non-detect........... 100 2,2-Dichloropropane................ Non-detect........... 30 2,3,4,5-Tetrachlorophenol.......... Non-detect........... 100 2,3,4-Trichlorophenol.............. Non-detect........... 100 2,3,5-Trichlorophenol.............. Non-detect........... 100 2,3,6-Trichlorophenol.............. Non-detect........... 100 2,3,7,8-Tetrachlorodibenzo-p-dioxin Non-detect........... 30 2,3,7,8-Tetrachlorodibenzo-p-furan. Non-detect........... 30 2,3-Dichloro-1-propene............. Non-detect........... 30 2,3-Dichlorophenol................. Non-detect........... 100 2,4-D.............................. Non-detect........... 6.0 2,5-Dichlorophenol................. Non-detect........... 100 2-Fluoroacetamide.................. Non-detect........... 100 2-Methylnaphthalene................ 3400................. ............ 2-Nitropropane..................... Non-detect........... 30 3,3'-Dimethoxybenzidine............ Non-detect........... 100 3,4-Dichlorophenol................. Non-detect........... 100 3,5-Dichlorophenol................. Non-detect........... 100 3-/4-Chlorophenol.................. Non-detect........... 100 3-Nitroaniline..................... Non-detect........... 1200 4,4'-methylene-bis(2-chloroaniline) Non-detect........... 100 4-Aminopyrridine................... Non-detect........... 100 4-Chlorophenyl phenyl ether........ Non-detect........... 1200 6-Propyl-2-thiouracil.............. Non-detect........... 100 Acenaphthene....................... Non-detect........... 1200 Acetone cyanohydrin................ Non-detect........... 100 Allyl alcohol...................... Non-detect........... 30 Ammonium vanadate.................. Non-detect........... 28 Anthracene......................... Non-detect........... 1200 Arochlor-1016...................... Non-detect........... 1.2 Arochlor-1221...................... Non-detect........... 1.2 Arochlor-1232...................... Non-detect........... 1.2 Arochlor-1242...................... Non-detect........... 1.2 Arochlor-1248...................... Non-detect........... 1.2 Arochlor-1254...................... Non-detect........... 1.2 Arochlor-1260...................... Non-detect........... 1.2 Arsenic acid....................... Non-detect........... 0.23 Arsenic pentoxide.................. Non-detect........... 0.18 Arsenic trioxide................... Non-detect........... 0.16 Barium Cyanide..................... Non-detect........... 3.7 Benzal chloride.................... Non-detect........... 100 Benzenethiol....................... Non-detect........... 30 Benzyl chloride.................... Non-detect........... 100 Bis(2-chloroethoxy)methane......... Non-detect........... 1200 Bis(2-chloroethyl)ether............ Non-detect........... 1200 Bis(2-ethylhexyl)phthalate......... Non-detect........... 1200 Bromide............................ Non-detect........... 5.0 Bromodichloromethane............... Non-detect........... 34 Calcium Cyanide.................... Non-detect........... 1.8 Calcium chromate................... Non-detect........... 3.6 Chlordane.......................... Non-detect........... 12

[[Page 43506]]

                                                                        
Chloride........................... Non-detect........... 5.0 Chloroethane....................... Non-detect........... 34 Copper Cyanide..................... Non-detect........... 1.7 Cyanide............................ Non-detect........... 1.0 Cyanogen Bromide................... Non-detect........... 6.6 Cyanogen Chloride.................. Non-detect........... 8.6 Di-selenium-tetra-sulfide.......... Non-detect........... 370 Dibenzofuran....................... Non-detect........... 1200 Dibromochloromethane............... Non-detect........... 34 Endosulfan I....................... Non-detect........... 1.2 Endosulfan II...................... Non-detect........... 1.2 Endothal........................... Non-detect........... 100 Endrin............................. Non-detect........... 1.2 Endrin aldehyde.................... Non-detect........... 1.2 Endrin ketone...................... Non-detect........... 1.2 Epichlorohydrin.................... Non-detect........... 30 Ethyl carbamate.................... Non-detect........... 100 Ethylene glycol monoethyl ether.... Non-detect........... 100 Ethylenethiourea (2- Non-detect........... 12
 Imidazolidinethione).                                                  
Fluoride........................... Non-detect........... 3.0 Heptachlor......................... Non-detect........... 1.2 Heptachlor epoxide................. Non-detect........... 2.4 Lead acetate....................... Non-detect........... 22 Lead phosphate..................... Non-detect........... 15 MNNG (N-Metyl-N-nitroso-N'- Non-detect........... 12
 nitroguanidine).                                                       
Methomyl........................... Non-detect........... 6.0 N-Nitrosodiphenylamine............. Non-detect........... 1200 Nickel Cyanide..................... Non-detect........... 3.5 Nickel carbonyl.................... Non-detect........... 7.0 Nicotine........................... Non-detect........... 100 Octachlorodibenzodioxin............ Non-detect........... 150 Octachlorodibenzofuran............. Non-detect........... 150 Osmium tetraoxide.................. Non-detect........... 40 Phenanthrene....................... 860.................. ............ Phenylthiourea..................... Non-detect........... 6.0 Potassium Cyanide.................. Non-detect........... 2.5 Potassium Silver Cyanide........... Non-detect........... 2.9 Propargyl alcohol.................. Non-detect........... 30 Pyrene............................. Non-detect........... 1200 Selenium dioxide................... Non-detect........... 0.21 Selenium sulfide................... Non-detect........... 0.34 Silver Cyanide..................... Non-detect........... 2.6 Silvex............................. Non-detect........... 6.0 Strychnine......................... Non-detect........... 100 Tetra-selenium-tetra-sulfide....... Non-detect........... 710 Tetraethyl lead.................... Non-detect........... 18 Thallium acetate................... Non-detect........... 15 Thallium carbonate................. Non-detect........... 14 Thallium chloride.................. Non-detect........... 14 Thallium nitrate................... Non-detect........... 16 Thallium oxide..................... Non-detect........... 12 Thallium sulfate................... Non-detect........... 15 Thioacetamide...................... Non-detect........... 6.0 Thiofanox.......................... Non-detect........... 100 Thiourea........................... Non-detect........... 6.0 Toluene-2,4-diamine................ Non-detect........... 6.0 Toluene-2,6-diamine................ Non-detect........... 6.0 Vanadium pentoxide................. Non-detect........... 18 Zinc Cyanide....................... Non-detect........... 2.3 Zinc phosphide..................... Non-detect........... 0.32 alpha-BHC.......................... Non-detect........... 1.2 beta-BHC........................... Non-detect........... 1.2 delta-BHC.......................... Non-detect........... 1.2 gamma-BHC (Lindane)................ Non-detect........... 1.2 m-Dinitrobenzene................... Non-detect........... 1200 p-Toluidine........................ Non-detect........... 100 trans-1,3-Dichloropropene.......... Non-detect........... 34

