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| Orientation and Training Food and Drug Administration |
| DOCUMENT NO.: IV-05 | VERSION NO.:1.2 | Section 5 - Pesticides Analysis | EFFECTIVE DATE: 10/01/2003 | REVISED: 06/27/2008 |
5.7 Sample Results, Evaluation, and Reporting
A. Objective To evaluate gas chromatograms and identify pesticide residues. B. Assignment - Under the trainer's observation, put the correct GC instrumentation into operation for multiresidue determination of the previously prepared samples.
- Submit daily chromatograms demonstrating proper analyte separation and instrumentation sensitivity, according to laboratory SOP.
- Inject the correct volumes of the prepared samples. With trainer assistance, evaluate, identify, and quantify residues, and report results.
C. References - U.S. Food & Drug Administration, Center for Food Safety and Applied Nutrition, Office of Plant, Dairy Foods and Beverages. Makovi, C. M. (Ed.), McMahon, B. M. (Ed. Emerita). (1994). Pesticide analytical manual-multiresidue methods (3rd ed., Vol. I, Appendix I, PESTDATA, updated October 1999). R.O.W. Sciences, Inc.
- FACTS reporting manual.
- Pesticide Glossary.
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