USGS OFR-02-94 Table 4, Method 3

Table 4. Stream sampling sites analyzed for selected human pharmaceutical compounds (Method 3) in 1999 and 2000
[All concentrations are in micrograms per liter. <, less than indicated detected limit; E, estimated; --, data not collected; Number in parentheses () is the Chemical Abstracts Service Registry Number]

Site code	Date (month-day-year)	Time (24-hour)	Type of sample	Acetaminophen (103-90-2)	Caffeine (58-08-2)	Cimetidine (51481-61-9)	Codeine (76-57-3)	Cotinine (486-56-6)	Dehydronifedipine (67035-22-7)	Digoxigenin (1672-46-4)	Digoxin (20830-75-5)	Diltiazem (42399-41-7)	1,7-Dimethylxanthine (611-59-6)
AR02	05-02-99	1630	regular	--	--	--	--	--	--	--	--	--	--
AR06	05-04-99	2050	do.	--	--	--	--	--	--	--	--	--	--
AZ01	06-29-00	1115	do.	<0.009	3.3	0.016	<.024	0.099	<.01	<0.008	<.26	<.012	0.84
AZ02	06-27-00	1625	do.	.50	1.2	<.007	<.024	.30	.013	<.008	<.26	.037	1.4
AZ03	06-29-00	0710	do.	.048	3.1	.58	<.024	.69	E.003	<.008	<.26	.034	1.8
AZ04	06-27-00	1035	do.	<.009	<.014	<.007	<.024	E.003	<.01	<.008	<.26	.012	.032
CA01	05-18-00	1130	do.	.025	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
CA02	06-28-00	1300	do.	.39	.68	<.007	E.019	<.023	<.01	<.008	<.26	.017	.21
CA03	08-16-00	1700	do.	<.009	.022	<.007	<.024	.071	<.01	<.008	<.26	<.012	<.018
CA04	08-09-00	1700	do.	<.009	<.014	<.007	<.024	<.023	.012	<.008	<.26	<.012	<.018
CA05	04-15-99	1700	do.	<.009	.11	.12	--	.048	.030	<.008	--	<.012	<.018
CA06	04-11-99	0715	do.	--	--	--	--	--	--	--	--	--	--
CA07	09-21-99	1110	do.	<.009	<.014	<.007	--	<.023	<.01	<.008	--	<.012	<.018
CA08	09-21-99	1600	do.	E.004	<.014	<.007	--	<.023	<.01	<.008	--	<.012	<.018
CA09	09-22-99	1120	do.	E.004	<.014	<.007	--	<.023	<.01	<.008	--	<.012	<.018
CA10	09-22-99	1320	do.	<.009	<.014	<.007	--	<.023	<.01	<.008	--	<.012	<.018
CO01	04-21-99	1250	do.	<.009	<.014	<.007	--	.90	<.01	<.008	--	.049	.053
DE01	05-23-99	1130	do.	--	--	--	--	--	--	--	--	--	--
DE01	05-23-99	1140	duplicate	--	--	--	--	--	--	--	--	--	--
FL01	08-28-00	1215	regular	<.009	.053	<.007	<.024	<.023	<.01	<.008	<.26	<.012	.067
FL02	08-23-00	1215	do.	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
GA01	05-26-99	1400	do.	--	--	--	--	--	--	--	--	--	--
GA02	05-25-99	1130	do.	--	--	--	--	--	--	--	--	--	--
GA03	05-25-99	1030	do.	--	--	--	--	--	--	--	--	--	--
GA04	05-25-99	0840	do.	--	--	--	--	--	--	--	--	--	--
GA05	05-26-99	1130	do.	<.009	.049	<.007	--	E.014	<.01	<.008	--	<.012	<.018
GA06	05-24-99	1215	do.	--	--	--	--	--	--	--	--	--	--
GA07	05-24-99	1420	do.	<.009	E.001	<.007	--	<.023	E.001	<.008	--	E.014	<.018
IA01	09-13-00	1600	do.	<.009	.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
IA02	09-12-00	1200	do.	<.009	.025	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
IA04	09-11-00	1700	do.	<.009	.14	.51	<.024	.024	<.01	<.008	<.26	<.012	.27
IA05	04-05-99	1445	do.	--	--	--	--	--	--	--	--	--	--
IA07	04-08-99	1000	do.	.018	.07	<.007	--	<.023	<.01	<.008	--	<.012	<.018
IA08	04-06-99	0935	do.	--	--	--	--	--	--	--	--	--	--
IA09	04-06-99	1245	do.	--	--	--	--	--	--	--	--	--	--
IA10	04-04-99	2000	do.	--	--	--	--	--	--	--	--	--	--
IA11	04-03-99	1855	do.	--	--	--	--	--	--	--	--	--	--
IA12	04-03-99	1245	do.	--	--	--	--	--	--	--	--	--	--
ID01	08-14-00	1110	do.	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
ID02	08-15-00	1250	do.	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
ID03	08-16-00	1222	do.	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
ID04	05-17-00	1215	do.	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
IL01	05-13-99	1300	do.	<.009	.086	<.007	--	<.023	<.01	<.008	--	<.012	<.018
IL02	05-17-99	1420	do.	--	--	--	--	--	--	--	--	--	--
IL03	05-19-99	1400	do.	<.009	.22	<.007	--	.048	<.01	<.008	--	<.012	<.018
IL04	05-19-99	1240	do.	<.009	.12	<.007	--	.026	<.01	<.008	--	<.012	<.018
IL05	05-20-99	0810	do.	<.009	.056	.053	--	<.023	E.011	<.008	--	E.023	<.018
IL06	05-17-99	1230	do.	--	--	--	--	--	--	--	--	--	--
IL07	05-13-99	1710	do.	--	--	--	--	--	--	--	--	--	--
LA01	04-19-99	1130	do.	<.009	.068	<.007	--	<.023	<.01	<.008	--	<.012	<.018
MA01	05-12-99	0840	do.	<.009	.16	<.007	--	E.011	<.01	<.008	--	<.012	<.018
MA02	07-25-00	0630	do.	<.009	.13	<.007	<.024	E.003	<.01	<.008	<.26	<.012	E.017
MA03	07-25-00	0750	blank	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
MA03	07-25-00	0800	regular	<.009	.085	<.007	<.024	E.018	<.01	<.008	<.26	<.012	<.018
MA03	07-25-00	0810	duplicate	E.007	.067	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
MA04	07-25-00	0900	regular	.40	.74	E.004	<.024	.15	<.01	<.008	<.26	<.012	3.1
MA05	07-25-00	1100	do.	.010	.69	<.007	<.024	E.006	<.01	<.008	<.26	<.012	.26
MA06	07-25-00	1010	do.	.94	2.1	<.007	<.024	.031	<.01	<.008	<.26	E.011	.60
MA07	07-25-00	1130	do.	<.009	.048	<.007	<.024	E.021	<.01	<.008	<.26	<.012	.057
MD01	09-17-99	0930	do.	--	--	--	--	--	--	--	--	--	--
MD02	05-19-99	1710	do.	--	--	--	--	--	--	--	--	--	--
MI01	06-15-99	1030	do.	--	--	--	--	--	--	--	--	--	--
MI02	06-15-99	1430	do.	--	--	--	--	--	--	--	--	--	--
MI03	06-16-99	1045	do.	<.009	<.014	E.012	--	<.023	<.01	<.008	--	<.012	<.018
MN03	10-03-00	1105	blank	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
MN03	10-03-00	1115	do.	<.009	E.002	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
MN04	07-13-99	1300	do.	<.009	E.009	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