[[Page 43507]]

Table 3.--Detection and Detection Limit Values for a Possile Number 4

                         Fuel Oil Specification                         

                                                               Maximum  
                                      Concentration limit     detection 
Chemical name (mg/kg at 10,000 Btu/ limit (mg/
                                              lb)                kg)    

1,1,1-Trichloroethane.............. Non-detect........... 17 1,1,2-Trichloro-1,2,2- Non-detect........... 29
 trifluoroethane.                                                       
1,1-Dichloro-1-propene............. Non-detect........... 29 1,1-Dichloroethane................. Non-detect........... 17 1,2,3,4,6,7,8-Heptachlorodibenzo-p- Non-detect........... 72
 dioxin.                                                                
1,2,3,4,6,7,8-Heptachlorodibenzo-p- Non-detect........... 72
 furan.                                                                 
1,2,3,4-Tetrachlorobenzene......... Non-detect........... 100 1,2,3,5-Tetrachlorobenzene......... Non-detect........... 100 1,2,3,6,7,8-Hexachlorodibenzo-p- Non-detect........... 72
 dioxin.                                                                
1,2,3,6,7,8-Hexachlorodibenzo-p- Non-detect........... 72
 furan.                                                                 
1,2,3,7,8-Pentachlorodibenzo-p- Non-detect........... 72
 dioxin.                                                                
1,2,3,7,8-Pentachlorodibenzo-p- Non-detect........... 72
 furan.                                                                 
1,2,3-Trichlorobenzene............. Non-detect........... 100 1,2-Dichloroethane................. Non-detect........... 17 1,2-Dichloropropane................ Non-detect........... 17 1,3-Dichloro-2-propanol............ Non-detect........... 29 1,3-Dichloropropane................ Non-detect........... 29 1,3-Propane sultone................ Non-detect........... 100 1-Chloronaphthalene................ Non-detect........... 100 2,2-Dichloropropane................ Non-detect........... 29 2,3,4,5-Tetrachlorophenol.......... Non-detect........... 100 2,3,4-Trichlorophenol.............. Non-detect........... 100 2,3,5-Trichlorophenol.............. Non-detect........... 100 2,3,6-Trichlorophenol.............. Non-detect........... 100 2,3,7,8-Tetrachlorodibenzo-p-dioxin Non-detect........... 29 2,3,7,8-Tetrachlorodibenzo-p-furan. Non-detect........... 29 2,3-Dichloro-1-propene............. Non-detect........... 29 2,3-Dichlorophenol................. Non-detect........... 100 2,4-D.............................. Non-detect........... 5.7 2,5-Dichlorophenol................. Non-detect........... 100 2-Fluoroacetamide.................. Non-detect........... 100 2-Methylnaphthalene................ 1000................. - 2-Nitropropane..................... Non-detect........... 29 3,3'-Dimethoxybenzidine............ Non-detect........... 100 3,4-Dichlorophenol................. Non-detect........... 100 3,5-Dichlorophenol................. Non-detect........... 100 3-/4-Chlorophenol.................. Non-detect........... 100 3-Nitroaniline..................... Non-detect........... 200 4,4'-methylene-bis(2-chloroaniline) Non-detect........... 100 4-Aminopyrridine................... Non-detect........... 100 4-Chlorophenyl phenyl ether........ Non-detect........... 200 6-Propyl-2-thiouracil.............. Non-detect........... 100 Acenaphthene....................... Non-detect........... 200 Acetone cyanohydrin................ Non-detect........... 100 Allyl alcohol...................... Non-detect........... 29 Ammonium vanadate.................. Non-detect........... 68 Anthracene......................... Non-detect........... 200 Arochlor-1016...................... Non-detect........... 1.1 Arochlor-1221...................... Non-detect........... 1.1 Arochlor-1232...................... Non-detect........... 1.1 Arochlor-1242...................... Non-detect........... 1.1 Arochlor-1248...................... Non-detect........... 1.1 Arochlor-1254...................... Non-detect........... 1.1 Arochlor-1260...................... Non-detect........... 1.1 Arsenic acid....................... Non-detect........... 0.43 Arsenic pentoxide.................. Non-detect........... 0.35 Arsenic trioxide................... Non-detect........... 0.30 Barium Cyanide..................... Non-detect........... 3.7 Benzal chloride.................... Non-detect........... 100 Benzenethiol....................... Non-detect........... 29 Benzyl chloride.................... Non-detect........... 100 Bis(2-chloroethoxy)methane......... Non-detect........... 200 Bis(2-chloroethyl)ether............ Non-detect........... 200 Bis(2-ethylhexyl)phthalate......... Non-detect........... 200 Bromide............................ Non-detect........... 5.0 Bromodichloromethane............... Non-detect........... 17 Calcium Cyanide.................... Non-detect........... 1.8 Calcium chromate................... Non-detect........... 6.9 Chlordane.......................... Non-detect........... 11

