[Code of Federal Regulations] [Title 49, Volume 2] [Revised as of October 1, 2002] From the U.S. Government Printing Office via GPO Access [CITE: 49CFR173.315] [Page 574-585] TITLE 49--TRANSPORTATION CHAPTER I--RESEARCH AND SPECIAL PROGRAMS ADMINISTRATION, DEPARTMENT OF TRANSPORTATION PART 173--SHIPPERS--GENERAL REQUIREMENTS FOR SHIPMENTS AND PACKAGINGS--Table of Contents Subpart G--Gases; Preparation and Packaging Sec. 173.315 Compressed gases in cargo tanks and portable tanks. (a) Liquefied compressed gases that are transported in UN portable tanks must be loaded and offered for transportation in accordance with portable tank provision T50 in Sec. 172.102 of this subchapter. A liquefied compressed gas offered for transportation in a cargo tank motor vehicle or a portable tank must be prepared in accordance with this section, Sec. 173.32, Sec. 173.33 and subpart E or subpart G of part 180 of this subchapter, as applicable. For cryogenic liquids, see Sec. 173.318. For marking requirements, see Secs. 172.326 and 172.328 of this subchapter. Except for UN portable tanks, a liquefied compressed gas must be loaded and offered for transportation in accordance with the following table: ---------------------------------------------------------------------------------------------------------------- Maximum permitted filling density Specification container required ------------------------------------------------------------------------------- Kind of gas Percent by volume Percent by weight (see par. (f) of Type (see Note 2) Minimum design (see Note 1) this section) pressure (psig) ---------------------------------------------------------------------------------------------------------------- Ammonia, anhydrous or Ammonia 56................ 82, See Note 5.... DOT-51, MC-330, MC- 265; See Note 17. solutions with greater than 50 331; See Notes 12 percent ammonia (see Notes 14 and 17. and 17). Ammonia solutions with more than See par. (c) of See Note 7........ DOT-51, MC-330, MC- 100; See par. (c) 35 percent but not more than 50 this section. 331; see Note 12. of this section. percent ammonia. Bromotrifluoromethane (R-13B1 or 133............... See Note 7........ DOT-51, MC-330, MC- 365. H-1301); (See Note 9). 331. Butadiene, stabilized........... See par. (b) of See par. (b) of DOT-51, MC-330, MC- 100. this section. this section. 331. Carbon dioxide, refrigerated See par. (c)(1) of 95................ ......do.......... 200; see Note 3. liquid. this section. Chlorine........................ 125............... See Note 7........ DOT-51, MC-330, MC- 225; See Notes 4 331. and 8. Chlorodifluoroethane (R-142b) (1- 100............... See Note 7........ DOT-51, MC-330, MC- 100. Chloro 1,1-difluoroethane); 331. (See Note 9). Chlorodifluoromethane (R-22); 105............... See Note 7........ DOT-51, MC-330, MC- 250. (See Note 9). 331. Chloropentafluoroethane (R-115); See par. (c) of See Note 7........ DOT-51, MC-330, MC- See par. (c) of (See Note 9). this section. 331. this section. Chlorotrifluoromethane (R-13); See par. (c) of See Note 7........ DOT-51, MC-330, MC- See par. (c) of (See Note 9). this section. 331. this section. Dichlorodifluoromethane (R-12); 119............... See Note 7........ DOT-51, MC-330, MC- 150. (See Note 9). 331. [[Page 575]] Difluoroethane (R-152a); (See 79................ See Note 7........ DOT-51, MC-330, MC- 150. Note 9). 331. Dimethyl ether (see Note 16).... 59................ ......do.......... ......do.......... 200. Dimethylamine, anhydrous........ 59................ See Note 7........ DOT-51, MC-330, MC- 150. 331. Division 2.1, materials not See par. (c) of See Note 7........ DOT-51, MC-330, MC- See Note 18. specifically provided for in this section. 331. this table. Division 2.2, materials not See par. (c) of See Note 7........ DOT-51, MC-330, MC- See Note 19. specifically provided for in this section. 331. this table. Division 2.3, Hazard Zone A, See par. (c) of See Note 7........ DOT-51, MC-330, MC- See Note 20. materials not specifically this section. 331; See Note 23. provided for in this table. Division 2.3, Hazard Zone B, See par. (c) of See Note 7........ DOT-51, MC-330, MC- See Note 20. materials not specifically this section. 331; See Note 23. provided for in this table. Division 2.3, Hazard Zone C, See par. (c) of See Note 7........ DOT-51, MC-330, MC- See Note 21. materials not specifically this section. 331; See Note 24. provided for in this table. Division 2.3, Hazard Zone D, See par. (c) of See Note 7........ DOT-51, MC-330, MC- See Note 22. materials not specifically this section. 331; See Note 25. provided for in this table. Ethane, refrigerated liquid..... .................. See par. (c) of MC-331, MC-338.... 100; see Note 11. this section. Ethane-propane mixture, .................. See par. (c) of MC-331, MC-338.... 275; see Note 11. refrigerated liquid. this section. Hexafluoropropylene............. 110............... See Note 7........ DOT-51, MC-330, MC- 250. 331. Hydrogen chloride, refrigerated 103.0............. See Note 7........ MC-331, MC-338.... 100; see Note 11. liquid. 91.6.............. ......do.......... ......do.......... 300; see Note 11. 86.7.............. ......do.......... ......do.......... 450; see Note 11. Liquefied petroleum gas (see See par. (b) of See par. (b) of DOT-51, MC-330, MC- See par. (c) of Note 15). this section. this section. 331; See Note 26. this section. Methylacetylene-propadiene, 53................ 90................ DOT 51, MC 330, MC 200. stabilized (see Note 13). 331. Methylamine, anhydrous.......... 60................ See Note 7........ DOT-51, MC-330, MC- .................. 331.. Methyl chloride................. 84................ 88.5.............. ......do.......... 150. Methyl chloride (optional ......do.......... See Note 6........ DOT-51............ 225. portable tank 2,000 pounds water capacity, fusible plug). Methyl mercaptan................ 80................ 