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Evaluation of the Laboratory Asphalt
Stability Test

February 2005

Publication No. FHWA-HRT-04-111

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Turner-Fairbank Highway Research Center
63000 Georgetown Pike
McLean, VA 22101


FOREWORD

The Laboratory Asphalt Stability Test (LAST) was proposed by the researchers of the National Cooperative Highway Research Program (NCHRP) 9-10 program as a possible new method to evaluate the storage stability of modified asphalts. Federal Highway Administration (FHWA) was assigned the responsibility for evaluating the LAST device. This involved three tasks:

The modified asphalts used in NCHRP 90-07 were investigated in this study. These included elastomers, plastomers, elasto-plastomers, and crumb rubber. The eight binders chosen all met the Superpave performance grading of 70-28 (PG70-28). This report details the work at FHWA's Turner-Fairbank Highway Research Center in evaluating the thermal stability of modified binders using the LAST device.

Paul Teng, Director
Office of Infrastructure Research and Development

Notice

This document is disseminated under the sponsorship of the U.S. Department of Transportation in the interest of information exchange. The U.S. Government assumes no liability for the use of the information contained in this document. This report does not constitute a standard, specification, or regulation.

The U.S. Government does not endorse products or manufacturers. Trademarks or manufacturers' names appear in this report only because they are considered essential to the objective of the document.

Quality Assurance Statement

The Federal Highway Administration (FHWA) provides high-quality information to serve Government, industry, and the public in a manner that promotes public understanding. Standards and policies are used to ensure and maximize the quality, objectivity, utility, and integrity of its information. FHWA periodically reviews quality issues and adjusts its programs and processes to ensure continuous quality improvement.


1. Report No. FHWA-RD-04-111 2. Government Accession No. 3. Recipient's Catalog No.
4. Title and Subtitle
Evaluation of the Laboratory Asphalt Stability Test
5. Report Date
February 2005
6. Performing Organization Code
7. Author(s)
Jack Youtcheff , N. Wijayatilleke, and A. Shenoy
8. Performing Organization Report No.
9. Performing Organization Name and Address
Office of Infrastructure Research and Development Federal Highway Administration 6300 Georgetown Pike McLean, VA 22101-2296
10. Work Unit No.

11. Contract or Grant No.

In House Report

12. Sponsoring Agency Name and Address
Office of Infrastructure Research and Development Federal Highway Administration 6300 Georgetown Pike McLean, VA 22101-2296
13. Type of Report and Period Covered
Final—July 2003
14. Sponsoring Agency Code
15. Supplementary Notes
FHWA Contact: Jack Youtcheff, HRDI-11
16. Abstract
The Laboratory Asphalt Stability Test (LAST) was proposed by the researchers of the National Cooperative Highway Research Program (NCHRP) 9-10 program as a possible new method to evaluate the storage stability of modified asphalts. The test involved exposing the binders with and without mechanical agitation at elevated temperatures for extended lengths of time to assess the thermal stability of the binders. The Federal Highway Administration (FHWA) was assigned the responsibility for evaluating the LAST. The task involved (a) procuring a commercial version of the LAST, (b) correcting perceived deficiencies, and (c) evaluating the test method thoroughly.
17. Key Words
Storage stability, LAST, test method, polymer-modified asphalt binders
18. Distribution Statement No restrictions. This document is available to the public through the National Technical Information Service, Springfield, VA 22161.
19. Security Classif. (of this report)
Unclassified
20. Security Classif. (of this page)
Unclassified
21. No of Pages
50
22. Price

Form DOT F 1700.7 (8-72) Reproduction of completed pages authorized


SI* (Modern Metric) Conversion Factors


TABLE OF CONTENTS

1. INTRODUCTION

2. EXPERIMENTAL DESIGN

3. RESULTS AND DISCUSSION

4. CONCLUDING REMARKS

APPENDIX A

APPENDIX B

APPENDIX C

ACKNOWLEDGEMENTS

REFERENCE

ADDITIONAL SOURCES

 

LIST OF FIGURES

  1. Schematic diagram of the original prototype LAST device

  2. The commercial LAST device 6

  3. Plot of temperature versus time showing the temperature control efficacy of the heating mantles used in the commercial unit of the LAST device 9

  4. Reproducibility of the G* value for six different samples of EVA grafted (B6232) with glass pipette

LIST OF TABLES

  1. Dimensional details of the LAST device

  2. List of the modified binders and some select Superpave values

  3. Time to failure in separation ratio Rs and degradation ratio Rd for the modified binders used in the study

  4. Results of the CTS test for the modified binders

  5. Results of the LAST device without agitation for the modified binders

  6. Elvaloy (B6228) separation ratios

  7. Elvaloy (B6228) degradation ratios

  8. SBS-lg (B6229) separation ratios

  9. SBS-lg (B6229) degradation ratios

  10. SBS-1 (B6230) separation ratios

  11. SBS-1 (B6230) degradation ratios

  12. SBS-rg (B6231) separation ratios

  13. SBS-rg (B6231) degradation ratios

  14. EVA (B6232) separation ratios

  15. EVA (B6232) degradation ratios

  16. EVA-g (B6233) separation ratios

  17. EVA-g (B6233) degradation ratios

  18. ESI (B6243) separation ratios

  19. ESI (B6243) degradation ratios

  20. CMCRA (B6251) separation ratios

  21. CMCRA (B6251) degradation ratios

  22. Elvaloy (B6228) separation ratios on replicates

  23. Elvaloy (B6228) degradation ratios on replicates

  24. Elvaloy (B6228) separation ratios on replicate reruns

  25. Elvaloy (B6228) degradation ratios on replicate reruns

  26. SBS-lg (B6299) separation ratios on replicates

  27. SBS-lg (B6229) degradation ratios on replicates

  28. SBS-lg (B6299) separation ratios on replicate reruns

  29. SBS-lg (B6229) degradation ratios on replicate reruns

  30. SBS-1 (B6230) separation ratios on replicates

  31. SBS-1 (B6230) degradation ratios on replicates

  32. SBS-rg (B6231) separation ratios on replicates

  33. SBS-rg (B6231) degradation ratios on replicates

  34. SBS-rg (B6231) separation ratios on replicate reruns

  35. SBS-rg (B6231) degradation ratios on replicate reruns

  36. EVA (B6232) separation ratios on replicates

  37. EVA (B6232) degradation ratios on replicates

  38. EVA (B6232) separation ratios on replicate reruns

  39. EVA (B6232) degradation ratios on replicate reruns

  40. EVA-g (B6233) separation ratios on replicates

  41. EVA-g (B6233) degradation ratios on replicates

  42. EVA-g (B6233) separation ratios on replicate reruns

  43. EVA-g (B6233) degradation ratios on replicate reruns

  44. ESI (B6243) separation ratios on replicates

  45. ESI (B6243) degradation ratios on replicates

  46. CMCRA (B6251) separation ratios on replicates

  47. CMCRA (B6251) degradation ratios on replicates

  48. CMCRA (B6251) separation ratios on replicate reruns

  49. CMCRA (B6251) degradation ratios on replicate reruns

  50. Data of separation rates and degradation rates

  51. Data of separation rates and degradation rate returns

 

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