Argonne National Laboratory

Advanced Photon Source

A U.S. Department of Energy, Office of Science,
Office of Basic Energy Sciences national synchrotron x-ray research facility

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APS Beamline Directory

APS Synchrotron Techniques

The unique properties of synchrotron radiation are its continuous spectrum, high flux and brightness, and high coherence, which make it an indispensable tool in the exploration of matter. The wavelengths of the emitted photons span a range of dimensions from the atomic level to biological cells, thereby providing incisive probes for advanced research in materials science, physical and chemical sciences, metrology, geosciences, environmental sciences, biosciences, medical sciences, and pharmaceutical sciences. The features of synchrotron radiation are especially well matched to the needs of nanoscience.

This breadth of problems requires an extensive suite of probes. The basic components of a beamline, however, share general similarities as shown in the schematic diagram below.


synchrotron radiation diagram

The fundamental parameters that we use to perceive the physical world (energy, momentum, position, and time) correspond to three broad categories of synchrotron experimental measurement techniques: spectroscopy, scattering, and imaging. By exploiting the short pulse lengths of synchrotron radiation, each technique can be performed in a timing fashion.

Spectroscopy is used to study the energies of particles that are emitted or absorbed by samples that are exposed to the light-source beam and is commonly used to determine the characteristics of chemical bonding and electron motion.

Scattering makes use of the patterns of light produced when x-rays are deflected by the closely spaced lattice of atoms in solids and is commonly used to determine the structures of crystals and large molecules such as proteins.

Imaging techniques use the light-source beam to obtain pictures with fine spatial resolution of the samples under study and are used in diverse research areas such as cell biology, lithography, infrared microscopy, radiology, and x-ray tomography.

SPECTROSCOPY

Technique Beamline
Hard X-Ray Spectroscopy
Diffraction anomalous fine structure (DAFS) 10-ID-B
Fluorescence spectroscopy 12-BM-B
Intensity fluctuation spectroscopy 8-ID-I , 8-ID-E*
Magnetic circular dichroism (XMCD-Hard X-ray) 4-ID-D
Micro-XAFS 20-BM-B , 20-ID-B,C , 18-ID-D , 13-ID-C,D , 10-ID-B , 2-ID-D
Time Resolved XAFS 7-ID-B,C,D , 11-ID-D , 20-ID-B,C
X-ray Emission Spectroscopy 16-ID-D , 16-ID
X-ray Raman Scattering 16-ID-D , 20-ID-B,C , 16-ID
X-ray absorption fine structure (XAFS) 12-BM-B , 13-BM-D , 20-BM-B , 20-ID-B,C , 5-BM-D , 11-ID-D , 9-BM-B,C , 13-ID-C,D , 10-ID-B
X-ray photon correlation spectroscopy 8-ID-I , 8-ID-E*
Metrology, Optics, Detector Calibration, Etc.
X-ray Optics Development/Techniques 5-ID-B,C,D
Soft X-Ray Spectroscopy
Magnetic circular dichroism (XMCD-Soft X-ray) 4-ID-C
X-ray Photoemission spectroscopy (XPS) 4-ID-C
X-ray magnetic linear dichroism (XMLD) 4-ID-C