90................ DOT-51, MC-330, MC- 100. 331; See Note 23. Nitrous oxide, refrigerated See par. (c)(1) of 95................ DOT-51, MC-330, MC- 200; See Note 3. liquid. this section. 331. Refrigerant gas, n.o.s. or See par. (c) of See Note 7........ DOT-51, MC-330, MC- See par. (c) of Dispersant gas, n.o.s. (See this section. 331. this section. Note 9). Sulfur dioxide (tanks not over 125............... 87.5.............. DOT-51, MC-330, MC- 150; See Note 4. 1,200 gallons water capacity). 331; See Note 24. Sulfur dioxide (tanks over 1,200 125............... 87.5.............. DOT-51, MC-330, MC- 125; See Note 4. gallons water capacity). 331; See Note 24. Sulfur dioxide (optional 125............... See Note 6........ DOT-51; See Note 225. portable tank 1,000-2,000 24. pounds water capacity, fusible plug). Trimethylamine, anhydrous....... 57................ See Note 7........ DOT-51, MC-330, MC- 150. 331. Vinyl chloride.................. 84 (see Note 13).. See Note 7........ MC-330, MC-331.... 150. Vinyl fluoride, stabilized...... 66................ ......do.......... ......do.......... 250; see Note 11. Vinyl methyl ether.............. 68................ See Notes 7 and 13 ......do.......... 100. ---------------------------------------------------------------------------------------------------------------- Note 1: Maximum filling density for liquefied gases is hereby defined as the percent ratio of the weight of gas in the tank to the weight of water that the tank will hold. For determining the water capacity of the tank in pounds, the weight of a gallon (231 cubic inches) of water at 60 deg.F. in air shall be 8.32828 pounds. Note 2: See Sec. 173.32 for authority to use other portable tanks and for manifolding cargo tanks, see paragraph (q) of this section. Specifications MC 330 cargo tanks may be painted as specified for MC 331 cargo tanks. Note 3: If cargo tanks and portable tank containers for carbon dioxide, refrigerated liquid and nitrous oxide, refrigerated liquid are designed to conform to the requirements of the ASME Code for Low Temperature Operation, the design pressure may be reduced to 100 p.s.i.g. or the controlled pressure, whichever is greater. [[Page 576]] Note 4: Material must be steel. Packagings must have a corrosion allowance of 20 percent or 0.10 inch, whichever is less, added to the metal thickness. The minimum wall thickness for chlorine packagings is 0.300 inch for stainless steel or 0.625 inch for carbon steel, including corrosion allowance. Note 5: Unlagged cargo tanks and portable tank containers for liquid anhydrous ammonia may be filled to 87.5 percent by volume provided the temperature of the anhydrous ammonia being loaded into such tanks is determined to be not lower than 30 deg.F. or provided the filling of such tanks is stopped at the first indication of frost or ice formation on the outside surface of the tank and is not resumed until such frost or ice has disappeared. Note 6: Tanks equipped with fusible plugs must be filled by weight. Note 7: Tanks must be filled by weight. Note 8: Chlorine packagings may be shipped only if the contents are to be unloaded at one unloading point. Note 9: This gas may be transported in authorized cargo tanks and portable tanks marked ``dispersant gas,'' or ``refrigerant gas.'' Note 10: [Reserved] Note 11: MC-330, MC-331 and MC-338 cargo tanks must be insulated. Cargo tanks must meet all the following requirements. Each tank must have a design service temperature of minus 100 deg.F., or no warmer than the boiling point at one atmosphere of the hazardous material to be shipped therein, whichever is colder, and must conform to the low-temperature requirements of the ASME Code. When the normal travel time is 24 hours or less, the tank's holding time as loaded must be at least twice the normal travel time. When the normal travel time exceeds 24 hours, the tank's holding time as loaded must be at least 24 hours greater than the normal travel time. The holding time is the elapsed time from loading until venting occurs under equilibrium conditions. The cargo tank must have an outer jacket made of steel when the cargo tank is used to transport a flammable gas. Note 12: No aluminum, copper, silver, zinc or an alloy of any of these metals shall be used in packaging construction where it comes into contact with the lading. Note 13: All parts of valves and safety devices in contact with contents of tank must be of a metal or other material suitably treated if necessary, which will not cause formation of any acetylides. Note 14: Specifications MC 330 and MC 331 cargo tanks constructed of other than quenched and tempered steel ``(NQT)'' are authorized for all grades of anhydrous ammonia. Specifications MC 330 and MC 331 cargo tanks constructed of quenched and tempered steel ``(QT)'' (see marking requirements of Sec. 172.328(c) of this subchapter) are authorized for anhydrous ammonia having a minimum water content of 0.2 percent by weight. Any tank being placed in anhydrous ammonia service or a tank which has been in other service or has been opened for inspection, test, or repair, must be cleaned of the previous product and must be purged of air before loading. See Sec. 172.203(h) of this subchapter for special shipping paper requirements. Note 15: Specifications MC 330 and MC 331 cargo tanks constructed of other than quenched and tempered steel (NQT) are authorized for all grades of liquefied petroleum gases. Only grades of liquefied petroleum gases determined to be ``noncorrosive'' are authorized in Specification MC 330 and MC 331 cargo tanks constructed of quenched and tempered steel (QT). ``Noncorrosive'' means the corrosiveness of the gas does not exceed the limitations for classification 1 of the ASTM Copper Strip Classifications when tested in accordance with ASTM D1838-64, ``Copper Strip Corrosion by Liquefied Petroleum (LP) Gases.'' (For (QT) and (NQT) marking requirements see