[[Page 43508]]

                                                                        
Chloride........................... Non-detect........... 5.0 Chloroethane....................... Non-detect........... 17 Copper Cyanide..................... Non-detect........... 1.7 Cyanide............................ Non-detect........... 1.0 Cyanogen Bromide................... Non-detect........... 6.6 Cyanogen Chloride.................. Non-detect........... 8.6 Di-selenium-tetra-sulfide.......... Non-detect........... 1300 Dibenzofuran....................... Non-detect........... 200 Dibromochloromethane............... Non-detect........... 17 Endosulfan I....................... Non-detect........... 1.1 Endosulfan II...................... Non-detect........... 1.1 Endothal........................... Non-detect........... 100 Endrin............................. Non-detect........... 1.1 Endrin aldehyde.................... Non-detect........... 1.1 Endrin ketone...................... Non-detect........... 1.1 Epichlorohydrin.................... Non-detect........... 29 Ethyl carbamate.................... Non-detect........... 100 Ethylene glycol monoethyl ether.... Non-detect........... 100 Ethylenethiourea (2- Non-detect........... 110
 Imidazolidinethione).                                                  
Fluoride........................... Non-detect........... 3.0 Heptachlor......................... Non-detect........... 1.1 Heptachlor epoxide................. Non-detect........... 2.3 Lead acetate....................... Non-detect........... 34 Lead phosphate..................... Non-detect........... 24 MNNG (N-Metyl-N-nitroso-N'- Non-detect........... 110
 nitroguanidine).                                                       
Methomyl........................... Non-detect........... 57 N-Nitrosodiphenylamine............. Non-detect........... 200 Nickel Cyanide..................... Non-detect........... 3.5 Nickel carbonyl.................... Non-detect........... 13 Nicotine........................... Non-detect........... 100 Octachlorodibenzodioxin............ Non-detect........... 140 Octachlorodibenzofuran............. Non-detect........... 140 Osmium tetraoxide.................. Non-detect........... 40 Phenanthrene....................... 250.................. - Phenylthiourea..................... Non-detect........... 57 Potassium Cyanide.................. Non-detect........... 2.5 Potassium Silver Cyanide........... Non-detect........... 2.9 Propargyl alcohol.................. Non-detect........... 29 Pyrene............................. Non-detect........... 200 Selenium dioxide................... Non-detect........... 0.35 Selenium sulfide................... Non-detect........... 0.56 Silver Cyanide..................... Non-detect........... 2.6 Silvex............................. Non-detect........... 5.7 Strychnine......................... Non-detect........... 100 Tetra-selenium-tetra-sulfide....... Non-detect........... 2400 Tetraethyl lead.................... Non-detect........... 29 Thallium acetate................... Non-detect........... 30 Thallium carbonate................. Non-detect........... 26 Thallium chloride.................. Non-detect........... 27 Thallium nitrate................... Non-detect........... 30 Thallium oxide..................... Non-detect........... 24 Thallium sulfate................... Non-detect........... 28 Thioacetamide...................... Non-detect........... 57 Thiofanox.......................... Non-detect........... 100 Thiourea........................... Non-detect........... 57 Toluene-2,4-diamine................ Non-detect........... 57 Toluene-2,6-diamine................ Non-detect........... 57 Vanadium pentoxide................. Non-detect........... 18 Zinc Cyanide....................... Non-detect........... 2.3 Zinc phosphide..................... Non-detect........... 0.75 alpha-BHC.......................... Non-detect........... 1.1 beta-BHC........................... Non-detect........... 1.1 delta-BHC.......................... Non-detect........... 1.1 gamma-BHC (Lindane)................ Non-detect........... 1.1 m-Dinitrobenzene................... Non-detect........... 200 p-Toluidine........................ Non-detect........... 100 trans-1,3-Dichloropropene.......... Non-detect........... 17

[[Page 43509]]

Table 4.--Detection and Detection Limit Values for a Possible Number 6

                         Fuel Oil Specification                         

                                                               Maximum  
                                      Concentration limit     detection 
Chemical name (mg/kg at 10,000 Btu/ limit (mg/
                                              lb)                kg)    

