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NIOSH Manual of Analytical Methods (NMAM)

 

Protocols for Method Evaluation

  • General Laboratory Protocol
    NIOSH has a general protocol for evaluating methods of laboratory analysis:

    Kennedy, E.R.; Fischbach, T.J.; Song, R; Eller, P.M.; Shulman, S.A.: "Guidelines for Air Sampling and Analytical Method Development and Evaluation" DHHS(NIOSH) Publication No. 95-117.

    Downloadable software is available that assists with understanding the tests and calculating the results.

  • Diffusive Samplers- for routine evaluation of many samplers and analytes, the following are equivalent:

    • ASTM: Standard Practice for Evaluating the Performance of Diffusive Samplers, American Society for Testing and Materials (ASTM), D 6246, 1998. Order at www.astm.org.
    • ISO: Workplace Atmospheres - Protocol for Evaluating the Performance of Diffusive Samplers, International Organization for Standardization (ISO), ISO/FDIS 16107, 1999. Order at www.iso.ch.

  • Diffusive Samplers - for more detailed sampler design:
    Cassinelli, M.E.; Hull, R.D.; Crable, J.; Teass, A.: Protocol for the Evaluation of Passive Monitors, in Diffusive Sampling, Royal Society of Chemistry, London, England, pp. 190 - 202, 1987.
NIOSH Manual of Analytical Methods (NMAM®), 4th ed.
DHHS (NIOSH) Publication 94-113 (August, 1994),
1st Supplement Publication 96-135, 2nd Supplement Publication 98-119,
3rd Supplement 2003-154
Schlecht, P.C. & O'Connor, P.F. (pfo1@cdc.gov), Eds.
NMAM

NIOSH Manual of Analytical Methods