Sec. 172.328(c) of this subchapter. For special shipping paper requirements, see Sec. 172.203(h) of this subchapter.) Note 16: Openings, inlets, and outlets on MC 330 and MC 331 cargo tanks must conform to Sec. 178.337-8(a) of this subchapter. MC 330 and MC 331 cargo tanks must be equipped with emergency discharge control equipment as specified in Sec. 178.337-11(a) of this subchapter. Note 17: A Specification MC-330 or MC-331 cargo tank or a nonspecification cargo tank meeting, and marked in conformance with, the edition of the ASME Code in effect when it was fabricated, may be used for the transportation of anhydrous ammonia if it: (1) Has a minimum design pressure not lower than 250 psig; (2) Was manufactured in conformance with the ASME Code prior to January 1, 1981, according to its ASME name plate and manufacturer's data report; (3) Is painted white or aluminum; (4) Complies with Note 12 of this paragraph; (5) Has been inspected and tested in accordance with subpart E of part 180 of this subchapter as specified for MC 331 cargo tanks. (6) Was used to transport anhydrous ammonia prior to January 1, 1981; (7) Is operated exclusively in intrastate commerce (including its operation by a motor carrier otherwise engaged in interstate commerce) in a state where its operation was permitted by the laws of that State (not including the incorporation of this subchapter) prior to January 1, 1981; and (8) Is operated in conformance with all other requirements of this subchapter. Note 18: The minimum packaging design pressure must not be less than the vapor pressure at the reference temperature of the lading plus one percent or 173.4 kPa (25 psig), whichever is less. Note 19: The minimum packaging design pressure must not be less than the vapor pressure at the reference temperature of the lading. Note 20: The minimum packaging design pressure must not be less than 1.5 times the vapor pressure of the lading at 46 deg.C (115 deg.F). Note 21: The minimum packaging design pressure must not be less than 1.3 times the vapor pressure of the lading at 46 deg.C (115 deg.F). Note 22: The minimum packaging design pressure must not be less than 1.1 times the vapor pressure of the lading at 46 deg.C (115 deg.F). Note 23: Packagings must be made of stainless steel except that steel other than stainless steel may be used in accordance with the provisions of Sec. 173.24b(b) of this part. Thickness of stainless steel for shell and heads must be the greater of 7.62 mm (0.300 inch) or the thickness required for the packaging at its minimum design pressure. Note 24: Packagings must be made of stainless steel except that steel other than stainless steel may be used in accordance with the provisions of Sec. 173.24b(b) of this part. Thickness of stainless steel for shell and heads must be the greater of 6.35 mm (0.250 inch) or the thickness required for the packaging at its minimum design pressure. For sulphur dioxide, this Note does not apply until October 1, 1994. Note 25: Packagings must be made of stainless steel except that steel other than stainless steel may be used in accordance with the provisions of Sec. 173.24b(b) of this part. Thickness for shell and heads must be as calculated for the packaging at its minimum design pressure. Note 26: Non-specification cargo tanks may be used for the transportation of liquefied petroleum gas, subject to the conditions prescribed in paragraph (k) of this section. [[Page 577]] (b) Maximum permitted filling densities for cargo and portable tank containers for transportation of butadiene, stabilized, and liquefied petroleum gas are as follows: ------------------------------------------------------------------------ Maximum permitted filling density in percent of the water- weight capacity of the Maximum specific gravity of the liquid material tanks (percent) See at 60 deg.F. Note 1 ----------------------- 1200 gallons or Over 1200 less gallons ------------------------------------------------------------------------ 0.473 to 0.480.................................. 38 41 0.481 to 0.488.................................. 39 42 0.489 to 0.495.................................. 40 43 0.496 to 0.503.................................. 41 44 0.504 to 0.510.................................. 42 45 0.511 to 0.519.................................. 43 46 0.520 to 0.527.................................. 44 47 0.528 to 0.536.................................. 45 48 0.537 to 0.544.................................. 46 49 0.545 to 0.552.................................. 47 50 0.553 to 0.560.................................. 48 51 0.561 to 0.568.................................. 49 52 0.569 to 0.576.................................. 50 53 0.577 to 0.584.................................. 51 54 0.585 to 0.592.................................. 52 55 0.593 to 0.600.................................. 53 56 0.601 to 0.608.................................. 54 57 0.609 to 0.617.................................. 55 58 0.618 to 0.626.................................. 56 59 0.627 and over.................................. 57 60 ------------------------------------------------------------------------ Note 1: Filling is permitted by volume provided the same filling density is used as permitted by weight, except when using fixed length dip tube or other fixed maximum liquid level indicators (paragraph (f) of this section), in which case the maximum permitted filling density shall not exceed 97 percent of the maximum permitted filling density by weight contained in the table. (1) Odorization. All liquefied petroleum gas shall be effectively odorized as required in Note 2 of this paragraph to indicate positively, by a distinctive odor, the presence of gas down to a concentration in air of not over one-fifth the lower limit of combustibility: Provided, however, That odorization is not required if harmful in the use or further processing of the liquefied petroleum gas, or