MO01	05-06-99	1130	do.	<.009	.75	<.007	--	E.016	<.01	<.008	--	<.012	.097
MO02	04-29-99	1245	do.	10	E6.0	<.007	--	.22	<.01	<.008	--	<.012	1.9
MO03	04-30-99	0830	do.	.24	.68	<.007	<.024	<.023	<.01	<.008	<.26	<.012	.29
MO04	04-30-99	1300	do.	.54	.24	<.007	<.024	<.023	<.01	<.008	<.26	<.012	.13
MO05	05-15-99	1315	do.	<.009	<.014	<.007	--	<.023	<.01	<.008	--	<.012	<.018
MO06	04-07-99	0845	do.	--	--	--	--	--	--	--	--	--	--
MO07	04-05-99	1530	do.	--	--	--	--	--	--	--	--	--	--
MO08	04-07-99	0840	do.	<.009	.079	<.007	--	E.02	E.005	<.008	--	<.012	<.018
MT01	03-16-00	1040	do.	<.009	<.014	<.007	--	<.023	<.01	<.008	--	<.012	<.018
MT02	03-16-00	1400	do.	<.009	<.014	<.007	--	<.023	<.01	<.008	--	<.012	<.018
MT03	03-17-00	1100	do.	<.009	<.014	<.007	--	<.023	<.01	<.008	--	<.012	.061
MT04	03-06-00	1400	do.	<.009	.057	<.007	--	<.023	<.01	<.008	--	<.012	<.018
MT05	03-22-00	1130	do.	<.009	<.014	<.007	--	<.023	<.01	<.008	--	<.012	<.018
NC01	05-06-99	1015	do.	--	--	--	--	--	--	--	--	--	--
NC02	05-06-99	1230	do.	--	--	--	--	--	--	--	--	--	--
NC03	05-06-99	1430	do.	--	--	--	--	--	--	--	--	--	--
NC04	05-06-99	1545	do.	--	--	--	--	--	--	--	--	--	--
NC05	05-13-99	1245	do.	--	--	--	--	--	--	--	--	--	--
NE01	06-24-99	1330	do.	--	--	--	--	--	--	--	--	--	--
NE02	06-15-99	1730	do.	--	--	--	--	--	--	--	--	--	--
NE03	06-14-99	1600	do.	--	--	--	--	--	--	--	--	--	--
NE04	06-15-99	1700	do.	--	--	--	--	--	--	--	--	--	--
NE05	06-03-99	1230	do.	--	--	--	--	--	--	--	--	--	--
NE06	06-04-99	1030	do.	--	--	--	--	--	--	--	--	--	--
NE07	06-17-99	1130	do.	--	--	--	--	--	--	--	--	--	--
NJ01	06-01-99	1020	do.	.16	.078	<.007	<.024	E.001	<.01	<.008	<.26	<.012	.045
NJ02	05-27-99	1330	do.	<.009	.033	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
NJ03	05-27-99	1550	do.	<.009	E.013	<.007	--	E.019	E.013	<.008	--	<.012	<.018
NJ04	05-27-99	1120	do.	<.009	E.015	.096	--	.039	.020	<.008	--	E.021	<.018
NY01	03-28-00	1310	do.	<.009	<.014	<.007	--	<.023	<.01	<.008	--	<.012	<.018
NY02	08-08-00	1150	do.	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
NY03	08-23-00	1340	do.	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
NY04	08-08-00	1100	do.	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
NY05	08-08-00	1300	do.	<.009	.019	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
NY06	08-08-00	1500	do.	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
NY07	08-08-00	1410	do.	.059	.23	<.007	<.024	E.002	<.01	<.008	<.26	<.012	<.018
NY07	08-08-00	1415	duplicate	.055	.24	<.007	<.024	E.001	<.01	<.008	<.26	<.012	<.018
NY08	08-30-00	1430	regular	<.009	E.003	<.007	E.009	<.023	<.01	<.008	<.26	<.012	E.01
NY09	08-10-00	1215	do.	<.009	.083	<.007	<.024	<.023	<.01	<.008	<.26	<.012	.021
NY10	08-10-00	1120	do.	.45	E4.7	<.007	<.024	.21	<.01	<.008	<.26	<.012	1.9
NY11	08-10-00	1609	blank	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
NY11	08-10-00	1625	regular	E9.4	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
NY12	08-10-00	1515	do.	<.009	.025	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
OH01	05-18-99	1330	do.	.027	.14	<.007	<.024	E.002	<.01	<.008	<.26	<.012	<.018
OH02	05-24-99	1015	do.	--	--	--	--	--	--	--	--	--	--
OH03	05-06-99	1045	do.	--	--	--	--	--	--	--	--	--	--
OH04	05-06-99	1340	do.	--	--	--	--	--	--	--	--	--	--
OH05	05-20-99	1000	do.	<.009	E.006	<.007	--	E.024	<.01	<.008	--	<.012	<.018
OH06	05-24-99	1245	do.	--	--	--	--	--	--	--	--	--	--
OH07	06-02-99	1145	do.	<.009	<.014	<.007	--	.05	.019	<.008	--	.026	<.018
OH08	06-14-99	1120	do.	--	--	--	--	--	--	--	--	--	--
OK01	05-13-99	1315	do.	<.009	.12	<.007	--	E.016	<.01	<.008	--	<.012	<.018
OK03	05-03-99	1045	do.	<.009	.052	<.007	--	<.023	<.01	<.008	--	<.012	<.018
OK04	05-24-99	1300	do.	E.003	<.014	<.007	--	<.023	<.01	<.008	--	E.011	<.018
OR02	07-10-00	1400	do.	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
OR03	06-03-00	1030	do.	<.009	.007	<.007	E.012	<.023	<.01	<.008	<.26	<.012	.048
OR04	07-24-00	1130	do.	<.009	.019	<.007	<.024	<.023	<.01	<.008	<.26	<.012	E.010
PA01	05-24-99	1030	do.	--	--	--	--	--	--	--	--	--	--
PA02	06-08-99	1120	do.	--	--	--	--	--	--	--	--	--	--
PA03	05-27-99	1520	do.	--	--	--	--	--	--	--	--	--	--
PA04	05-27-99	1000	do.	--	--	--	--	--	--	--	--	--	--
PA05	05-27-99	1140	do.	--	--	--	--	--	--	--	--	--	--
TX01	08-09-99	0830	do.	<.009	.05	<.007	--	.059	.027	<.008	--	<.012	<.018
UT01	06-14-99	1230	do.	<.009	<.014	<.007	--	E.017	<.01	<.008	--	<.012	<.018
VA01	08-01-00	1500	do.	E.006	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
WA01	07-19-00	0930	do.	<.009	<.014	<.007	<.024	<.023	<.01	<.008	<.26	<.012	<.018
WA02	05-18-99	1530	do.	<.009	.13	<.007	--	<.023	<.01	<.008	--	<.012	<.018
WA03	05-14-99	1530	do.	--	--	--	--	--	--	--	--	--	--
WA04	05-06-99	1050	do.	<.009	.17	<.007	--	<.023	<.01	<.008	--	<.012	<.018
WA05	05-14-99	1200	do.	--	--	--	--	--	--	--	--	--	--
WA06	03-29-00	1000	do.	<.009	<.014	<.007	--	<.023	<.01	<.008	--	<.012	<.018
WI01	04-23-99	0955	do.	--	--	--	--	--	--	--	--	--	--
WI02	04-23-99	0910	do.	--	--	--	--	--	--	--	--	--	--
WI03	05-17-99	1230	do.	--	--	--	--	--	--	--	--	--	--
WI04	04-23-99	1450	do.	--	--	--	--	--	--	--	--	--	--
WI05	04-23-99	1115	do.	--	--	--	--	--	--	--	--	--	--
WI06	04-23-99	1330	do.	--	--	--	--	--	--	--	--	--	--
WI07	04-23-99	0820	do.	--	--	--	--	--	--	--	--	--	--