1,1,1-Trichloroethane.............. Non-detect........... 21 1,1,2-Trichloro-1,2,2- Non-detect........... 26
 trifluoroethane.                                                       
1,1-Dichloro-1-propene............. Non-detect........... 26 1,1-Dichloroethane................. Non-detect........... 21 1,2,3,4,6,7,8-Heptachlorodibenzo-p- Non-detect........... 64
 dioxin.                                                                
1,2,3,4,6,7,8-Heptachlorodibenzo-p- Non-detect........... 64
 furan.                                                                 
1,2,3,4-Tetrachlorobenzene......... Non-detect........... 100 1,2,3,5-Tetrachlorobenzene......... Non-detect........... 100 1,2,3,6,7,8-Hexachlorodibenzo-p- Non-detect........... 64
 dioxin.                                                                
1,2,3,6,7,8-Hexachlorodibenzo-p- Non-detect........... 64
 furan.                                                                 
1,2,3,7,8-Pentachlorodibenzo-p- Non-detect........... 64
 dioxin.                                                                
1,2,3,7,8-Pentachlorodibenzo-p- Non-detect........... 64
 furan.                                                                 
1,2,3-Trichlorobenzene............. Non-detect........... 100 1,2-Dichloroethane................. Non-detect........... 21 1,2-Dichloropropane................ Non-detect........... 21 1,3-Dichloro-2-propanol............ Non-detect........... 26 1,3-Dichloropropane................ Non-detect........... 26 1,3-Propane sultone................ Non-detect........... 100 1-Chloronaphthalene................ Non-detect........... 100 2,2-Dichloropropane................ Non-detect........... 26 2,3,4,5-Tetrachlorophenol.......... Non-detect........... 100 2,3,4-Trichlorophenol.............. Non-detect........... 100 2,3,5-Trichlorophenol.............. Non-detect........... 100 2,3,6-Trichlorophenol.............. Non-detect........... 100 2,3,7,8-Tetrachlorodibenzo-p-dioxin Non-detect........... 26 2,3,7,8-Tetrachlorodibenzo-p-furan. Non-detect........... 26 2,3-Dichloro-1-propene............. Non-detect........... 26 2,3-Dichlorophenol................. Non-detect........... 100 2,4-D.............................. Non-detect........... 5.1 2,5-Dichlorophenol................. Non-detect........... 100 2-Fluoroacetamide.................. Non-detect........... 100 2-Methylnaphthalene................ 4200................. ............ 2-Nitropropane..................... Non-detect........... 26 3,3'-Dimethoxybenzidine............ Non-detect........... 100 3,4-Dichlorophenol................. Non-detect........... 100 3,5-Dichlorophenol................. Non-detect........... 100 3-/4-Chlorophenol.................. Non-detect........... 100 3-Nitroaniline..................... Non-detect........... 980 4,4'-methylene-bis(2-chloroaniline) Non-detect........... 100 4-Aminopyrridine................... Non-detect........... 100 4-Chlorophenyl phenyl ether........ Non-detect........... 980 6-Propyl-2-thiouracil.............. Non-detect........... 100 Acenaphthene....................... Non-detect........... 980 Acetone cyanohydrin................ Non-detect........... 100 Allyl alcohol...................... Non-detect........... 26 Ammonium vanadate.................. Non-detect........... 590 Anthracene......................... Non-detect........... 980 Arochlor-1016...................... Non-detect........... 1.0 Arochlor-1221...................... Non-detect........... 1.0 Arochlor-1232...................... Non-detect........... 1.0 Arochlor-1242...................... Non-detect........... 1.0 Arochlor-1248...................... Non-detect........... 1.0 Arochlor-1254...................... Non-detect........... 1.0 Arochlor-1260...................... Non-detect........... 1.0 Arsenic acid....................... Non-detect........... 0.39 Arsenic pentoxide.................. Non-detect........... 0.31 Arsenic trioxide................... Non-detect........... 0.27 Barium Cyanide..................... Non-detect........... 3.7 Benzal chloride.................... Non-detect........... 100 Benzenethiol....................... Non-detect........... 26 Benzyl chloride.................... Non-detect........... 100 Bis(2-chloroethoxy)methane......... Non-detect........... 980 Bis(2-chloroethyl)ether............ Non-detect........... 980 Bis(2-ethylhexyl)phthalate......... Non-detect........... 980 Bromide............................ Non-detect........... 5.0 Bromodichloromethane............... Non-detect........... 21 Calcium Cyanide.................... Non-detect........... 1.8 Calcium chromate................... Non-detect........... 6.1 Chlordane.......................... Non-detect........... 10

[[Page 43510]]