if odorization will serve no useful purpose as a warning agent in such use or further processing. Note 1: The lower limits of combustibility of the more commonly used liquefied petroleum gases are: Propane, 2.15 percent; butane, 1.55 percent. These figures represent volumetric percentages of gas-air mixtures in each case. Note 2: The use of 1.0 pound of ethyl mercaptan, 1.0 pound of thiophane, or 1.4 pounds of amyl mercaptan per 10,000 gallons of liquefied petroleum gas shall be considered sufficient to meet the requirements of Sec. 173.315(b)(1). This note does not exclude the use of any other odorant in sufficient quantity to meet the requirements of Sec. 173.315(b)(1). (c) Except as otherwise provided, the loading of a liquefied gas into a cargo tank or portable tank shall be determined by weight or by a suitable liquid level gauging device. The vapor pressure (psig) at 115 deg.F. must not exceed the design pressure of the cargo tank or portable tank container. The outage and filling limits for liquefied gases must be as prescribed in Sec. 173.24b of this part, except that this requirement does not apply to: (1) A tank containing carbon dioxide, refrigerated liquid or nitrous oxide, refrigerated liquid. Such tank is required to be equipped with suitable pressure control valves and may not be filled to a level exceeding 95 percent of the volumetric capacity of the tank. (2) A tank containing ethane, refrigerated liquid; ethane-propane mixture, refrigerated liquid; or hydrogen chloride, refrigerated liquid. Such tank must be filled to allow at least two percent outage below the inlet of the pressure relief valve or pressure control valve under conditions of incipient opening, with the tank in a level attitude. (d) If the loading of cargo tanks and portable tank containers with liquefied gases is to be determined by weight, the gross weight shall be checked after the filling line is disconnected in each instance. The gross weight shall be calculated from the tank capacity and tare weight set forth on the metal plate required by the specification, and the maximum filling density permitted for the material being loaded into the tank as set forth in the table, paragraph (a) of this section. (e) If the loading of cargo tanks and portable tank containers with liquefied gases is to be determined by adjustable liquid level device, each tank and each compartment thereof shall have a thermometer well, so that the internal liquid temperature can easily be determined, and the amount of liquid in the tank shall be corrected to a 60 deg.F. basis. Liquid levels shall not exceed a level corresponding to the maximum filling density permitted for the material being loaded into the tank as set forth in the table in paragraph (a) of this section. [[Page 578]] (f) When the loading of cargo tanks and portable tank containers with liquefied gases is determined only by fixed length dip tube or other fixed maximum liquid level indicator, the device shall be arranged to function at a level not to exceed the maximum permitted volume prescribed by the table, paragraph (a) of this section. Loading shall be stopped when the device functions. (g) Containers, the liquid level of which has been determined by means of a fixed length dip tube gauging device, shall not be acceptable for stowage as cargo on vessels in commerce subject to the jurisdiction of the United States Coast Guard. Nothing contained in this section shall be so construed as to prohibit the transportation on car floats or car ferries of motor vehicles laden with containers nor cargo tanks the liquid level of either of which has been determined by means of fixed length dip tube devices. (h) Each cargo tank and portable tank, except a tank filled by weight, must be equipped with one or more of the gauging devices described in the following table which indicate accurately the maximum permitted liquid level. Additional gauging devices may be installed but may not be used as primary controls for filling of cargo tanks and portable tanks. Gauge glasses are not permitted on any cargo tank or portable tank. Primary gauging devices used on cargo tanks of less than 3500 gallons water capacity are exempt from the longitudinal location requirements specified in paragraphs (h)(2) and (3) of this section provided: The tank length does not exceed three times the tank diameter; and the cargo tank is unloaded within 24 hours after each filling of the tank. ------------------------------------------------------------------------ Gaging device permitted for Kind of gas filling purposes ------------------------------------------------------------------------ Anhydrous ammonia......................... Rotary tube; adjustable slip tube; fixed length dip tube. Anhydrous dimethylamine................... None. Anhydrous monomethylamine................. Do. Anhydrous trimethylamine.................. Do. Aqua ammonia solution containing anhydrous Rotary tube; adjustable slip ammonia. tube; fixed length dip tube. Butadiene, stabilized..................... Do. Carbon dioxide, refrigerated liquid....... Do. Chlorine.................................. None. Dichlorodifluoromethane................... Do. Difluoroethane............................ Do. Difluoromonochloroethane.................. Do. Dimethyl ether............................ Do. Ethane, refrigerated liquid............... Rotary tube; adjustable slip tube; fixed length dip tube. Ethane-propane mixture, refrigerated Do. liquid. Hexafluoropropylene....................... None. Hydrogen chloride, refrigerated liquid.... Do. Liquefied petroleum gases................. Rotary tube; adjustable slip tube; fixed length dip tube. Methyl chloride........................... Fixed length dip tube. Methyl mercaptan.......................... Rotary tube; adjustable slip tube; fixed length dip tube. Monochlorodifluoromethane................. None. Nitrous oxide, refrigerated liquid........ Rotary tube; adjustable slip tube; fixed length dip tube. Methylacetylenepropadiene, stabilized..... Do. Refrigerant gas, n.o.s. or Dispersant gas, None. n.o.s. Sulfur dioxide............................ Fixed length dip tube. Vinyl chloride............................ None. Vinyl fluoride, inhibited................. Do. ------------------------------------------------------------------------ (1) The design pressure of the liquid level gauging devices shall be at least equal to the design pressure of the tank. (2) If the primary gauging device is adjustable, it must be capable of adjustment so that the end of the tube will be in the location specified in paragraph (h)(3) of this section for at least one of the ladings to be transported, at the filling level corresponding to an average loading temperature. Exterior means must be provided to indicate this adjustment. The gauging device must be legibly and permanently marked in increments not exceeding 20 Fahrenheit degrees (or not exceeding 25 p.s.i.g. on tanks for carbon dioxide, refrigerated liquid or nitrous oxide, refrigerated liquid), to indicate the maximum levels to which the tank may be filled with liquid at temperatures above 20 deg.F. However, if it is not practicable to so mark the gauging device, this information must be legibly and permanently marked on a plate affixed to the tank adjacent to the gauging device. (3) A dip tube gauging device consists of a pipe or tube with a valve at its outer end with its intake limited by an orifice not larger than 0.060 inch in diameter. If a fixed length dip tube is [[Page 579]] used, the intake must be located midway of the tank both longitudinally and laterally and at maximum permitted filling level. In tanks for liquefied petroleum gases, the intake must be located at the level reached by the lading when the tank is loaded to maximum filling density at 40 deg.F. (4) Except on a tank used exclusively for the transportation of carbon dioxide, refrigerated liquid or nitrous oxide, refrigerated liquid, each opening for a pressure gauge must be restricted at or inside the tank by an orifice no larger than 0.060 inch in diameter. For carbon dioxide, refrigerated liquid or nitrous oxide, refrigerated liquid service, the pressure gauge need only be used during the filling operation. (i) Each tank must be provided with one or more pressure relief devices which, unless otherwise specified in this part, must be of the spring-loaded type. Each valve must be arranged to discharge upward and unobstructed to the outside of the protective housing to prevent any impingement of escaping gas upon the tank. For each chlorine tank the protective housing must be in compliance with the requirements set forth in the applicable specification. (1) The safety relief valves on each tank must meet the following conditions: (i) The total relieving capacity, as determined by the flow formulas contained in Section 5 of CGA Pamphlet S-1.2, must be sufficient to prevent a maximum pressure in the tank of more than 120 percent of the design pressure; (ii) The flow capacity rating, testing and marking must be in accordance with Sections 5, 6 and 7 of CGA Pamphlet S-1.2. (iii) For an insulated tank, the required relieving capacity of the relief devices must be the same as for an uninsulated tank, unless the insulation will remain in place and will be effective under fire conditions. In this case, except for UN portable tanks, each insulated tank must be covered by a sheet metal jacket of not less than 16 gauge thickness. For UN portable tanks where the relieving capacity of the valves has been reduced on the basis of the insulation system, the insulation system must remain effective at all temperatures less than 649 deg.C (1200.2 deg.F) and be jacketed with a material having a melting point of 700 deg.C (1292.0 deg.F) or greater. (iv) An MC 330 cargo tank that has relief valves sized by Fetterly's formula dated November 27, 1928, may be continued in service. (2) Each safety relief valve must be arranged to minimize the possibility of tampering. If the pressure setting or adjustment is external to the valve, the safety relief valve must be provided with means for sealing the adjustment and it must be sealed. (3) Each safety relief valve on a portable tank, other than a UN portable tank, must be set to start-to-discharge at pressure no higher than 110% of the tank design pressure and no lower than the design pressure specified in paragraph (a) of this section for the gas transported. For UN portable tanks used for liquefied compressed gases and constructed in accordance with the requirements of Sec. 178.276 of this subchapter, the pressure relief device(s) must conform to Sec. 178.276(e) of this subchapter. (4) Except for UN portable tanks, each safety relief valve must be plainly and permanently marked with the pressure in p.s.i.g. at which it is set to discharge, with the actual rate of discharge of the device in cubic feet per minute of the gas or of air at 60 deg.F (15.6 deg.C) and 14.7 p.s.i.a., and with the manufacturer's name or trade name and catalog number. The start-to-discharge valve marking must be visible after the valve is installed. The rated discharge capacity of the device must be determined at a pressure of 120% of the design pressure of the tank. For UN portable tanks, each pressure relief device must be clearly and permanently marked as specified in Sec. 178.274(f)(1) of this subchapter. (5) Each safety relief valve must have direct communication with the vapor space in the tank. (6) Each connection to a safety relief valve must be of sufficient size to provide the required rate of discharge through the safety relief valve. (7) [RESERVED] (9) On tanks for carbon dioxide, refrigerated liquid or nitrous oxide, refrigerated liquid each safety relief device must be installed and located so [[Page 580]] that the cooling effect of the contents will not prevent the