Site code

Date (month-day-year)

Time (24-hour)

Type of sample

Acetaminophen (103-90-2)

Caffeine (58-08-2)

Cimetidine (51481-61-9)

Codeine (76-57-3)

Cotinine (486-56-6)

Dehydronifedipine (67035-22-7)

Digoxigenin (1672-46-4)

Digoxin (20830-75-5)

Diltiazem (42399-41-7)

1,7-Dimethylxanthine (611-59-6)

AR02

05-02-99

1630

regular

AR06

05-04-99

2050

do.

AZ01

06-29-00

1115

do.

<0.009

3.3

0.016

<.024

0.099

<.01

<0.008

<.26

<.012

0.84

AZ02

06-27-00

1625

do.

.50

1.2

<.007

<.024

.30

.013

<.008

<.26

.037

1.4

AZ03

06-29-00

0710

do.

.048

3.1

.58

<.024

.69

E.003

<.008

<.26

.034

1.8

AZ04

06-27-00

1035

do.

<.009

<.014

<.007

<.024

E.003

<.01

<.008

<.26

.012

.032

CA01

05-18-00

1130

do.

.025

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

CA02

06-28-00

1300

do.

.39

.68

<.007

E.019

<.023

<.01

<.008

<.26

.017

.21

CA03

08-16-00

1700

do.

<.009

.022

<.007

<.024

.071

<.01

<.008

<.26

<.012

<.018

CA04

08-09-00

1700

do.

<.009

<.014

<.007

<.024

<.023

.012

<.008

<.26

<.012

<.018

CA05

04-15-99

1700

do.

<.009

.11

.12

.048

.030

<.008

<.012

<.018

CA06

04-11-99

0715

do.

CA07

09-21-99

1110

do.

<.009

<.014

<.007

<.023

<.01

<.008

<.012

<.018

CA08

09-21-99

1600

do.

E.004

<.014

<.007

<.023

<.01

<.008

<.012

<.018

CA09

09-22-99

1120

do.

E.004

<.014

<.007

<.023

<.01

<.008

<.012

<.018

CA10

09-22-99

1320

do.

<.009

<.014

<.007

<.023

<.01

<.008

<.012

<.018

CO01

04-21-99

1250

do.