                                                                        
Chloride........................... Non-detect........... 5.0 Chloroethane....................... Non-detect........... 21 Copper Cyanide..................... Non-detect........... 1.7 Cyanide............................ Non-detect........... 1.0 Cyanogen Bromide................... Non-detect........... 6.6 Cyanogen Chloride.................. Non-detect........... 8.6 Di-selenium-tetra-sulfide.......... Non-detect........... 1400 Dibenzofuran....................... Non-detect........... 980 Dibromochloromethane............... Non-detect........... 21 Endosulfan I....................... Non-detect........... 1.0 Endosulfan II...................... Non-detect........... 1.0 Endothal........................... Non-detect........... 100 Endrin............................. Non-detect........... 1.0 Endrin aldehyde.................... Non-detect........... 1.0 Endrin ketone...................... Non-detect........... 1.0 Epichlorohydrin.................... Non-detect........... 26 Ethyl carbamate.................... Non-detect........... 100 Ethylene glycol monoethyl ether.... Non-detect........... 100 Ethylenethiourea (2- Non-detect........... 100
 Imidazolidinethione).                                                  
Fluoride........................... Non-detect........... 3.0 Heptachlor......................... Non-detect........... 1.0 Heptachlor epoxide................. Non-detect........... 2.0 Lead acetate....................... Non-detect........... 110 Lead phosphate..................... Non-detect........... 79 MNNG (N-Metyl-N-nitroso-N'- Non-detect........... 100
 nitroguanidine).                                                       
Methomyl........................... Non-detect........... 50 N-Nitrosodiphenylamine............. Non-detect........... 980 Nickel Cyanide..................... Non-detect........... 3.5 Nickel carbonyl.................... Non-detect........... 330 Nicotine........................... Non-detect........... 100 Octachlorodibenzodioxin............ Non-detect........... 130 Octachlorodibenzofuran............. Non-detect........... 130 Osmium tetraoxide.................. Non-detect........... 40 Phenanthrene....................... 860.................. ............ Phenylthiourea..................... Non-detect........... 50 Potassium Cyanide.................. Non-detect........... 2.5 Potassium Silver Cyanide........... Non-detect........... 2.9 Propargyl alcohol.................. Non-detect........... 26 Pyrene............................. 610.................. ............ Selenium dioxide................... Non-detect........... 0.40 Selenium sulfide................... Non-detect........... 0.63 Silver Cyanide..................... Non-detect........... 2.6 Silvex............................. Non-detect........... 5.1 Strychnine......................... Non-detect........... 100 Tetra-selenium-tetra-sulfide....... Non-detect........... 2600 Tetraethyl lead.................... Non-detect........... 94 Thallium acetate................... Non-detect........... 26 Thallium carbonate................. Non-detect........... 23 Thallium chloride.................. Non-detect........... 24 Thallium nitrate................... Non-detect........... 27 Thallium oxide..................... Non-detect........... 21 Thallium sulfate................... Non-detect........... 25 Thioacetamide...................... Non-detect........... 50 Thiofanox.......................... Non-detect........... 100 Thiourea........................... Non-detect........... 50 Toluene-2,4-diamine................ Non-detect........... 50 Toluene-2,6-diamine................ Non-detect........... 50 Vanadium pentoxide................. Non-detect........... 18 Zinc Cyanide....................... Non-detect........... 2.3 Zinc phosphide..................... Non-detect........... 11 alpha-BHC.......................... Non-detect........... 5.0 beta-BHC........................... Non-detect........... 5.0 delta-BHC.......................... Non-detect........... 1.0 gamma-BHC (Lindane)................ Non-detect........... 1.0 m-Dinitrobenzene................... Non-detect........... 980 p-Toluidine........................ Non-detect........... 100 trans-1,3-Dichloropropene.......... Non-detect........... 21

[[Page 43511]]

Table 5.--Detection and Detection Limit Values for a Possible Composite Fuel Specification--50th Percentile Analysis


                                                               Maximum  
                                      Concentration limit     detection 
Chemical name (mg/kg at 10,000 Btu/ limit (mg/
                                              lb)                kg)    