effective operation of the device. In addition to the required safety relief valves, these tanks may be equipped with one or more pressure controlling devices. (10) Each tank for carbon dioxide, refrigerated liquid also may be equipped with one or more non-reclosing pressure relief devices set to function at a pressure not over two times nor less than 1.5 times the design pressure of the tank. (11) Each portion of connected liquid piping or hose that can be closed at both ends must be provided with a safety relief valve without an intervening shut-off valve to prevent excessive hydrostatic pressure that could burst the piping or hose. (12) Subject to conditions of paragraph (a) of this section for the methyl chloride and sulfur dioxide optional portable tanks, one or more fusible plugs examined by the Bureau of Explosives and approved by the Associate Administrator may be used on these tanks in place of safety relief valves of the spring-loaded type. The fusible plug or plugs must be in accordance with CGA Pamphlet S-1.2, to prevent a pressure rise in the tank of more than 120 percent of the design pressure. If the tank is over 30 inches long, each end must have the total specified safety discharge area. (13) A safety relief valve on a chlorine cargo tank must conform to one of the following standards of The Chlorine Institute, Inc.: Type 1\1/2\ JQ225, Dwg. H51970, dated October 7, 1968; or Type 1\1/2\ JQ225, Dwg. H50155, Revision A, dated April 28, 1969. (j) Storage containers for liquefied petroleum gas for permanent installation on consumer premises may be shipped by private motor carrier only under the following conditions: (1) Each container must be constructed in compliance with the requirements of the ASME Code (containers built in compliance with earlier editions starting with 1943 are authorized) and must be marked to indicate compliance in the manner specified by the respective Code. (2) Each container must be equipped with safety devices in compliance with the requirements for safety devices on containers as specified in NFPA Pamphlet No. 58. (3) The containers shall be so braced or otherwise secured on the vehicle as to prevent relative motion while in transit. Valves or other fittings shall be adequately protected against damage during transportation. (See Sec. 177.834(g) of this subchapter.) (4) Except as provided in paragraph (j)(5) of this section, containers shall not be shipped when charged with liquefied petroleum gas to more than 5 percent of their water capacity. (5) Storage containers of less than 1,042 pounds water capacity (125 gallons) may be shipped when charged with liquefied petroleum gas in compliance with DOT filling density. (k) A nonspecification cargo tank meeting, and marked in conformance with, the edition of the ASME Code in effect when it was fabricated may be used for the transportation of liquefied petroleum gas provided it meets all of the following conditions: (1) It must have a minimum design pressure no lower than 250 psig. (2) It must have a capacity of 13,247.5 L (3,500 water gallons) or less. (3) It must have been manufactured in conformance with the ASME Code prior to January 1, 1981, according to its ASME name plate and manufacturer's data report. (4) It must conform to applicable provisions of NFPA Pamphlet 58, except to the extent that provisions of Pamphlet 58 are inconsistent with requirements in parts 178 and 180 of this subchapter. (5) It must be inspected, tested, and equipped in accordance with subpart E of part 180 of this subchapter as specified for MC 331 cargo tank motor vehicles. (6) Except as provided in this paragraph (k), it must be operated exclusively in intrastate commerce, including its operation by a motor carrier otherwise engaged in interstate commerce, in a state where its operation was permitted by law (not including the incorporation of this subchapter) prior to January 1, 1981. A cargo tank motor vehicle operating under authority of this section may cross state lines to travel to and from a qualified assembly, repair, maintenance, or requalification facility. The cargo tank need [[Page 581]] not be cleaned and purged, but it may not contain liquefied petroleum gas in excess of five percent of the water capacity of the cargo tank. If the vehicle engine is supplied fuel from the cargo tank, enough fuel in excess of five percent of the cargo tank's water capacity may be carried for the trip to or from the facility. (7) It must have been used to transport liquefied petroleum gas prior to January 1, 1981. (8) It must be operated in conformance with all other requirements of this subchapter. (l) Anhydrous ammonia must not be offered for transportation or transported in specification MC 330 and MC 331 cargo tanks constructed of quenched and tempered (``QT'') steel except as provided in this paragraph. (1) The ammonia must have a minimum water content of 0.2 percent by weight. Any addition of water must be made using steam condensate, deionized, or distilled water. (2) Except as otherwise provided in this paragraph, each person offering for transportation or transporting anhydrous ammonia shall perform a periodic analysis for prescribed water content in the ammonia. The analysis must be performed: (i) From a sample of the ammonia in storage taken at least once every 7 days, or each time ammonia is added to the storage tanks, whichever is less frequent; or (ii) At the time the cargo tanks are loaded, then a sample of the ammonia taken from at least one loaded cargo tank out of each 10 loads, or from one cargo tank every 24 hours, whichever is less frequent; or (iii) At the same frequency as described in paragraph (l)(2)(ii) of this section, from a sample taken from the loading line to the cargo tank. (3) If water is added at the time of loading: (i) The sample for analysis must be taken from a point in the loading line between the water injection equipment and the cargo tank; and (ii) Positive provisions must be made to assure water injection equipment is operating. (4) If water injection equipment becomes inoperative, suitable corrective maintenance must be performed after which a sample from the first loaded cargo tank must be analyzed for prescribed water content. (5) The analysis method for water content must be as prescribed in CGA Pamphlet G-2.2, titled ``Tentative Standard Method for Determining Minimum of 0.2 per cent water in Anhydrous Ammonia,'' 1975 edition. (6) Records indicating the results of the analysis taken, as required by this paragraph, must be retained for 2 years and must be open to inspection by a representative of the Department. (7) Each person receiving anhydrous ammonia containing 0.2 per cent water by weight may offer for transportation or transport that ammonia without performing the prescribed analysis for water content provided: (i) The ammonia received was certified as containing 0.2 percent water as prescribed in Secs. 172.203(h)(l)(i) and 177.817(a) of this subchapter; and (ii) The amount of water in the ammonia has not been reduced by any means. (m) A cargo tank (commonly known as a nurse tank and considered an implement of husbandry) transporting anhydrous ammonia, and operated by a private carrier exclusively for agricultural purposes does not have to meet the specification requirements of part 178 of this subchapter if it: (1) Has a minimum design pressure of 250 psig and meets the requirements of the edition of the ASME code in effect at the time it was manufactured and is marked accordingly; (2) Is equipped with safety relief valves meeting the requirements of CGA pamphlet S1.2; (3) Is painted white or aluminum; (4) Has capacity of 3,000 gallons or less; (5) Is loaded to a filling density no greater than 56 percent; (6) Is securely mounted on a farm wagon; and (7) Is in conformance with the requirements of part 172 of this subchapter except that shipping papers are not required; and it need not be marked or placarded on one end if that end contains valves, fittings, regulators or gauges when those appurtenances prevent the markings and [[Page 582]] placard from being properly placed and visible. (n) Emergency discharge control for cargo tank motor vehicles in liquefied compressed gas service.--(1) Required emergency discharge control equipment. Each cargo tank motor vehicle in liquefied compressed gas service must have an emergency discharge control capability as specified in the following table: [[Page 583]] -------------------------------------------------------------------------------------------------------------------------------------------------------- Required emergency discharge control Sec. 173.315(n)(1)(*) Material Delivery service capability -------------------------------------------------------------------------------------------------------------------------------------------------------- (i)............................. Division 2.2 materials with no subsidiary All..................... None. hazard, excluding anhydrous ammonia. -------------------------------------------------------------------------------------------------------------------------------------------------------- (ii)............................ Division 2.3 materials....................... All..................... Paragraph (n)(2) of this section. -------------------------------------------------------------------------------------------------------------------------------------------------------- (iii)........................... Division 2.2 materials with a subsidiary Other than metered Paragraph (n)(2) of this section. hazard, Division 2.1 materials, and delivery service. anhydrous ammonia. -------------------------------------------------------------------------------------------------------------------------------------------------------- (iv)............................ Division 2.2 materials with a subsidiary Metered delivery service Paragraph (n)(3) of this section. hazard, Division 2.1 materials, and anhydrous ammonia in a cargo tank motor vehicle with a capacity of 13,247.5 L (3,500 water gallons) or less. -------------------------------------------------------------------------------------------------------------------------------------------------------- (v)............................. Division 2.2 materials with a subsidiary Metered delivery service Paragraph (n)(3) of this section, and, for hazard, Division 2.1 materials, and obstructed view deliveries where permitted anhydrous ammonia in a cargo tank motor by Sec. 177.840(p) of this subchapter, vehicle with a capacity greater than paragraph (n)(2) or (n)(4) of this section. 13,247.5 L (3,500 water gallons). -------------------------------------------------------------------------------------------------------------------------------------------------------- [[Page 584]] (2) Cargo tank motor vehicles in other than metered delivery service. A cargo tank motor vehicle in other than metered delivery service must have a means to automatically shut off the flow of product without the need for human intervention within 20 seconds of an unintentional release caused by a complete separation of a liquid delivery hose (passive shut-down capability). (i) Designed flow of product through a bypass in the valve is acceptable when authorized by this subchapter. (ii) The design for the means to automatically shut off product flow must be certified by a Design Certifying Engineer. The certification must consider any specifications of the original component manufacturer and must explain how the passive means to shut off the flow of product operates. It must also outline the parameters (e.g., temperature, pressure, types of product) within which the passive means to shut off the flow of product is designed to operate. All components of the discharge system that are integral to the design must be included in the certification. A copy of the design