<.009

<.014

<.007

.90

<.01

<.008

.049

.053

DE01

05-23-99

1130

do.

DE01

05-23-99

1140

duplicate

FL01

08-28-00

1215

regular

<.009

.053

<.007

<.024

<.023

<.01

<.008

<.26

<.012

.067

FL02

08-23-00

1215

do.

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

GA01

05-26-99

1400

do.

GA02

05-25-99

1130

do.

GA03

05-25-99

1030

do.

GA04

05-25-99

0840

do.

GA05

05-26-99

1130

do.

<.009

.049

<.007

E.014

<.01

<.008

<.012

<.018

GA06

05-24-99

1215

do.

GA07

05-24-99

1420

do.

<.009

E.001

<.007

<.023

E.001

<.008

E.014

<.018

IA01

09-13-00

1600

do.

<.009

.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

IA02

09-12-00

1200

do.

<.009

.025

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

IA04

09-11-00

1700

do.

<.009

.14

.51

<.024

.024

<.01

<.008

<.26

<.012

.27

IA05

04-05-99

1445

do.

IA07

04-08-99

1000

do.

.018

.07

<.007

<.023

<.01

<.008

<.012

<.018

IA08

04-06-99

0935

do.

IA09

04-06-99

1245

do.

IA10

04-04-99

2000

do.

IA11

04-03-99

1855

do.

IA12

04-03-99

1245

do.

ID01

08-14-00

1110

do.

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

ID02

08-15-00

1250

do.

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

ID03

08-16-00

1222

do.

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

ID04

05-17-00

1215

do.

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

IL01

05-13-99

1300

do.

<.009

.086

<.007

<.023

<.01

<.008

<.012

<.018

IL02

05-17-99

1420

do.

IL03

05-19-99

1400

do.

<.009

.22

<.007

.048

<.01

<.008

<.012

<.018

IL04

05-19-99

1240

do.

<.009

.12

<.007

.026

<.01

<.008

<.012

<.018

IL05

05-20-99

0810

do.

<.009

.056

.053

<.023

E.011

<.008

E.023

<.018

IL06

05-17-99

1230

do.

IL07

05-13-99

1710

do.

LA01

04-19-99

1130

do.

<.009

.068

<.007

<.023

<.01

<.008

<.012

<.018

MA01

05-12-99

0840

do.

<.009

.16

<.007

E.011

<.01

<.008

<.012

<.018

MA02

07-25-00

0630

do.

<.009

.13

<.007

<.024

E.003

<.01

<.008

<.26

<.012

E.017

MA03

07-25-00

0750

blank

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

MA03

07-25-00

0800

regular

<.009

.085

<.007

<.024

E.018

<.01

<.008

<.26

<.012

<.018

MA03

07-25-00

0810

duplicate

E.007

.067

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

MA04

07-25-00

0900

regular

.40

.74

E.004

<.024

.15

<.01

<.008

<.26

<.012

3.1

MA05

07-25-00

1100

do.

.010

.69

<.007

<.024

E.006

<.01

<.008

<.26

<.012

.26

MA06

07-25-00

1010

do.

.94

2.1

<.007

<.024

.031

<.01

<.008

<.26

E.011

.60

MA07

07-25-00

1130

do.

<.009

.048

<.007

<.024

E.021

<.01

<.008

<.26

<.012

.057

MD01

09-17-99

0930

do.

MD02

05-19-99

1710

do.

MI01

06-15-99

1030

do.

MI02

06-15-99

1430

do.

MI03

06-16-99

1045

do.

<.009

<.014

E.012

<.023

<.01

<.008

<.012

<.018

MN03

10-03-00

1105

blank

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

MN03

10-03-00

1115

do.

<.009

E.002

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

MN04

07-13-99

1300

do.

<.009

E.009

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

MO01

05-06-99

1130

do.

<.009

.75

<.007

E.016

<.01

<.008

<.012

.097

MO02

04-29-99

1245

do.

E6.0

<.007

.22

<.01

<.008

<.012

1.9

MO03

04-30-99

0830

do.

.24

.68

<.007

<.024

<.023

<.01

<.008

<.26

<.012

.29

MO04

04-30-99

1300

do.

.54

.24

<.007

<.024

<.023

<.01

<.008

<.26

<.012

.13

MO05

05-15-99

1315

do.

<.009

<.014

<.007

<.023

<.01

<.008

<.012

<.018

MO06

04-07-99

0845

do.

MO07

04-05-99

1530

do.

MO08

04-07-99

0840

do.

<.009

.079

<.007

E.02

E.005

<.008

<.012

<.018

MT01

03-16-00

1040

do.

<.009

<.014

<.007

<.023

<.01

<.008

<.012

<.018

MT02

03-16-00

1400

do.

<.009

<.014

<.007

<.023

<.01

<.008

<.012

<.018

MT03

03-17-00

1100

do.

<.009

<.014

<.007

<.023

<.01

<.008

<.012

.061

MT04

03-06-00

1400

do.

<.009

.057

<.007

<.023

<.01

<.008

<.012

<.018

MT05

03-22-00

1130

do.

<.009

<.014

<.007

<.023

<.01

<.008

<.012

<.018

NC01

05-06-99

1015

do.

NC02

05-06-99

1230

do.

NC03

05-06-99

1430

do.

NC04

05-06-99

1545

do.

NC05

05-13-99

1245

do.

NE01

06-24-99

1330

do.

NE02

06-15-99

1730

do.

NE03

06-14-99

1600

do.

NE04

06-15-99

1700

do.

NE05

06-03-99

1230

do.

NE06

06-04-99

1030

do.

NE07

06-17-99

1130

do.

NJ01

06-01-99

1020

do.

.16

.078

<.007

<.024

E.001

<.01

<.008

<.26

<.012

.045

NJ02

05-27-99

1330

do.

<.009

.033

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

NJ03

05-27-99

1550

do.

<.009

E.013

<.007

E.019

E.013

<.008

<.012

<.018

NJ04

05-27-99

1120

do.