SCATTERING

Technique Beamline
Hard X-Ray Diffraction
General Diffraction 33-ID-D,E , 12-BM-B , 6-ID-B,C , 33-ID-E* , 33-BM-C , 2-BM-B , 11-ID-D
High Pressure Multi-Anvil Press (LVP) 13-BM-D , 13-ID-C,D
High Presure Diamond Anvil Cell (DAC) 3-ID-B,C,D , 13-BM-D , 13-BM-C , 13-ID-C,D , 16-ID
High energy x-ray diffraction 6-ID-D , 11-ID-C , 5-BM-D , 1-ID-C
Magnetic x-ray scattering 6-ID-B,C , 6-ID-D , 4-ID-C , 4-ID-D
Micro - diffraction 34-ID-C,E , 23-ID-D , 23-ID-B , 16-ID-B , 2-BM-B , 34-ID-E , 15-ID-B,C,D , 18-ID-D* , 13-ID-C,D , 16-ID , 2-ID-D
Powder ADXD diffraction 16-BM-D
Powder EDXD diffraction 16-BM-B
Powder diffraction 12-BM-B , 16-ID-B , 6-ID-D , 5-BM-C , 33-BM-C , 5-ID-B,C,D , 16-ID
Single crystal diffraction 16-BM-B , 16-ID-B , 31-ID-D , 16-BM-D , 15-ID-B,C,D , 13-BM-C , 16-ID
Surface diffraction 33-ID-D,E , 12-ID-B,C,D , 33-ID-E* , 5-ID-B,C,D* , 13-BM-C , 20-ID-B,C* , 15-ID-B,C,D
Surface diffraction (UHV) 6-ID-B,C*
Hard X-Ray Scattering
Anomalous and Resonant Scattering (Hard X-ray) 33-ID-D,E , 6-ID-B,C , 33-BM-C , 15-ID-B,C,D , 4-ID-D
Coherent x-ray scattering 34-ID-C,E , 8-ID-I*
Diffuse x-ray scattering 33-ID-D,E , 33-BM-C , 11-ID-C
Fiber Diffraction 14-BM-C , 31-ID-D , 18-ID-D
Grazing Incidence Diffraction 6-ID-B,C , 33-BM-C
Grazing Incidence Small Angle Sattering ( GISAXS ) 12-ID-B,C,D , 8-ID-E
Inelastic X-ray Scattering 3-ID-B,C,D , 9-ID-B,C , 30-ID-B,C , 16-ID-D , 13-ID-C,D , 16-ID
Liquid scattering 9-ID-B,C , 6-ID-B,C* , 15-ID-B,C,D
Nuclear Resonant Scattering 3-ID-B,C,D , 16-ID-D , 16-ID
Pair Distribution Function (PDF) 6-ID-D , 11-ID-B , 11-ID-C
Resonant Inelastic X-ray Scattering 9-ID-B,C
Small angle x-ray scattering (SAXS) 8-ID-I* , 12-ID-B,C,D , 5-ID-B,C,D , 15-ID-B,C,D , 18-ID-D
Time-resolved x-ray scattering 7-ID-B,C,D , 18-ID-D* , 14-ID-B
Ultra-small Angle X-ray Scattering (USAXS) 32-ID-B,C
Wide angle x-ray scattering (WAXS) 12-ID-B,C,D , 15-ID-B,C,D , 5-ID-B,C,D
X-ray Reflectivity 33-ID-D,E , 12-BM-B , 33-BM-C , 5-ID-B,C,D* , 8-ID-E*
X-ray standing waves 33-ID-D,E , 5-ID-B,C,D*
Macromolecular Crystallography
Anomalous diffraction (MAD/SAD) 23-ID-B , 19-BM-D , 23-ID-D , 17-ID-B , 21-ID-G , 19-ID-D , 21-ID-D , 24-ID-C , 17-BM-B , 21-ID-F , 14-ID-B
Biohazards at the BSL2/3 level 14-BM-C , 14-ID-B
Laue crystallography 14-ID-B
Macromolecular crystallography 23-ID-B , 24-ID-E , 23-ID-D , 22-ID-D , 31-ID-D , 14-BM-C , 22-BM-D , 21-ID-G , 21-ID-F , 21-ID-D , 24-ID-C , 17-BM-B , 14-ID-B , 17-ID-B
Micro-beam 24-ID-E , 23-ID-D , 23-ID-B
Multi wavelength anomalous dispersion (MAD) 22-ID-D
Single wavelength anomalous dispersion (SAD) 31-ID-D
Subatomic (<0.85 Å) resolution 23-ID-D , 23-ID-B , 14-BM-C , 19-ID-D
Ultra low temperature (15K) 19-BM-D , 19-ID-D
Soft X-Ray Scattering
Anomalous and Resonant Scattering (Soft X-ray) 4-ID-C
Coherent x-ray scattering (Soft X-ray) 2-ID-B

IMAGING

Technique Beamline
Hard X-Ray Imaging
Micro-Fluorescence ( Hard X-ray ) 20-BM-B , 2-ID-E , 20-ID-B,C , 2-ID-D , 18-ID-D , 13-ID-C,D , 10-ID-B
Phase contrast imaging 2-BM-B , 32-ID-B,C
Radiography 7-ID-B,C,D , 32-ID-B,C
Tomography 13-BM-D , 5-BM-C , 2-BM-B
Soft X-Ray Imaging
Micro-Fluorescence (Soft X-ray ) 2-ID-B
X-ray Photoemission electron microscopy (X-PEEM) 4-ID-C

* denotes that the beamline will only accept a proposal for that technique if it is a collaboration with the CAT