1,1,1-Trichloroethane.............. Non-detect........... 17 1,1,2-Trichloro-1,2,2- Non-detect........... 29
 trifluoroethane.                                                       
1,1-Dichloro-1-propene............. Non-detect........... 29 1,1-Dichloroethane................. Non-detect........... 17 1,2,3,4,6,7,8-Heptachlorodibenzo-p- Non-detect........... 64
 dioxin.                                                                
1,2,3,4,6,7,8-Heptachlorodibenzo-p- Non-detect........... 64
 furan.                                                                 
1,2,3,4-Tetrachlorobenzene......... Non-detect........... 100 1,2,3,5-Tetrachlorobenzene......... Non-detect........... 100 1,2,3,6,7,8-Hexachlorodibenzo-p- Non-detect........... 64
 dioxin.                                                                
1,2,3,6,7,8-Hexachlorodibenzo-p- Non-detect........... 64
 furan.                                                                 
1,2,3,7,8-Pentachlorodibenzo-p- Non-detect........... 64
 dioxin.                                                                
1,2,3,7,8-Pentachlorodibenzo-p- Non-detect........... 64
 furan.                                                                 
1,2,3-Trichlorobenzene............. Non-detect........... 100 1,2-Dichloroethane................. Non-detect........... 17 1,2-Dichloropropane................ Non-detect........... 17 1,3-Dichloro-2-propanol............ Non-detect........... 29 1,3-Dichloropropane................ Non-detect........... 29 1,3-Propane sultone................ Non-detect........... 100 1-Chloronaphthalene................ Non-detect........... 100 2,2-Dichloropropane................ Non-detect........... 29 2,3,4,5-Tetrachlorophenol.......... Non-detect........... 100 2,3,4-Trichlorophenol.............. Non-detect........... 100 2,3,5-Trichlorophenol.............. Non-detect........... 100 2,3,6-Trichlorophenol.............. Non-detect........... 100 2,3,7,8-Tetrachlorodibenzo-p-dioxin Non-detect........... 26 2,3,7,8-Tetrachlorodibenzo-p-furan. Non-detect........... 26 2,3-Dichloro-1-propene............. Non-detect........... 29 2,3-Dichlorophenol................. Non-detect........... 100 2,4-D.............................. Non-detect........... 5.7 2,5-Dichlorophenol................. Non-detect........... 100 2-Fluoroacetamide.................. Non-detect........... 100 2-Methylnaphthalene................ 1000................. ............ 2-Nitropropane..................... Non-detect........... 29 3,3'-Dimethoxybenzidine............ Non-detect........... 100 3,4-Dichlorophenol................. Non-detect........... 100 3,5-Dichlorophenol................. Non-detect........... 100 3-/4-Chlorophenol.................. Non-detect........... 100 3-Nitroaniline..................... Non-detect........... 220 4,4'-methylene-bis(2-chloroaniline) Non-detect........... 100 4-Aminopyrridine................... Non-detect........... 100 4-Chlorophenyl phenyl ether........ Non-detect........... 220 6-Propyl-2-thiouracil.............. Non-detect........... 100 Acenaphthene....................... Non-detect........... 220 Acetone cyanohydrin................ Non-detect........... 100 Allyl alcohol...................... Non-detect........... 29 Ammonium vanadate.................. Non-detect........... 31 Anthracene......................... Non-detect........... 220 Arochlor-1016...................... Non-detect........... 1.1 Arochlor-1221...................... Non-detect........... 1.1 Arochlor-1232...................... Non-detect........... 1.1 Arochlor-1242...................... Non-detect........... 1.1 Arochlor-1248...................... Non-detect........... 1.1 Arochlor-1254...................... Non-detect........... 1.1 Arochlor-1260...................... Non-detect........... 1.1 Arsenic acid....................... Non-detect........... 0.27 Arsenic pentoxide.................. Non-detect........... 0.22 Arsenic trioxide................... Non-detect........... 0.19 Barium Cyanide..................... Non-detect........... 3.7 Benzal chloride.................... Non-detect........... 100 Benzenethiol....................... Non-detect........... 29 Benzyl chloride.................... Non-detect........... 100 Bis(2-chloroethoxy)methane......... Non-detect........... 220 Bis(2-chloroethyl)ether............ Non-detect........... 220 Bis(2-ethylhexyl)phthalate......... Non-detect........... 220 Bromide............................ Non-detect........... 5.0 Bromodichloromethane............... Non-detect........... 17 Calcium Cyanide.................... Non-detect........... 1.8 Calcium chromate................... Non-detect........... 4.2

[[Page 43512]]

                                                                        
Chlordane.......................... Non-detect........... 11 Chloride........................... 2.6.................. ............ Chloroethane....................... Non-detect........... 17 Copper Cyanide..................... Non-detect........... 1.7 Cyanide............................ Non-detect........... 1.0 Cyanogen Bromide................... Non-detect........... 6.6 Cyanogen Chloride.................. Non-detect........... 8.6 Di-selenium-tetra-sulfide.......... Non-detect........... 420 Dibenzofuran....................... Non-detect........... 220 Dibromochloromethane............... Non-detect........... 17 Endosulfan I....................... Non-detect........... 1.1 Endosulfan II...................... Non-detect........... 1.1 Endothal........................... Non-detect........... 100 Endrin............................. Non-detect........... 1.1 Endrin aldehyde.................... Non-detect........... 1.1 Endrin ketone...................... Non-detect........... 1.1 Epichlorohydrin.................... Non-detect........... 29 Ethyl carbamate.................... Non-detect........... 100 Ethylene glycol monoethyl ether.... Non-detect........... 100 Ethylenethiourea (2- Non-detect........... 14
 Imidazolidinethione).                                                  
Fluoride........................... Non-detect........... 3.0 Heptachlor......................... Non-detect........... 1.1 Heptachlor epoxide................. Non-detect........... 2.3 Lead acetate....................... Non-detect........... 26 Lead phosphate..................... Non-detect........... 18 MNNG (N-Metyl-N-nitroso-N'- Non-detect........... 14
 nitroguanidine).                                                       
Methomyl........................... Non-detect........... 7.0 N-Nitrosodiphenylamine............. Non-detect........... 220 Nickel Cyanide..................... Non-detect........... 3.5 Nickel carbonyl.................... Non-detect........... 8.2 Nicotine........................... Non-detect........... 100 Octachlorodibenzodioxin............ Non-detect........... 130 Octachlorodibenzofuran............. Non-detect........... 130 Osmium tetraoxide.................. Non-detect........... 40 Phenanthrene....................... 250.................. ............ Phenylthiourea..................... Non-detect........... 7.0 Potassium Cyanide.................. Non-detect........... 2.5 Potassium Silver Cyanide........... Non-detect........... 2.9 Propargyl alcohol.................. Non-detect........... 29 Pyrene............................. 140.................. ............ Selenium dioxide................... Non-detect........... 0.26 Selenium sulfide................... Non-detect........... 0.41 Silver Cyanide..................... Non-detect........... 2.6 Silvex............................. Non-detect........... 5.7 Strychnine......................... Non-detect........... 100 Tetra-selenium-tetra-sulfide....... Non-detect........... 810 Tetraethyl lead.................... Non-detect........... 22 Thallium acetate................... Non-detect........... 18 Thallium carbonate................. Non-detect........... 16 Thallium chloride.................. Non-detect........... 17 Thallium nitrate................... Non-detect........... 18 Thallium oxide..................... Non-detect........... 15 Thallium sulfate................... Non-detect........... 17 Thioacetamide...................... Non-detect........... 7.0 Thiofanox.......................... Non-detect........... 100 Thiourea........................... Non-detect........... 7.0 Toluene-2,4-diamine................ Non-detect........... 7.0 Toluene-2,6-diamine................ Non-detect........... 7.0 Vanadium pentoxide................. Non-detect........... 18 Zinc Cyanide....................... Non-detect........... 2.3 Zinc phosphide..................... Non-detect........... 0.37 alpha-BHC.......................... Non-detect........... 1.2 beta-BHC........................... Non-detect........... 1.2 delta-BHC.......................... Non-detect........... 1.1 gamma-BHC (Lindane)................ Non-detect........... 1.1 m-Dinitrobenzene................... Non-detect........... 220 p-Toluidine........................ Non-detect........... 100