<.009

E.015

.096

.039

.020

<.008

E.021

<.018

NY01

03-28-00

1310

do.

<.009

<.014

<.007

<.023

<.01

<.008

<.012

<.018

NY02

08-08-00

1150

do.

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

NY03

08-23-00

1340

do.

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

NY04

08-08-00

1100

do.

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

NY05

08-08-00

1300

do.

<.009

.019

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

NY06

08-08-00

1500

do.

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

NY07

08-08-00

1410

do.

.059

.23

<.007

<.024

E.002

<.01

<.008

<.26

<.012

<.018

NY07

08-08-00

1415

duplicate

.055

.24

<.007

<.024

E.001

<.01

<.008

<.26

<.012

<.018

NY08

08-30-00

1430

regular

<.009

E.003

<.007

E.009

<.023

<.01

<.008

<.26

<.012

E.01

NY09

08-10-00

1215

do.

<.009

.083

<.007

<.024

<.023

<.01

<.008

<.26

<.012

.021

NY10

08-10-00

1120

do.

.45

E4.7

<.007

<.024

.21

<.01

<.008

<.26

<.012

1.9

NY11

08-10-00

1609

blank

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

NY11

08-10-00

1625

regular

E9.4

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

NY12

08-10-00

1515

do.

<.009

.025

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

OH01

05-18-99

1330

do.

.027

.14

<.007

<.024

E.002

<.01

<.008

<.26

<.012

<.018

OH02

05-24-99

1015

do.

OH03

05-06-99

1045

do.

OH04

05-06-99

1340

do.

OH05

05-20-99

1000

do.

<.009

E.006

<.007

E.024

<.01

<.008

<.012

<.018

OH06

05-24-99

1245

do.

OH07

06-02-99

1145

do.

<.009

<.014

<.007

.05

.019

<.008

.026

<.018

OH08

06-14-99

1120

do.

OK01

05-13-99

1315

do.

<.009

.12

<.007

E.016

<.01

<.008

<.012

<.018

OK03

05-03-99

1045

do.

<.009

.052

<.007

<.023

<.01

<.008

<.012

<.018

OK04

05-24-99

1300

do.

E.003

<.014

<.007

<.023

<.01

<.008

E.011

<.018

OR02

07-10-00

1400

do.

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

OR03

06-03-00

1030

do.

<.009

.007

<.007

E.012

<.023

<.01

<.008

<.26

<.012

.048

OR04

07-24-00

1130

do.

<.009

.019

<.007

<.024

<.023

<.01

<.008

<.26

<.012

E.010

PA01

05-24-99

1030

do.

PA02

06-08-99

1120

do.

PA03

05-27-99

1520

do.

PA04

05-27-99

1000

do.

PA05

05-27-99

1140

do.

TX01

08-09-99

0830

do.

<.009

.05

<.007

.059

.027

<.008

<.012

<.018

UT01

06-14-99

1230

do.

<.009

<.014

<.007

E.017

<.01

<.008

<.012

<.018

VA01

08-01-00

1500

do.

E.006

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

WA01

07-19-00

0930

do.

<.009

<.014

<.007

<.024

<.023

<.01

<.008

<.26

<.012

<.018

WA02

05-18-99

1530

do.

<.009

.13

<.007

<.023

<.01

<.008

<.012

<.018

WA03

05-14-99

1530

do.

WA04

05-06-99

1050

do.

<.009

.17

<.007

<.023

<.01

<.008

<.012

<.018

WA05

05-14-99

1200

do.

WA06

03-29-00

1000

do.

<.009

<.014

<.007

<.023

<.01

<.008

<.012

<.018

WI01

04-23-99

0955

do.

WI02

04-23-99

0910

do.

WI03

05-17-99

1230

do.

WI04

04-23-99

1450

do.

WI05

04-23-99

1115

do.

WI06

04-23-99

1330

do.

WI07

04-23-99

0820

do.