certification must be provided to the owner of the cargo tank motor vehicle on which the equipment will be installed. (iii) Installation must be performed under the supervision of a Registered Inspector unless the equipment is installed and removed as part of regular operation (e.g., a hose). The Registered Inspector must certify that the equipment is installed and tested, if it is possible to do so without damaging the equipment, in accordance with the Design Certifying Engineer's certification. The Registered Inspector must provide the certification to the owner of the cargo tank motor vehicle. (3) Cargo tank motor vehicles in metered delivery service. When required by the table in paragraph (n)(1) of this section, a cargo tank motor vehicle must have an off-truck remote means to close the internal self-closing stop valve and shut off all motive and auxiliary power equipment upon activation by a qualified person attending the unloading of the cargo tank motor vehicle (off-truck remote shut-off). It must function reliably at a distance of 45.72 m (150 feet). The off-truck remote shut-off activation device must not be capable of reopening the internal self-closing stop valve after emergency activation. (i) The emergency discharge control equipment must be installed under the supervision of a Registered Inspector. Each wireless transmitter/receiver must be tested to demonstrate that it will close the internal self-closing stop valve and shut off all motive and auxiliary power equipment at a distance of 91.44 m (300 feet) under optimum conditions. Emergency discharge control equipment that does not employ a wireless transmitter/receiver must be tested to demonstrate its functioning at the maximum length of the delivery hose. (ii) The Registered Inspector must certify that the remote control equipment is installed in accordance with the original component manufacturer's specifications and is tested in accordance with paragraph (n)(3)(i) of this section. The Registered Inspector must provide the owner of the cargo tank motor vehicle with this certification. (4) Query systems. When a transmitter/receiver system is used to satisfy the requirements of paragraph (n)(1)(v) of this section, it must close the internal self-closing stop valve and shut off all motive and auxiliary power equipment unless the qualified person attending the unloading operation prevents it from doing so at least once every five minutes. Testing and certification must be as specified in paragraph (n)(3) of this section. (5) Compliance dates. (i) Each specification MC 331 cargo tank motor vehicle with a certificate of construction issued two or more years after July 1, 1999, must have an appropriate emergency discharge control capability as specified in this paragraph (n). (ii) No MC 330, MC 331, or nonspecification cargo tank motor vehicle authorized under paragraph (k) of this section may be operated unless it has an appropriate emergency discharge control capability as specified in this paragraph (n) no later than the date of its first scheduled pressure retest required after July 1, 2001. No MC 330, MC 331 or nonspecification cargo tank [[Page 585]] motor vehicle authorized under paragraph (k) of this section may be operated after July 1, 2006, unless it has been equipped with emergency discharge control equipment as specified in this paragraph (n). (iii) No MC 330 or MC 331 cargo tank motor vehicle with a capacity over 13,247 L (3,500 gallons) used in metered delivery service may be operated unless it has an appropriate discharge control capability as specified in this paragraph (n) no later than July 1, 2003, or the date of its first scheduled pressure retest required after July 1, 2001, whichever is earlier. (o) Chlorine cargo tank motor vehicles. Each cargo tank motor vehicle used for the transportation of chlorine must meet the requirements in the following: (1) Any hose, piping, or tubing used for loading or unloading that is mounted or carried on the motor vehicle may not be attached to any valve and must be capped at all ends to prevent the entry of moisture, except at the time of loading or unloading. Except at the time of loading and unloading, the pipe connection of each angle valve must be closed with a screw plug which is chained or otherwise fastened to prevent misplacement. (2) Each chlorine cargo tank motor vehicle angle valve must be tested to be leak free at not less than 225 psig using dry air or inert gas before installation and thereafter every 2 years when performing the required periodic retest in Sec. 180.407(c) of this subchapter. Prior to each loading, the cargo tank motor vehicle must be inspected and the angle valves and gasketed joints must be examined and tested at a pressure of not less than 50 psig to determine that they are not leaking and are in proper condition for transportation. Any leaks must be corrected before the cargo tank motor vehicle is offered for transportation. (3) Excess flow valves on the cargo tank motor vehicle must meet the requirements of paragraph (n) of this section. (p) Fusible elements. Each MC 330, MC 331, or nonspecification cargo tank authorized under paragraph (k) of this section must have a thermal means of closure for each internal self-closing stop valve as specified in Sec. 178.337-8(a)(4) of this subchapter. (q) Manifolding is authorized for cargo tanks containing anhydrous ammonia provided each individual cargo tank is equipped with a pressure relief device or valves and gauging devices as required by paragraphs (h) and (i) of this section. Each valve must be tightly closed while the cargo tank is in transit. Each cargo tank must be filled separately. [29 FR 18743, Dec. 29, 1964. Redesignated at 32 FR 5606, Apr. 5, 1967] Editorial Note: For Federal Register citations affecting Sec. 173.315, see the List of CFR Sections Affected which appears in the Finding Aids section of the printed volume and on GPO Access.