[[Page 43513]]

                                                                        
trans-1,3-Dichloropropene.......... Non-detect........... 17

Table 6.--Detection and Detection Limit Values for a Possible Composite Fuel Specification--90th Percentile

                                                    Analysis                                                    

                                                                                                      Maximum   
                      Chemical name                         Concentration limit (mg/kg at 10,000     detection  
                                                                          Btu/lb)                  limit (mg/kg)

1,1,1-Trichloroethane.................................... Non-detect........................... 34 1,1,2-Trichloro-1,2,2-trifluoroethane.................... Non-detect........................... 30 1,1-Dichloro-1-propene................................... Non-detect........................... 30 1,1-Dichloroethane....................................... Non-detect........................... 34 1,2,3,4,6,7,8-Heptachlorodibenzo-p-dioxin................ Non-detect........................... 74 1,2,3,4,6,7,8-Heptachlorodibenzo-p-furan................. Non-detect........................... 74 1,2,3,4-Tetrachlorobenzene............................... Non-detect........................... 100 1,2,3,5-Tetrachlorobenzene............................... Non-detect........................... 100 1,2,3,6,7,8-Hexachlorodibenzo-p-dioxin................... Non-detect........................... 74 1,2,3,6,7,8-Hexachlorodibenzo-p-furan.................... Non-detect........................... 74 1,2,3,7,8-Pentachlorodibenzo-p-dioxin.................... Non-detect........................... 74 1,2,3,7,8-Pentachlorodibenzo-p-furan..................... Non-detect........................... 74 1,2,3-Trichlorobenzene................................... Non-detect........................... 100 1,2-Dichloroethane....................................... Non-detect........................... 34 1,2-Dichloropropane...................................... Non-detect........................... 34 1,3-Dichloro-2-propanol.................................. Non-detect........................... 30 1,3-Dichloropropane...................................... Non-detect........................... 30 1,3-Propane sultone...................................... Non-detect........................... 100 1-Chloronaphthalene...................................... Non-detect........................... 100 2,2-Dichloropropane...................................... Non-detect........................... 30 2,3,4,5-Tetrachlorophenol................................ Non-detect........................... 100 2,3,4-Trichlorophenol.................................... Non-detect........................... 100 2,3,5-Trichlorophenol.................................... Non-detect........................... 100 2,3,6-Trichlorophenol.................................... Non-detect........................... 100 2,3,7,8-Tetrachlorodibenzo-p-dioxin...................... Non-detect........................... 30 2,3,7,8-Tetrachlorodibenzo-p-furan....................... Non-detect........................... 30 2,3-Dichloro-1-propene................................... Non-detect........................... 30 2,3-Dichlorophenol....................................... Non-detect........................... 100 2,4-D.................................................... Non-detect........................... 6.7 2,5-Dichlorophenol....................................... Non-detect........................... 100 2-Fluoroacetamide........................................ Non-detect........................... 100 2-Methylnaphthalene...................................... 2500................................. - 2-Nitropropane........................................... Non-detect........................... 30 3,3'-Dimethoxybenzidine.................................. Non-detect........................... 100 3,4-Dichlorophenol....................................... Non-detect........................... 100 3,5-Dichlorophenol....................................... Non-detect........................... 100 3-/4-Chlorophenol........................................ Non-detect........................... 100 3-Nitroaniline........................................... Non-detect........................... 700 4,4'-methylene-bis(2-chloroaniline)...................... Non-detect........................... 100 4-Aminopyrridine......................................... Non-detect........................... 100 4-Chlorophenyl phenyl ether.............................. Non-detect........................... 700 6-Propyl-2-thiouracil.................................... Non-detect........................... 100 Acenaphthene............................................. Non-detect........................... 700 Acetone cyanohydrin...................................... Non-detect........................... 100 Allyl alcohol............................................ Non-detect........................... 30 Ammonium vanadate........................................ Non-detect........................... 86 Anthracene............................................... Non-detect........................... 700 Arochlor-1016............................................ Non-detect........................... 1.3 Arochlor-1221............................................ Non-detect........................... 1.3 Arochlor-1232............................................ Non-detect........................... 1.3 Arochlor-1242............................................ Non-detect........................... 1.3 Arochlor-1248............................................ Non-detect........................... 1.3 Arochlor-1254............................................ Non-detect........................... 1.3 Arochlor-1260............................................ Non-detect........................... 1.3 Arsenic acid............................................. Non-detect........................... 0.41 Arsenic pentoxide........................................ Non-detect........................... 0.34 Arsenic trioxide......................................... Non-detect........................... 0.29 Barium Cyanide........................................... Non-detect........................... 3.7