Site code	Date (month-day-year)	Time (24-hour)	Type of sample	Enalaprilat (76420-72-9)	Fluoxetine (54910-89-3)	Gemfibrozil (25812-30-0)	Ibuprofen (15687-27-1)	Metformin (657-24-9)	Paroxetine metabolite	Ranitidine (66357-35-5)	Albuterol (18559-94-9)	Sulfamethoxazole (723-46-6)	Trimethoprim (738-70-5)	Warfarin (81-81-2)
AR02	05-02-99	1630	regular	--	--	--	--	--	--	--	--	--	--	--
AR06	05-04-99	2050	do.	--	--	--	--	--	--	--	--	--	--	--
AZ01	06-29-00	1115	do.	<0.152	<.018	<.015	<.018	<0.003	<.26	<0.01	<0.029	.39	0.20	<.001
AZ02	06-27-00	1625	do.	<.152	<.018	<.015	.36	<.003	<.26	<.01	<.029	.52	.048	<.001
AZ03	06-29-00	0710	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	.35	.11	<.001
AZ04	06-27-00	1035	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	.049	<.014	<.001
CA01	05-18-00	1130	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
CA02	06-28-00	1300	do.	<.152	<.018	.031	.16	<.003	<.26	<.01	<.029	<.023	.030	<.001
CA03	08-16-00	1700	do.	<.152	E.012	<.015	<.018	<.003	<.26	<.01	<.029	.16	<.014	<.001
CA04	08-09-00	1700	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	E.004	<.001
CA05	04-15-99	1700	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	.058	<.001
CA06	04-11-99	0715	do.	--	--	--	--	--	--	--	--	--	--	--
CA07	09-21-99	1110	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
CA08	09-21-99	1600	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
CA09	09-22-99	1120	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
CA10	09-22-99	1320	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
CO01	04-21-99	1250	do.	<.152	<.018	.79	<.018	<.003	<.26	<.01	<.029	<.023	.30	<.001
DE01	05-23-99	1130	do.	--	--	--	--	--	--	--	--	--	--	--
DE01	05-23-99	1140	duplicate	--	--	--	--	--	--	--	--	--	--	--
FL01	08-28-00	1215	regular	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
FL02	08-23-00	1215	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
GA01	05-26-99	1400	do.	--	--	--	--	--	--	--	--	--	--	--
GA02	05-25-99	1130	do.	--	--	--	--	--	--	--	--	--	--	--
GA03	05-25-99	1030	do.	--	--	--	--	--	--	--	--	--	--	--
GA04	05-25-99	0840	do.	--	--	--	--	--	--	--	--	--	--	--
GA05	05-26-99	1130	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
GA06	05-24-99	1215	do.	--	--	--	--	--	--	--	--	--	--	--
GA07	05-24-99	1420	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	.16	.036	<.001
IA01	09-13-00	1600	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	E.004	<.014	<.001
IA02	09-12-00	1200	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
IA04	09-11-00	1700	do.	<.152	<.018	<.015	<.018	<.003	<.26	.014	<.029	.088	.022	<.001
IA05	04-05-99	1445	do.	--	--	--	--	--	--	--	--	--	--	--
IA07	04-08-99	1000	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
IA08	04-06-99	0935	do.	--	--	--	--	--	--	--	--	--	--	--
IA09	04-06-99	1245	do.	--	--	--	--	--	--	--	--	--	--	--
IA10	04-04-99	2000	do.	--	--	--	--	--	--	--	--	--	--	--
IA11	04-03-99	1855	do.	--	--	--	--	--	--	--	--	--	--	--
IA12	04-03-99	1245	do.	--	--	--	--	--	--	--	--	--	--	--
ID01	08-14-00	1110	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
ID02	08-15-00	1250	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
ID03	08-16-00	1222	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
ID04	05-17-00	1215	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
IL01	05-13-99	1300	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
IL02	05-17-99	1420	do.	--	--	--	--	--	--	--	--	--	--	--
IL03	05-19-99	1400	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	E.013	<.001
IL04	05-19-99	1240	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	E.012	<.001
IL05	05-20-99	0810	do.	<.152	<.018	<.015	<.018	.14	<.26	<.01	<.029	.099	.060	<.001
IL06	05-17-99	1230	do.	--	--	--	--	--	--	--	--	--	--	--
IL07	05-13-99	1710	do.	--	--	--	--	--	--	--	--	--	--	--
LA01	04-19-99	1130	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MA01	05-12-99	0840	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	E.005	<.001
MA02	07-25-00	0630	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MA03	07-25-00	0750	blank	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MA03	07-25-00	0800	regular	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MA03	07-25-00	0810	duplicate	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MA04	07-25-00	0900	regular	<.152	<.018	<.015	.45	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MA05	07-25-00	1100	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MA06	07-25-00	1010	do.	<.152	<.018	<.015	.10	<.003	<.26	<.01	<.029	<.023	E.001	<.001
MA07	07-25-00	1130	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MD01	09-17-99	0930	do.	--	--	--	--	--	--	--	--	--	--	--
MD02	05-19-99	1710	do.	--	--	--	--	--	--	--	--	--	--	--
MI01	06-15-99	1030	do.	--	--	--	--	--	--	--	--	--	--	--
MI02	06-15-99	1430	do.	--	--	--	--	--	--	--	--	--	--	--
MI03	06-16-99	1045	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	E.011	<.001
MN03	10-03-00	1105	blank	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MN03	10-03-00	1115	regular	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MN04	07-13-99	1300	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	E.009	<.014	<.001
MO01	05-06-99	1130	do.	<.152	<.018	.048	.11	<.003	<.26	<.01	<.029	<.023	E.011	<.001
MO02	04-29-99	1245	do.	<.152	<.018	<.015	1.0	<.003	<.26	<.01	<.029	<.023	E.023	<.001
MO03	04-30-99	0830	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MO04	04-30-99	1300	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MO05	05-15-99	1315	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MO06	04-07-99	0845	do.	--	--	--	--	--	--	--	--	--	--	--
MO07	04-05-99	1530	do.	--	--	--	--	--	--	--	--	--	--	--
MO08	04-07-99	0840	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	E.009	<.001
MT01	03-16-00	1040	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MT02	03-16-00	1400	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MT03	03-17-00	1100	do.	.046	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MT04	03-06-00	1400	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
MT05	03-22-00	1130	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
NC01	05-06-99	1015	do.	--	--	--	--	--	--	--	--	--	--	--
NC02	05-06-99	1230	do.	--	--	--	--	--	--	--	--	--	--	--
NC03	05-06-99	1430	do.	--	--	--	--	--	--	--	--	--	--	--
NC04	05-06-99	1545	do.	--	--	--	--	--	--	--	--	--	--	--
NC05	05-13-99	1245	do.	--	--	--	--	--	--	--	--	--	--	--
NE01	06-24-99	1330	do.	--	--	--	--	--	--	--	--	--	--	--
NE02	06-15-99	1730	do.	--	--	--	--	--	--	--	--	--	--	--
NE03	06-14-99	1600	do.	--	--	--	--	--	--	--	--	--	--	--
NE04	06-15-99	1700	do.	--	--	--	--	--	--	--	--	--	--	--
NE05	06-03-99	1230	do.	--	--	--	--	--	--	--	--	--	--	--
NE06	06-04-99	1030	do.	--	--	--	--	--	--	--	--	--	--	--
NE07	06-17-99	1130	do.	--	--	--	--	--	--	--	--	--	--	--
NJ01	06-01-99	1020	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
NJ02	05-27-99	1330	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
NJ03	05-27-99	1550	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
NJ04	05-27-99	1120	do.	<.152	<.018	<.015	<.018	.08	<.26	<.01	<.029	<.023	.078	<.001
NY01	03-28-00	1310	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
NY02	08-08-00	1150	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
NY03	08-23-00	1340	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
NY04	08-08-00	1100	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
NY05	08-08-00	1300	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	E.002	<.014	<.001
NY06	08-08-00	1500	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	E.003	<.014	<.001
NY07	08-08-00	1410	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	.071	E.009	<.001
NY07	08-08-00	1415	duplicate	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	.075	E.009	<.001
NY08	08-30-00	1430	regular	<.152	<.018	<.015	E.032	<.003	<.26	<.01	<.029	.061	E.008	<.001
NY09	08-10-00	1215	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
NY10	08-10-00	1120	do.	<.152	<.018	<.015	.24	<.003	<.26	<.01	<.029	<.023	<.014	<.001
NY11	08-10-00	1609	blank	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
NY11	08-10-00	1625	regular	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
NY12	08-10-00	1515	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
OH01	05-18-99	1330	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
OH02	05-24-99	1015	do.	--	--	--	--	--	--	--	--	--	--	--
OH03	05-06-99	1045	do.	--	--	--	--	--	--	--	--	--	--	--
OH04	05-06-99	1340	do.	--	--	--	--	--	--	--	--	--	--	--
OH05	05-20-99	1000	do.	<.152	<.018	<.015	<.018	.042	<.26	<.01	<.029	<.023	E.01	<.001
OH06	05-24-99	1245	do.	--	--	--	--	--	--	--	--	--	--	--
OH07	06-02-99	1145	do.	<.152	<.018	<.015	<.018	0.15	<.26	<.01	<.029	<.023	<.014	<.001
OH08	06-14-99	1120	do.	--	--	--	--	--	--	--	--	--	--	--
OK01	05-13-99	1315	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
OK03	05-03-99	1045	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
OK04	05-24-99	1300	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
OR02	07-10-00	1400	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
OR03	06-03-00	1030	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	.004	E.005	<.001
OR04	07-24-00	1130	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
PA01	05-24-99	1030	do.	--	--	--	--	--	--	--	--	--	--	--
PA02	06-08-99	1120	do.	--	--	--	--	--	--	--	--	--	--	--
PA03	05-27-99	1520	do.	--	--	--	--	--	--	--	--	--	--	--
PA04	05-27-99	1000	do.	--	--	--	--	--	--	--	--	--	--	--
PA05	05-27-99	1150	do.	--	--	--	--	--	--	--	--	--	--	--
TX01	08-09-99	0830	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
UT01	06-14-99	1140	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	E.023	<.014	<.001
VA01	08-01-00	1500	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
WA01	07-19-00	0930	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
WA02	05-18-99	1530	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
WA03	05-14-99	1530	do.	--	--	--	--	--	--	--	--	--	--	--
WA04	05-06-99	1050	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
WA05	05-14-99	1200	do.	--	--	--	--	--	--	--	--	--	--	--
WA06	03-29-00	1000	do.	<.152	<.018	<.015	<.018	<.003	<.26	<.01	<.029	<.023	<.014	<.001
WI01	04-23-99	0955	do.	--	--	--	--	--	--	--	--	--	--	--
WI02	04-23-99	0910	do.	--	--	--	--	--	--	--	--	--	--	--
WI03	05-17-99	1230	do.	--	--	--	--	--	--	--	--	--	--	--
WI04	04-23-99	1450	do.	--	--	--	--	--	--	--	--	--	--	--
WI05	04-23-99	1115	do.	--	--	--	--	--	--	--	--	--	--	--
WI06	04-23-99	1330	do.	--	--	--	--	--	--	--	--	--	--	--
WI07	04-23-99	0820	do.	--	--	--	--	--	--	--	--	--	--	--

Site code

Date (month-day-year)

Time (24-hour)

Type of sample

Enalaprilat (76420-72-9)

Fluoxetine (54910-89-3)

Gemfibrozil (25812-30-0)

Ibuprofen (15687-27-1)

Metformin (657-24-9)

Paroxetine metabolite

Ranitidine (66357-35-5)

Albuterol (18559-94-9)

Sulfamethoxazole (723-46-6)

Trimethoprim (738-70-5)

Warfarin (81-81-2)

AR02

05-02-99

1630

regular

AR06

05-04-99

2050

do.

AZ01

06-29-00

1115

do.

<0.152

<.018

<.015

<.018

<0.003

<.26

<0.01

<0.029

.39

0.20

<.001

AZ02

06-27-00

1625

do.

<.152

<.018

<.015

.36

<.003

<.26

<.01

<.029

.52

.048

<.001

AZ03

06-29-00

0710

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

.35

.11

<.001

AZ04

06-27-00

1035

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

.049

<.014

<.001

CA01

05-18-00

1130

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

CA02

06-28-00

1300

do.

<.152

<.018

.031

.16

<.003

<.26

<.01

<.029

<.023

.030

<.001

CA03

08-16-00

1700

do.

<.152

E.012

<.015

<.018

<.003

<.26

<.01

<.029

.16

<.014

<.001

CA04

08-09-00

1700

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

E.004

<.001

CA05

04-15-99

1700

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

.058

<.001

CA06

04-11-99

0715

do.

CA07

09-21-99

1110

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

CA08

09-21-99

1600

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

CA09

09-22-99

1120

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

CA10

09-22-99

1320

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

CO01

04-21-99

1250

do.

<.152

<.018

.79

<.018

<.003

<.26

<.01

<.029

<.023

.30

<.001

DE01

05-23-99

1130

do.

DE01

05-23-99

1140

duplicate

FL01

08-28-00

1215

regular

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

FL02

08-23-00

1215

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

GA01

05-26-99

1400

do.

GA02

05-25-99

1130

do.

GA03

05-25-99

1030

do.

GA04

05-25-99

0840

do.

GA05

05-26-99

1130

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

GA06

05-24-99

1215

do.

GA07

05-24-99

1420

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

.16

.036

<.001

IA01

09-13-00

1600

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

E.004

<.014

<.001

IA02

09-12-00

1200

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

IA04

09-11-00

1700

do.