[[Page 43514]]

                                                                                                                
Benzal chloride.......................................... Non-detect........................... 100 Benzenethiol............................................. Non-detect........................... 30 Benzyl chloride.......................................... Non-detect........................... 100 Bis(2-chloroethoxy)methane............................... Non-detect........................... 700 Bis(2-chloroethyl)ether.................................. Non-detect........................... 700 Bis(2-ethylhexyl)phthalate............................... Non-detect........................... 700 Bromide.................................................. Non-detect........................... 5.0 Bromodichloromethane..................................... Non-detect........................... 34 Calcium Cyanide.......................................... Non-detect........................... 1.8 Calcium chromate......................................... Non-detect........................... 6.6 Chlordane................................................ Non-detect........................... 13 Chloride................................................. 2.7.................................. - Chloroethane............................................. Non-detect........................... 34 Copper Cyanide........................................... Non-detect........................... 1.7 Cyanide.................................................. Non-detect........................... 1.0 Cyanogen Bromide......................................... Non-detect........................... 6.6 Cyanogen Chloride........................................ Non-detect........................... 8.6 Di-selenium-tetra-sulfide................................ Non-detect........................... 1200 Dibenzofuran............................................. Non-detect........................... 700 Dibromochloromethane..................................... Non-detect........................... 34 Endosulfan I............................................. Non-detect........................... 1.3 Endosulfan II............................................ Non-detect........................... 1.3 Endothal................................................. Non-detect........................... 100 Endrin................................................... Non-detect........................... 1.3 Endrin aldehyde.......................................... Non-detect........................... 1.3 Endrin ketone............................................ Non-detect........................... 1.3 Epichlorohydrin.......................................... Non-detect........................... 30 Ethyl carbamate.......................................... Non-detect........................... 100 Ethylene glycol monoethyl ether.......................... Non-detect........................... 100 Ethylenethiourea (2-Imidazolidinethione)................. Non-detect........................... 110 Fluoride................................................. Non-detect........................... 3.0 Heptachlor............................................... Non-detect........................... 1.3 Heptachlor epoxide....................................... Non-detect........................... 2.7 Lead acetate............................................. Non-detect........................... 74 Lead phosphate........................................... Non-detect........................... 53 MNNG (N-Metyl-N-nitroso-N'-nitroguanidine)............... Non-detect........................... 110 Methomyl................................................. Non-detect........................... 54 N-Nitrosodiphenylamine................................... Non-detect........................... 700 Nickel Cyanide........................................... Non-detect........................... 3.5 Nickel carbonyl.......................................... Non-detect........................... 46 Nicotine................................................. Non-detect........................... 100 Octachlorodibenzodioxin.................................. Non-detect........................... 150 Octachlorodibenzofuran................................... Non-detect........................... 150 Osmium tetraoxide........................................ Non-detect........................... 40 Phenanthrene............................................. 730.................................. - Phenylthiourea........................................... Non-detect........................... 54 Potassium Cyanide........................................ Non-detect........................... 2.5 Potassium Silver Cyanide................................. Non-detect........................... 2.9 Propargyl alcohol........................................ Non-detect........................... 30 Pyrene................................................... 600.................................. - Selenium dioxide......................................... Non-detect........................... 0.34 Selenium sulfide......................................... Non-detect........................... 0.53 Silver Cyanide........................................... Non-detect........................... 2.6 Silvex................................................... Non-detect........................... 6.7 Strychnine............................................... Non-detect........................... 100 Tetra-selenium-tetra-sulfide............................. Non-detect........................... 2300 Tetraethyl lead.......................................... Non-detect........................... 63 Thallium acetate......................................... Non-detect........................... 28 Thallium carbonate....................................... Non-detect........................... 25 Thallium chloride........................................ Non-detect........................... 26 Thallium nitrate......................................... Non-detect........................... 29 Thallium oxide........................................... Non-detect........................... 23 Thallium sulfate......................................... Non-detect........................... 27 Thioacetamide............................................ Non-detect........................... 54 Thiofanox................................................ Non-detect........................... 100 Thiourea................................................. Non-detect........................... 54 Toluene-2,4-diamine...................................... Non-detect........................... 54 Toluene-2,6-diamine...................................... Non-detect........................... 54 Vanadium pentoxide....................................... Non-detect........................... 18

[[Page 43515]]

                                                                                                                
Zinc Cyanide............................................. Non-detect........................... 2.3 Zinc phosphide........................................... Non-detect........................... 1.7 alpha-BHC................................................ Non-detect........................... 1.4 beta-BHC................................................. Non-detect........................... 1.4 delta-BHC................................................ Non-detect........................... 1.3 gamma-BHC (Lindane)...................................... Non-detect........................... 1.3 m-Dinitrobenzene......................................... Non-detect........................... 700 p-Toluidine.............................................. Non-detect........................... 100 trans-1,3-Dichloropropene................................ Non-detect........................... 34

Dated: August 15, 1996.
Elizabeth A. Cotsworth,
Acting Director, Office of Solid Waste. [FR Doc. 96-21628 Filed 8-22-96; 8:45 am] BILLING CODE 6560-50-P

 
 


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