<.152

<.018

<.015

<.018

<.003

<.26

.014

<.029

.088

.022

<.001

IA05

04-05-99

1445

do.

IA07

04-08-99

1000

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

IA08

04-06-99

0935

do.

IA09

04-06-99

1245

do.

IA10

04-04-99

2000

do.

IA11

04-03-99

1855

do.

IA12

04-03-99

1245

do.

ID01

08-14-00

1110

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

ID02

08-15-00

1250

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

ID03

08-16-00

1222

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

ID04

05-17-00

1215

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

IL01

05-13-99

1300

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

IL02

05-17-99

1420

do.

IL03

05-19-99

1400

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

E.013

<.001

IL04

05-19-99

1240

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

E.012

<.001

IL05

05-20-99

0810

do.

<.152

<.018

<.015

<.018

.14

<.26

<.01

<.029

.099

.060

<.001

IL06

05-17-99

1230

do.

IL07

05-13-99

1710

do.

LA01

04-19-99

1130

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MA01

05-12-99

0840

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

E.005

<.001

MA02

07-25-00

0630

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MA03

07-25-00

0750

blank

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MA03

07-25-00

0800

regular

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MA03

07-25-00

0810

duplicate

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MA04

07-25-00

0900

regular

<.152

<.018

<.015

.45

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MA05

07-25-00

1100

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MA06

07-25-00

1010

do.

<.152

<.018

<.015

.10

<.003

<.26

<.01

<.029

<.023

E.001

<.001

MA07

07-25-00

1130

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MD01

09-17-99

0930

do.

MD02

05-19-99

1710

do.

MI01

06-15-99

1030

do.

MI02

06-15-99

1430

do.

MI03

06-16-99

1045

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

E.011

<.001

MN03

10-03-00

1105

blank

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MN03

10-03-00

1115

regular

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MN04

07-13-99

1300

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

E.009

<.014

<.001

MO01

05-06-99

1130

do.

<.152

<.018

.048

.11

<.003

<.26

<.01

<.029

<.023

E.011

<.001

MO02

04-29-99

1245

do.

<.152

<.018

<.015

1.0

<.003

<.26

<.01

<.029

<.023

E.023

<.001

MO03

04-30-99

0830

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MO04

04-30-99

1300

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MO05

05-15-99

1315

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MO06

04-07-99

0845

do.

MO07

04-05-99

1530

do.

MO08

04-07-99

0840

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

E.009

<.001

MT01

03-16-00

1040

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MT02

03-16-00

1400

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MT03

03-17-00

1100

do.

.046

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MT04

03-06-00

1400

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

MT05

03-22-00

1130

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

NC01

05-06-99

1015

do.

NC02

05-06-99

1230

do.

NC03

05-06-99

1430

do.

NC04

05-06-99

1545

do.

NC05

05-13-99

1245

do.

NE01

06-24-99

1330

do.

NE02

06-15-99

1730

do.

NE03

06-14-99

1600

do.

NE04

06-15-99

1700

do.

NE05

06-03-99

1230

do.

NE06

06-04-99

1030

do.

NE07

06-17-99

1130

do.

NJ01

06-01-99

1020

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

NJ02

05-27-99

1330

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

NJ03

05-27-99

1550

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

NJ04

05-27-99

1120

do.

<.152

<.018

<.015

<.018

.08

<.26

<.01

<.029

<.023

.078

<.001

NY01

03-28-00

1310

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

NY02

08-08-00

1150

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

NY03

08-23-00

1340

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

NY04

08-08-00

1100

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

NY05

08-08-00

1300

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

E.002

<.014

<.001

NY06

08-08-00

1500

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

E.003

<.014

<.001

NY07

08-08-00

1410

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

.071

E.009

<.001

NY07

08-08-00

1415

duplicate

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

.075

E.009

<.001

NY08

08-30-00

1430

regular

<.152

<.018

<.015

E.032

<.003

<.26

<.01

<.029

.061

E.008

<.001

NY09

08-10-00

1215

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

NY10

08-10-00

1120

do.

<.152

<.018

<.015

.24

<.003

<.26

<.01

<.029

<.023

<.014

<.001

NY11

08-10-00

1609

blank

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

NY11

08-10-00

1625

regular

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

NY12

08-10-00

1515

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

OH01

05-18-99

1330

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

OH02

05-24-99

1015

do.

OH03

05-06-99

1045

do.

OH04

05-06-99

1340

do.

OH05

05-20-99

1000

do.

<.152

<.018

<.015

<.018

.042

<.26

<.01

<.029

<.023

E.01

<.001

OH06

05-24-99

1245

do.

OH07

06-02-99

1145

do.

<.152

<.018

<.015

<.018

0.15

<.26

<.01

<.029

<.023

<.014

<.001

OH08

06-14-99

1120

do.

OK01

05-13-99

1315

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

OK03

05-03-99

1045

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

OK04

05-24-99

1300

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

OR02

07-10-00

1400

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

OR03

06-03-00

1030

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

.004

E.005

<.001

OR04

07-24-00

1130

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

PA01

05-24-99

1030

do.

PA02

06-08-99

1120

do.

PA03

05-27-99

1520

do.

PA04

05-27-99

1000

do.

PA05

05-27-99

1150

do.

TX01

08-09-99

0830

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

UT01

06-14-99

1140

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

E.023

<.014

<.001

VA01

08-01-00

1500

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

WA01

07-19-00

0930

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

WA02

05-18-99

1530

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

WA03

05-14-99

1530

do.

WA04

05-06-99

1050

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

WA05

05-14-99

1200

do.

WA06

03-29-00

1000

do.

<.152

<.018

<.015

<.018

<.003

<.26

<.01

<.029

<.023

<.014

<.001

WI01

04-23-99

0955

do.

WI02

04-23-99

0910

do.

WI03

05-17-99

1230

do.

WI04

04-23-99

1450

do.

WI05

04-23-99

1115

do.

WI06

04-23-99

1330

do.

WI07

04-23-99

0820

do.